• Journal of the Korean institute of surface engineering
• /
• v.44 no.2
• /
• pp.60-67
• /
• 2011

Ternary B-C-N coatings were deposited on Si(100) wafer substrate from $B_4C$ target by RF magnetron sputtering technique in $Ar+N_2+CH_4$ gas mixture. In this work, the effect of reactant gas ratio, $CH_4/(N_2+CH_4)$ on the composition, kinds and amounts of bonding states comprising B-C-N coatings were investigated using two different bias power sources of continuous and unipolar DCs. In addition, the tribological properties of coatings were studied with the composition and bonding state of coating. It was found that the substrate bias power had an effect on chemical composition, and all of the obtained coatings were nearly amorphous. Main bonding states of coatings were revealed from FTIR analyses to be h-BN, C-C, C-N, and B-C. The amount of C-C bonging mainly increased with increase of the reactant gas ratio. From our studies, both C-C and h-BN bonding states improved the tribological properties but B-C one was found to be harmful on those. The best coating from tribological points of view was found to be $BC_{1.9}N_{2.3}$ composition.

• Tribology and Lubricants
• /
• v.17 no.5
• /
• pp.386-390
• /
• 2001

Monolayers such as self-assembled monolayer (SAM) have received considerable attention to reduce stiction and friction in micro-devices and microelectromechanical systems (MEMS). Various organic molecular films were investigated to obtain better understanding of their tribological behaviors and adhesion property. The organic molecular films studied in this work are: epoxysilane SAMs, octadecyltricholosilane (OST), multi-layers composed of epoxysilane SAMs, poly[styrene-b-(ethylene-co-butylene)-b-styrene](SEBS) and compound of epoxy resin and poly (paraphenylene)(EP/PPP). The pull-off forces of these films were also obtained from force-distance curves measured in static mode of operation of atomic force microscope(AFM). Tribological tests were conducted with a ball-on-flat reciprocating friction tester. The OST showed the lowest pull-off force, indicating its low adhesion property. It was revealed that, the OST, EP/PPP and the multi-layer of epoxysilane SAMs, SEBS and EP/PPP exhibited good tribological properties at the lower load (0.3 N) whereas the OST showed best performance at the higher load (1.8 N).

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
• /
• 2001.06a
• /
• pp.49-54
• /
• 2001

Monolayers such as self-assembled monolayer (SAM) have received considerable attention to reduce stiction and friction in micro-devices and microelectromechanical systems (MEMS). Various organic molecular films were investigated to obtain better understanding of their tribological behaviors and adhesion property. The organic molecular films studied in this work are: epoxysilane SAMs, octadecyltricholosilane (OST), multi-layers composed of epoxysilane SAMs, poly〔styrene-b-(ethylene-co-butylene)-b-styrene〕(SEBS) and compound of epoxy resin and poly (paraphenylene) (EP/PPP). The pull-off forces of these films were also obtained from force-distance curves measured in static mode of operation of atomic force microscope (AFM). Tribological tests were conducted with a ball-on-flat reciprocating friction tester. The OST showed the lowest pull-off force, indicating its low adhesion property. It was revealed that, the OST, EP/PPP and the multi-layer of epoxysilane SAMs, SEBS and EP/PPP exhibited good tribological properties at the lower load (0.3 N) whereas the OST showed best performance at the higher load (1.8 N).

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
• /
• 1998.10a
• /
• pp.82-90
• /
• 1998

Machines that normally operate under fluid film lubricated condition also experience surface damage. This is largely due to the failure of the lubricant film which leads to boundary lubrication. Thus, it is important to have a good understanding of boundary lubrication behavior. In this paper the major tribological parameters that influence the boundary lubrication properties are evaluated. It is shown that disk roughness, hardness and normal load affect the friction and wear of metals in boundary lubrication. Also, the mechanism of surface damage is attributed to abrasion and wear particle interaction.

• The Korean Journal of Ceramics
• /
• v.3 no.3
• /
• pp.169-172
• /
• 1997

Sintered diamond/(WC-Co) composites were prepared by spark plasma sintering technique. Tribological properties were measured at temperatures from RT to $500^{\circ}C$ in sliding tests with alumina ball. They show coefficient of friction of 0.1 and below at RT and wear of the diamond composites is hardly detected. Effects of diamond grit size, diamond content and test temperature on the coefficient of friction and the wear are discussed. The wear scars were analyzed.

• Proceedings of the Korean Institute of Surface Engineering Conference
• /
• 2013.05a
• /
• pp.209-210
• /
• 2013

In this study, the tribological and thermal properties of TiAlCN coatings were investigated to evaluate their feasibility in automobile applications. TiAlCN coatings with carbon compositions between 25 and 65 at.% were prepared by inductively coupled plasma (ICP) assisted sputtering and were annealed at 400, 500, and $600^{\circ}C$ in air.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.26 no.9
• /
• pp.1842-1848
• /
• 2002

Although DLC coatings have good tribological properties, these are dependant on the deposition method, the property of contact surface, and test condition. Humidity, which has little influence on tribological behavior in macro scale, is an important factor of tribological behavior in small devices like MEMS. The objective of this study is to investigate the tribological behavior of DLC coatings with particular attention to their wettability at various humidities. DLC coatings were deposited on Si substrates and tested using a reciprocating friction tester against Si$_3$N$_4$balls at various humidities. The results showed that the tribological behavior of DLC coatings was dependant on relative humidity and wettablility of DLC coatings. Friction coefficient at high relative humidity was higher thar that at low relative humidity. The tungsten-containing DLC coatings had a good wear resistance at low relative humidity whereas DLC coatings derived from argon(Ar)+cesium(Cs) gases showed a good wear resistance at high relative humidity.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.20 no.5
• /
• pp.1468-1476
• /
• 1996

Surface integrity is dictated by the fabrication process of the metal part. In this work, steel specimens were prepared under various mechine conditions to achieve different degrees of deformation state. The tribological characteristics of the speciments were tested using a pin-on-disk type apparatus and other surface characterization tools. It is shown that though frictional characteristics are similar, the wear rate is significantrly affected by the properties of the surface. In the case of steel, surface cracks resulted in high wear despite the relatively high hardness of the specimen. Also, the sliding action were found to reduce the residual stress on the surface. These results indicate that there is a strong relationship between surface integrity and the tribological properties of steel, and therefore the machining condition should be optimized woth respect to tribological performance of a steel part.

• Tribology and Lubricants
• /
• v.11 no.5
• /
• pp.31-39
• /
• 1995

The surface integrity of a machined surface is an important factor that dictates several performance characteristics of a metal part. In this paper, the surface integrity aspects are presented specifically with respect to the tribological properties of steel. Test specimens were prepared under varying conditions to induce different levels of surface deformation and hardness. Sliding and rolling experiments were performed to assess the friction and wear characteristics of these specimens using a pinon-disk type tribotester and a plate-on-ball type set-up. It is reaffirmed that heat treated steels possess superior sliding and rolling fatigue resistance than raw steel. However, for the case of raw steels machined under varying conditions, the harder specimen resulted in higher wear. This result is attributed to the presence of surface cracks that were induced during machining. The results of such findings will aid in the optimization of surface preparation process for tribological applications of steel.

• Transactions on Electrical and Electronic Materials
• /
• v.7 no.3
• /
• pp.118-122
• /
• 2006

Diamond-like carbon (DLC) films were prepared on silicon substrates by the RF PECVD (Plasma Enhanced Chemical Vapor Deposition) method using methane $(CH_4)$ and hydrogen $(H_2)$ gas. We examined the effects of the post annealing temperature on the tribological properties of the DLC films using friction force microscopy (FFM). The films were annealed at various temperatures ranging from 300 to $900^{\circ}C$ in steps of $200^{\circ}C$ using RTA equipment in nitrogen ambient. The thickness of the film was observed by scanning electron microscopy (SEM) and surface profile analysis. The surface morphology and surface energy of the films were examined using atomic force microscopy and contact angle measurement, respectively. The hardness of the DLC film was measured as a function of the post annealing temperature using a nano-indenter. The tribological characteristics were investigated by atomic force microscopy in FFM mode.