• Title/Summary/Keyword: Titanium carbide

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Microstructure, Mechanical and Wear Properties of Hot-pressed $Si_3N_4-TiC$ Composites

  • Hyun Jin Kim;Soo Whon Lee;Tadachika Nakayama;Koichi Niihara
    • The Korean Journal of Ceramics
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    • v.5 no.4
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    • pp.317-323
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    • 1999
  • Si3N4-TiC composites have been known as electrically conductive ceramics. $Si_3N_4-TiC$ composites with 2 wt% $Al_2O_3$ and 4 wt% $Y_2O_3$ were hot pressed in $N_2$ environment. The mechanical properties including hardness, fracture toughness, and flexural strength and tribological properties were investigated as a function of TiC content. $Si_3N_4-40$ vol% TiC composite was hot pressed at $1,750^{\circ}C$, $1,800^{\circ}C$, and $1,850^{\circ}C$ for 1, 3 and 5 hours in $N_2$ gas. Mechanical and tribolgical properties depended on microstructures, which were controlled by hte TiC content, hot press temperature, and hot press holding time. However, mechanical properties and tribological behaviors were degraded by the chemical reaction between TiC and N. The chemically reacted products such as TiCN, SiC, and $SiO_2$ were detered by the X-ray diffraction analysis.

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Real-Time Prediction of Electrode Wear for the Small Hole Pass-Through by EDM-drill (방전 드릴을 이용한 미세 홀 관통 공정의 전극 소모량 실시간 예측)

  • Choi, Yong-Chan;Huh, Eun-Young;Kim, Jong-Min;Lee, Cheol-Soo
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.22 no.2
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    • pp.268-274
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    • 2013
  • Electric discharge machining drill (EDM-drill) is an efficient process for the fabrication of micro-diameter deep metal hole. As there is non-physical contact between tool (electrode) and workpiece, EDM-drill is widely used to machine the hard machining materials such as high strength steel, cemented carbide, titanium alloys. The electro-thermal energy forces the electrode to wear out together with the workpiece to be machined. The electrode wear occurs inside of a machining hole. and It causes hard to monitor the machining state, which leads the productivity and the quality to decrease. Thus, this study presents a methodology to estimated the electrode wear amount while two coefficients (scale factor and shape factor) of the logarithmic regression model are evaluated from the experiment result. To increase the accuracy of estimation model, the linear transformation method is adopted using the differences of initial electrode wear differences. The estimation model is verified through experiment. The experimental result shows that within minute error, the estimation model is able to predict accurately.

A Study in the Heat Resistance Properties of STD61 Steel using the Surface Hardening Method (STD61 강의 내열특성향상을 위한 표면경화에 관한 연구)

  • Lee, Gu-Hyeon
    • 연구논문집
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    • s.26
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    • pp.121-132
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    • 1996
  • The carburising surface modification treatment of the die steel has been used for improving wear resistance and heat cycle strength of the die and preventing a pitting on the surface because the carbides are forming in the matrix during carburising. Generally, the hot forging die was used after quenching-tempering treatment or nitriding after quenching-tempering treatment. The nitriding after carburising on the surface of a hot die steel and a wear resistance die steels was suggested by SOUCHARD, JACQUOT. and BUVRON. This surface modification treatment improved the adhesive and abrasive wear resistance and friction coefficient. The process was introduced to the forging die of stainless steel, titanium alloy steel, alloy and medium carbon steel and the physical properties of the die after the treatment were improved. The surface hardening treatment of the nitriding, the carburising, the boriding, and TD process were used to improved the life time of the forging die. Also, the coating process of PVD, CVD and PCVD were used and the hard chromium plating was occasionally used. Therefore, this study analyzed the effects of the carburising time and the conditions of nitriding on STD61 steel. The case depth, the surface hardness, the forming carbide size and shape during overcarburising process on the die steel were also examined.

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Shield Material Consideration in the LAR Tokamak Reactor

  • Hong, B.G.
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.08a
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    • pp.314-314
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    • 2010
  • For the optimal design of a tokamak-type reactor, self-consistent determination of a radial build of reactor systems is important and the radial build has to be determined by considering the plasma physics and engineering constraints which inter-relate various reactor systems. In a low aspect ratio (LAR) tokamak reactor with a superconducting toroidal field (TF) coil, the shield should provide sufficient protection for the superconducting TF coil and the shield plays a key role in determining the size of a reactor. To determine the radial build of a reactor, neutronic effects such as tritium breeding in the blanket, nuclear heating, and radiation damage to toroidal field (TF) coil has to be included in the systems analysis. In this work, the outboard blanket only is considered where tritium self-sufficiency is possible by using an inboard neutron reflector instead of breeding blanket. The reflecting shield should provide not only protection for the superconducting TF coil but also improved neutron economy for the tritium breeding in outboard blanket. Tungsten carbide, metal hydride such as titanium hydride and zirconium hydride can be used for improved shielding performance and thus smaller shield thickness. With the use of advanced technology in the shield, conceptual design of a compact superconducting LAR reactor with aspect ratio of less than 2 will be presented as a viable power plant.

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Calibration of Laser Scribe Force Using Finite Element Method (유한요소법을 이용한 레이저 화선력의 보정)

  • Chung, Chul-Sup
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.8 no.6
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    • pp.1319-1324
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    • 2007
  • Accurately controlling the shape of the read/write head structure is critical in the performance of a modem hard disk drive. The sliders investigated are composed of alumina and titanium carbide(AITiC) and act as an air bearing when passing over the disks. Controlling the curvature of the slider is of primary importance. A laser scribing system that produces curvature by inducing residual stress into the slider can be utilized. Predicting the curvature created by a pattern of scribes is of great importance to increase the control over the sliders' shape. The force system that produces stresses similar to the laser scribing is applied to the finite element analysis model. The curvatures created by the force system are calibrated to experimental measurements.

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Enhancement of Wear Resistance of CoCrNiAlTi Plasma Sprayed Coatings Using Titanium Carbide

  • De-Yong Li;Chul-Hee Lee
    • Tribology and Lubricants
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    • v.39 no.1
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    • pp.13-20
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    • 2023
  • Large drill bits may face high hardness ore and high working pressure when working. To optimize the use effect of large drill bits and prolong the use time, it is necessary to add a layer of pressure-resistant, wear-resistant, and low-friction coating on the surface of the drill bit. In this study, CoCrNiAlTi high-entropy alloy coatings and CoCrNiAlTi (70 wt%)-TiC (30 wt%) composite coatings are successfully prepared on Q235 steel by plasma spraying. The CoCrNiAlTi (70 wt%)-TiC (30 wt%) coating consists of FCC solid solution and a small amount of TiC phase. The effect of TiC on the composition phase, microhardness, and elastic modulus of HEA coating is studied by X-ray diffractometer (XRD) and microhardness tester. The effect of TiC on the friction and wear properties of HEA coatings is investigated using a wear tester. By improving the process parameters, the metallurgical bonding between the coating and the substrate is well combined, and a coating without pores and cracks is obtained. The experimental results confirm that the microhardness, elastic modulus, and wear resistance of CoCrNiAlTi-TiC composite coating are better, and the friction coefficient is lower.

Characteristics of Nickel_Titanium Dual-Metal Schottky Contacts Formed by Over-Etching of Field Oxide on Ni/4H-SiC Field Plate Schottky Diode and Improvement of Process (Ni/4H-SiC Field Plate Schottky 다이오드 제작 시 과도 식각에 의해 형성된 Nickel_Titanium 이중 금속 Schottky 접합 특성과 공정 개선 연구)

  • Oh, Myeong-Sook;Lee, Jong-Ho;Kim, Dae-Hwan;Moon, Jeong-Hyun;Yim, Jeong-Hyuk;Lee, Do-Hyun;Kim, Hyeong-Joon
    • Korean Journal of Materials Research
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    • v.19 no.1
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    • pp.28-32
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    • 2009
  • Silicon carbide (SiC) is a promising material for power device applications due to its wide band gap (3.26 eV for 4H-SiC), high critical electric field and excellent thermal conductivity. The Schottky barrier diode is the representative high-power device that is currently available commercially. A field plate edge-terminated 4H-SiC was fabricated using a lift-off process for opening the Schottky contacts. In this case, Ni/Ti dual-metal contacts were unintentionally formed at the edge of the Schottky contacts and resulted in the degradation of the electrical properties of the diodes. The breakdown voltage and Schottky barrier height (SBH, ${\Phi}_B$) was 107 V and 0.67 eV, respectively. To form homogeneous single-metal Ni/4H-SiC Schottky contacts, a deposition and etching method was employed, and the electrical properties of the diodes were improved. The modified SBDs showed enhanced electrical properties, as witnessed by a breakdown voltage of 635 V, a Schottky barrier height of ${\Phi}_B$=1.48 eV, an ideality factor of n=1.04 (close to one), a forward voltage drop of $V_F$=1.6 V, a specific on resistance of $R_{on}=2.1m{\Omega}-cm^2$ and a power loss of $P_L=79.6Wcm^{-2}$.

Fabrication of Ceramic Particulate Reinforced Steel Composites by Liquid Pressing Infiltration Process (용융가압함침공정을 이용한 세라믹 입자 강화 철강복합재료의 제조성 검증)

  • Cho, Seungchan;Lee, Yeong-Hwan;Ko, Seongmin;Park, Hyeon Jae;Lee, Donghyun;Shin, Sangmin;Jo, Ilguk;Lee, Sang-Kwan;Lee, Sang-Bok
    • Composites Research
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    • v.31 no.4
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    • pp.117-121
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    • 2018
  • Various ceramic particulate such as TiC, $TiB_2$, $Al_2O_3$ reinforced SUS431 matrix composites were successfully fabricated by a novel liquid pressing infiltration process. Microstructures of the SUS431 composite were analyzed to determine manufacturability of composites. $Al_2O_3$-SUS431 composite had lots of defects due to poor wettability between the $Al_2O_3$ and steel matrix. On the other hand, TiC was uniformly dispersed in the SUS431 matrix than $TiB_2$ and $Al_2O_3$ due to good wettability and interfacial properties.

Deformation Property of TiC-Mo Solid Solution Single Crystal at High Temperature by Compression Test (TiC-Mo 고용체 단결정의 고온 압축변형 특성)

  • Shin, Soon-Gi
    • Korean Journal of Materials Research
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    • v.24 no.11
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    • pp.625-631
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    • 2014
  • To investigate the deformation properties of TiC-(5-20) mol% Mo solid solution single crystals at high temperature by compression testing, single crystals of various compositions were grown by the radio frequency floating zone technique and were deformed by compression at temperature from 1250K to 2270K at strain rates from $5.1{\times}10^{-5}$ to $5.9{\times}10^{-3}/s$. The plastic flow property of solid solution single crystals was found to be clearly different among a three-temperature range (low, intermediate and high temperature ranges) whose boundaries were dependent on the strain rate. From the observed property, we conclude that the deformation in the low temperature range is controlled by the Peierls mechanism, in the intermediate temperature range by the dynamic strain aging and in the high temperature range by the solute atmosphere dragging mechanism. The work softening tends to become less evident with an increasing experimental temperature and with a decreasing strain rate. The temperature and strain rate dependence of the critical resolved shear stress is the strongest in the high temperature range. The curves are divided into three parts with different slopes by a transition temperature. The critical resolved shear stress (${\tau}_{0.2}$) at the high temperature range showed that Mo content dependence of ${\tau}_{0.2}$ with temperature and the dependence is very marked at lower temperature. In the higher temperature range, ${\tau}_{0.2}$ increases monotonously with an increasing Mo content.

Corrosion Behaviors of TiC Ceramic Particulate Reinforced Steel Composites Fabricated by Liquid Pressing Infiltration Process in Salt Water Environment (용융가압함침공정으로 제조된 TiC 세라믹 입자 강화 철강복합재의 염수환경에서의 부식 특성)

  • Lee, Yeong-Hwan;Ko, Seongmin;Shin, Sangmin;Cho, Seungchan;Kim, Yangdo;Kim, Junghwan;Lee, Sang-Kwan;Lee, Sang-Bok
    • Composites Research
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    • v.33 no.5
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    • pp.251-255
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    • 2020
  • In this study, TiC ceramic particulate reinforced steel composites was fabricated using a liquid pressing infiltration process. Studies were conducted on microstructure analysis and basic physical properties such as hardness and corrosion characteristics in salt water environment for comparison with commercial nodular cast iron. As a result of comparison of corrosion characteristics in a salt water environment, both corrosion potential and corrosion current density were lower than that of ductile graphite cast iron. The lower calculated corrosion rate confirms that the TiC-Fe metal composite has superior corrosion resistance than the cast iron.