• 소성∙가공
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• 제24권1호
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• pp.5-12
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• 2015

In the current study, fundamental deep drawing characteristics of Ti-6Al-4V alloy sheets were investigated to establish the effect of processing conditions on large size square deep drawn cups. To accomplish this study, FE-simulations (Abaqus) were performed to determine optimum blank size, friction coefficient, the gap between punch and die, etc. The simulated processing parameters were verified experimentally. Based on the FE-simulation results, deep drawing was performed with various blank holding loads and sample sizes. In order to improve the formability of Ti-6Al-4V sheet, various lubricant methods were evaluated. Tensile tests and thickness measurements were conducted on the formed sheets. Processing parameters including blank holding force, lubricants, and optimum blank size, were selected to achieve improved drawing quality. With the optimum processing condition, a $200mm{\times}200mm$ cup was deep drawn successfully.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2008년도 춘계학술대회 논문집
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• pp.435-438
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• 2008

High temperature deformation of Ti-6Al-4V alloy with a lamellar colony microstructure was investigated by hot compression and torsion tests. The torsion and compression tests were carried out under a wide range of temperatures and strain rates with true strain up to 2 and 0.7, respectively. The processing maps were generated on the basis of compression and torsion test data and using the principles of dynamic materials modeling (DMM). The shapes of the strain-stress curves in alpha-beta region and processing maps obtained on the two different tests have been compared with a view to evaluate the effect of the microstructure evolution on the flow softening behavior of Ti-6Al-4V alloy with a lamellar colony microstructure.

• 한국분말재료학회지
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• 제28권5호
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• pp.410-416
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• 2021

Ti-6Al-4V alloy has a wide range of applications, ranging from turbine blades that require smooth surfaces for aerodynamic purposes to biomedical implants, where a certain surface roughness promotes biomedical compatibility. Therefore, it would be advantageous if the high volumetric density is maintained while controlling the surface roughness during the LPBF of Ti-6Al-4V. In this study, the volumetric energy density is varied by independently changing the laser power and scan speed to document the changes in the relative sample density and surface roughness. The results where the energy density is similar but the process parameters are different are compared. For comparable energy density but higher laser power and scan speed, the relative density remained similar at approximately 99%. However, the surface roughness varies, and the maximum increase rate is approximately 172%. To investigate the cause of the increased surface roughness, a nonlinear finite element heat transfer analysis is performed to compare the maximum temperature, cooling rate, and lifetime of the melt pool with different process parameters.

• 한국재료학회지
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• 제31권5호
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• pp.245-254
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• 2021

Wire arc additive manufacturing (WAAM) is being considered as a technology to replace the conventional manufacturing process of titanium alloys. However, coarse β grains, which can extend through several deposited materials, result in strong textures and anisotropy. As a solution, we study the plastic deformation effects of ultrasonic needle peening (UNP) on the microstructure. UNP treated materials deform plastically and the dislocation density increases. Fine α+α' grains with low aspect ratio are observed in the UNP treated specimens. UNP treated WAAM Ti-6Al-4V alloys have higher strength and lower elongation than those characteristics of WAAM Ti-6Al-4V alloys. Due to UNP treatment, the z-axis directional specimens exhibit a greater effect of reducing elongation than do the x-axis directional specimens. The UNP treatment produces fine grains in proportion to the number of times UNP is performed, thereby increasing strength. UNP processes produce a large number of dislocations in the WAAM Ti-6Al-4V alloys, with the most dislocations being formed at the surface.

• 소성∙가공
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• 제33권2호
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• pp.112-117
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• 2024

In this study, the friction and wear characteristics of Inconel 600 in the superplastic forming process of Ti6Al4V were evaluated through pin-on-disc tests. To achieve an efficient and systematic experimental design, the Taguchi method was employed. The wear track of the Inconel 600 pin showed scratches in the sliding contact direction, confirming that the wear mechanism is abrasive wear. Through sensitivity analysis such as ANOVA and Main effects, it was confirmed that both normal force and sliding distance have a significant impact on the wear. Changes in sliding velocity and distance did not affect the friction coefficient, which remained relatively constant at approximately 0.380. The wear prediction model for Inconel 600 in the superplastic forming of Ti6Al4V was constructed, which can be utilized as a guideline for the prediction and management of tool wear.

• Corrosion Science and Technology
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• 제8권4호
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• pp.139-142
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• 2009

Recently, quaternary titanium alloys of the system Ti-Nb-Ta-Zr received considerable research interest as potential implant materials because of their excellent mechanical properties and biocompatibility. However, only few reported works were available on the corrosion behavior of such alloys. Hence, in the present work, electrochemical corrosion of Ti-35Nb-5Ta-7Zr alloy, which has been fabricated by arc melting and heat treatment, was studied in 0.9 wt% NaCl at $37\pm1^{\circ}C$, along with biomedical grade Ti-6Al-4V and CP-Ti. The phase and microstructure of the alloys were investigated employing XRD and SEM. The results of electrochemical studies indicated that the corrosion resistance of the quaternary alloy was inferior to that of Ti-6Al-4V and CP Ti.

• 한국군사과학기술학회지
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• 제5권3호
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• pp.89-97
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• 2002

In this study, the effect of $\alpha$-phase morphology on the dynamic deformation behavior at ultra high strain rate was investigated by EBW(Explosive Bridge Wire) test. All of tests and analyses were conducted on three typical microstructures of Ti-6Al-4V alloy, i.e. equiaxed, widmanstatten and bimodal microstructures. The spall strength and HEL(Hugoniot Elastic Limit) of the specimens that have the thickness of 2mm and 4mm were highest with the bimodal microstructure. These results were similar with previous study which was performed by dynamic torsion test(Kolsky torsion test).

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2002년도 춘계학술대회 논문집
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• pp.177-180
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• 2002

The effects of pressing temperatures on the formability and the microstructural evolution during equal channel angular pressing (ECAP) of lamellar Ti-6Al-4V alloy were investigated in this study. ECAP above isothermally 600$^{\circ}C$ was successful without producing any noticeable segments at the specimen surfaces after a single pass of pressing. After 4 passes of ECA pressing, lamellar microstructures were significantly refined revealing equiaxed grains of 0.3$\mu\textrm{m}$ in diameter consisting of high angle grain boundaries. Also these ultrafine grains were relatively stable with little grain growth when annealed up to 600$^{\circ}C$ for 1hour.

• 한국재료학회지
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• 제14권12호
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• pp.893-899
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• 2004

Even though Ti-6Al-4V has gained popularity as an implant material, the possible dissolution of Al and V ions in body fluids remains a matter of concern. Though commercially pure Ti (Cp-Ti) overcomes this problem, the mechanical strength of pure titanium remains very low. Thus, in this experiment Cp-Ti was processed by Equal channel angular processing (ECAP), in order to increase the mechanical strength. The biocompatibility of ECAP-Ti, Cp-Ti and Ti-6Al-4V was examined by the apatite formation on each sample surface, after treating the surface with 5M NaOH and soaking in Simulated body fluids (SBF). Initially, the samples were mechanically polished on silicone carbide paper (#2000). The polished samples were treated with 5M NaOH solution at $60^{\circ}C$ for 24 hours. The NaOH treated samples were washed gently with distill water and dried at $40^{\circ}C$ for 1 day. The dried samples were heat treated in air at $600^{\circ}C$ for 1 hour. The surface morphology of these samples were studied using SEM and XRD. The SEM studies showed network of pores in all samples. The XRD showed oxide layer formation on Cp-Ti and Ti-6Al-4V. samples. However the oxide layer in ECAP-Ti was not substantial. These samples were immersed in SBF, kept at $36.5^{\circ}C$ for seven days period. At the end of 7 days, the apatite formation was confirmed only on Cp-Ti and was not observed in Ti-6Al-4V and ECAP-Ti. These observations of apatite formation relate to the fact that Cp-Ti showed greater oxide layer than other samples. The apatite examined was confirmed as tricalcium phosphate (TCP) using EDS and XRD.

• Journal of Periodontal and Implant Science
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• 제26권1호
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• pp.143-160
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• 1996

The purpose of this study was to evaluate the response in aspect of attachment and growth rate of osteoblasts and growth rate of osteoblasts and human gingival fibroblasts to the commercially pure titanium(CP titanium)and titanium alloy(Ti-6AI-4V) that are used widely as implant materials, and to obtain the basic information to ideal implant materials. In the studly, commercially pure titanium in first test group, titanium alloy(Ti-6AI-4V) in second test group, cobalt-chrome-molybdenum alloy(Co-Cr-Mo alloy) in positive control group, and tissue culture polystyrene plate in negative control group were used. The results of this study were as follows. 1. Bone marrow cells cultured on CP titanium and Ti-6Al-4V showed significantly greater attachment and growth rate(p(0.05) compared to Co-Cr-Mo alloy in each time. 2. There were no significant differences(p>0.05) in attachment and growth rate of bone marrow cells cultured on CP titanium and Ti-6AI-4V or tissue culture plate. 3. Most bone marrow cells cultured on CP titanium, Ti-6Al-4V and tissue culture plate were attached well to each substratum in first 2days, and then, grew at higher growth rate. On the other hand, some cells cultured on Co-Cr-Mo alloy failed to attach in first 2 days, and then, attached cells grew at lower growth rate than other groups. 4. Attachment and growth rates of gingival fibroblasts cultured on CP titanium and Ti-6Al-4V showed no significant differences(p>0.05) compared to Co-Cr-Mo alloy in 2 days, but significantly greater increase(p<0.05) in 5 and 9 days. 5. There were no significantly differences(p>0.05) between growth rates on gingival fibroblasts cultured on CP titanium, Ti-6Al-4V and tissue culture plate in 2 and 5days, but a significant lower growth rate(p<0.05) on CP titanium and Ti-6Al-4V versus tissue culture plate. 6. Some gingival fibroblasts cultured on all specimen groups failed to attach, but attached cells grew well, especially on CP titanium, Ti-GAl-4V and tissue culture plate. 7. There were no significant differences(P>0.05) between growth rates of both bone marrow cells and gingival fibroblasts cultured on CP titanium and Ti-6AI-4V. As a result of this study, both commercially pure titanium and Ti-6AI-4V showed excellent biocompatibility and there was no significant difference in the cellular response to the both metals. Bone marrow cells cultured on each substratum showed significantly greater growth rate and responded sensitively to cytotoxic effects of metal surfaces compared to gingival fibroblasts. Considering cell response to the substrate, it was likely that the composition itself of titanium metals have no significant effect on the biocompatibility. Further study need to be done to evaluate the influence of surface characteristics on cellular responses.