• Title/Summary/Keyword: Three-dimensional printing dental resin

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Comparison between mechanical properties and biocompatibility of experimental 3D printing denture resins according to photoinitiators (광개시제에 따른 실험용 3D 프린팅 의치상 레진의 기계적 성질과 생체적합성 비교)

  • Park, Da Ryeong;Son, Ju lee
    • Journal of Technologic Dentistry
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    • v.42 no.4
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    • pp.355-361
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    • 2020
  • Purpose: In this study, we added two kinds of photoinitiators (CQ and TPO) to prepare two kinds of denture base resins (Bis-GMA series and UDMA series) for three-dimensional (3D) printing to compare and analyze their mechanical and biological properties and to find the optimal composition. Methods: Control specimens were made using the mold made of polyvinyl siloxane of the same size. Light curing was performed twice for 20 seconds on both the upper and lower surfaces with LED (light emitting diode) light-curing unit (n=10). Experimental 3D printing dental resins were prepared, to which two photoinitiators were added. Digital light processing type 3D printer (EMBER, Autodesk, CA, USA) was used for 3D printing. The specimen size was 64 mm×10 mm×3.3 mm according to ISO 20795-1. The final specimens were tested for flexural strength and flexural modulus, and MTT test was performed. Furthermore, one-way analysis of variance was performed, and the post-test was analyzed by Duncan's test at α=0.05. Results: The flexural strength of both Bis-GMA+CQ (97.12±6.47 MPa) and UDMA+TPO (97.40±3.75 MPa) was significantly higher (p<0.05) in the experimental group. The flexural modulus in the experimental group of UDMA+TPO (2.56±0.06 GPa) was the highest (p<0.05). MTT test revealed that all the experimental groups showed more than 70% cell activity. Conclusion: The composition of UDMA+TPO showed excellent results in flexural strength, flexural modulus, and biocompatibility.

A Study of Three-dimensional evaluation of the accuracy of resin provisional restorations fabricated with the DLP printer (DLP 프린터로 제작된 레진 임시수복물의 3차원적 정확도 평가)

  • Kang, Wol;Lee, Hee-Kyung
    • Journal of Technologic Dentistry
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    • v.42 no.1
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    • pp.35-41
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    • 2020
  • Purpose: The purpose of this study was to evaluate the accuracy of the DLP 3D printer by conducting 3-dimensional assesment of resin provisional restorations. Methods: The first premolar of the maxillary was prepared for the abutment. The abutment was scanned by using a scanner. The provisional restoration was designed by using CAD software. A total of 16 resin provisional restorations were produced using ZD200 and Veltz DLP 3D printer. Scanning was done of resin provisional restorations and 3-dimensional measurement was conducted for accuracy. The mean (SD) of RMS was reported for each group. Independent t-test was used to assess the statistical significance of the results. All analyses were done using SPSS 22.0. Results: The mean ± SD of RMS value for the accuracy of the resin provisional restorations that was fabricated by using ZD200 and Veltz DLP 3D printer were 50.85.±4.64㎛ and 70.33±6.31㎛. Independent t-test showed significant differences between groups(p<0.001). Conclusion: The resin provisional restorations made with DLP 3D printers showed clinically acceptable accuracy.

Observation of thermal properties of dental 3D printer materials (치과용 DLP 3D Printer 가공체의 열특성 관찰)

  • Song, Joon-Boo;Park, Yu-Jin;Choi, Sung-Min
    • Journal of Technologic Dentistry
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    • v.43 no.3
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    • pp.71-76
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    • 2021
  • Purpose: In this study, thermal properties were observed by measuring the extent of thermal expansion and the amount of thermal residue that appears upon burnout on a workpiece made by using a dental digital light processing (DLP) three-dimensional (3D) printer. Methods: Thermal properties of workpieces manufactured by using two 3D printers were observed. The specimens were designed in cylindrical form with dimensions 10 mm in diameter and 10 mm in height. The control specimen was made of wax, and the experimental specimen was made of resin. The thermal expansion rate was measured by applying heat to three types of specimens, and burnout residue was measured. Results: The thermal expansion rate of the wax pattern (WP) specimen was 0.93%±0.05%, of the RP1 specimen was 1.30%±0.08%, and of the RP2 specimen was 1.20%±0.09%. Measuring the recovered residue yielded residual amounts of 0.2% for the WP specimen, 1.1% for the RP2 specimen, and 1.8% for the RP1 specimen. Conclusion: 1. From measurements of the workpieces manufactured by dental DLP 3D printing, the thermal expansion rate was found to be higher than that of wax. 2. As a result of measuring burnout residues on the workpieces manufactured by dental DLP 3D printing, the required summoning temperature to obtain suitable castings was determined to >750℃.

An evaluation of marginal fit of resin single crown manufactured using a dental 3D printer (치과용 3D 프린터를 활용해 제작된 레진 단일치관보철의 변연적합 평가)

  • Ki-Baek Kim
    • Journal of Technologic Dentistry
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    • v.44 no.4
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    • pp.126-131
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    • 2022
  • Purpose: The purpose of this study is to evaluate the quality of dental fixed prostheses fabricated by 3DP (three-dimensional printing). Methods: Ten main models were prepared for the study. Ten specimens were printed by 3DP (3DP group). Ten specimens were fabricated by the lost wax technique and casting method to complete the control group (LWC group). The marginal fit was measured for 20 specimens. The measurement of marginal fit was performed using the silicon replica technique. Finally, the marginal fit of 10 specimens from each group was calculated. An independent sample t-test was run to see if the calculated averages for the two groups were mutually significant (α=0.05). Results: According to the experimental results, the mean marginal fit of the 3DP group was 71.9 ㎛, and the LWC group was 55.3 ㎛. The means of the two groups were found to be significantly different (p<0.001) in the results of the independent sample t-test. Conclusion: The marginal fit of fixed dental prostheses produced by 3DP technology was examined with values greater than those fabricated by traditional technology. However, as it appeared to be a value within the range of clinically acceptable range recommended by numerous studies, it was determined that clinical application would be feasible.

Effect of repair methods and materials on the flexural strength of 3D-printed denture base resin

  • Viotto, Hamile Emanuella do Carmo;Silva, Marcela Dantas Dias;Nunes, Thais Soares Bezerra Santos;Coelho, Sabrina Romao Goncalves;Pero, Ana Carolina
    • The Journal of Advanced Prosthodontics
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    • v.14 no.5
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    • pp.305-314
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    • 2022
  • PURPOSE. The aim of this study was to evaluate the flexural strength of a 3D-printed denture base resin (Cosmos Denture), after different immediate repair techniques with surface treatments and thermocycling. MATERIALS AND METHODS. Rectangular 3D-printed denture base resin (Cosmos Denture) specimens (N = 130) were thermocycled (5,000 cycles, 5℃ and 55℃) before and after the different repair techniques (n = 10 per group) using an autopolymerized acrylic resin (Jet, J) or a hard relining resin (Soft Confort, SC), and different surface treatments: Jet resin monomer for 180 s (MMA), blasting with aluminum oxide (JAT) or erbium: yttrium-aluminum-garnet laser (L). The control group were intact specimens. A three-point flexural strength test was performed, and data (MPa) were analyzed by ANOVA and Games-Howell post hoc test (α = 0.05). Each failure was observed and classified through stereomicroscope images and the surface treatments were viewed by scanning electron microscope (SEM). RESULTS. Control group showed the highest mean of flexural strength, statistically different from the other groups (P < .001), followed by MMA+J group. The groups with L treatment were statistically similar to the MMA groups (P > .05). The JAT+J group was better than the SC and JAT+SC groups (P < .05), but similar to the other groups (P > .05). Adhesive failures were most observed in JAT groups, especially when repaired with SC. The SEM images showed surface changes for all treatments, except JAT alone. CONCLUSION. Denture bases fabricated with 3D-printed resin should be preferably repaired with MMA+J. SC and JAT+SC showed the worst results. Blasting impaired the adhesion of the SC resin.

Creating a digitized database of maxillofacial prostheses (obturators): A pilot study

  • Elbashti, Mahmoud;Hattori, Mariko;Sumita, Yuka;Aswehlee, Amel;Yoshi, Shigen;Taniguchi, Hisashi
    • The Journal of Advanced Prosthodontics
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    • v.8 no.3
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    • pp.219-223
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    • 2016
  • PURPOSE. This study aimed to create a digitized database of fabricated obturators to be kept for patients' potential emergency needs. MATERIALS AND METHODS. A chairside intraoral scanner was used to scan the surfaces of an acrylic resin obturator. The scanned data was recorded and saved as a single standard tessellation language file using a three-dimensional modeling software. A simulated obturator model was manufactured using fused deposition modeling technique in a three-dimensional printer. RESULTS. The entire obturator was successfully scanned regardless of its structural complexity, modeled as three-dimensional data, and stored in the digital system of our clinic at a relatively small size (19.6 MB). A simulated obturator model was then accurately manufactured from these data. CONCLUSION. This study provides a proof-of-concept for the use of digital technology to create a digitized database of obturators for edentulous maxillectomy patients.

Evaluation of dimension stability according to UV-C ultrasonic cleaning of full arch artificial teeth made with DLP printer for photopolymerization (광중합용 DLP 프린터로 제작한 전악 인공치아의 UV-C 초음파 세척에 따른 체적 안정성 평가)

  • Kim, Dong-Yeon;Lee, Gwang-Young
    • Journal of Technologic Dentistry
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    • v.43 no.3
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    • pp.84-92
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    • 2021
  • Purpose: The purpose of this study was to compare the dimension safety evaluation between a general ultrasonic cleaner and an ultrasonic cleaner equipped with UV-C (ultraviolet-C). Methods: An edentulous model was prepared. A denture base and an occlusal rim were fabricated, and scanning was performed. After scanning, a denture base and full arch artificial teeth were designed. The full arch artificial teeth were printed using a three-dimensional printer (n=10). The residual resin was washed with alcohol and then scanned (reference data). The printed specimens were classified and cleaned using a general ultrasonic cleaner (GU group) and an ultrasonic cleaner equipped with UV-C (UC group). After each washing, a rescan was performed (scan data). Reference data and scan data were superimposed using overlapping software. Data were statistically analyzed using the Mann-Whitney test (α=0.05). Results: In the deviation values of full arch artificial teeth, the GU group showed a high deviation of 18.02 ㎛ and the UC group showed a low deviation of 15.02 ㎛. The two groups demonstrated a statistically significant difference (p<0.05). Conclusion: Full arch artificial teeth prepared using photopolymerized resin were deformed according to the temperature of water generated in the ultrasonic cleaner. It is judged that there is no deformation according to the UV-C ultrasonic cleaner.

Comparison of Flexural Strength of Three-Dimensional Printed Three-Unit Provisional Fixed Dental Prostheses according to Build Directions

  • Park, Sang-Mo;Park, Ji-Man;Kim, Seong-Kyun;Heo, Seong-Joo;Koak, Jai-Young
    • Journal of Korean Dental Science
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    • v.12 no.1
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    • pp.13-19
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    • 2019
  • Purpose: The aim of this study was to compare the flexural strength of provisional fixed dental prostheses which was three-dimensional (3D) printed by several build directions. Materials and Methods: A metal jig with two abutment teeth and pontic space in the middle was fabricated. This jig was scanned with a desktop scanner and provisional restoration was designed on dental computer-aided design program. On the preprocessing software, the build angles of the restorations were arranged at $0^{\circ}$, $30^{\circ}$, $45^{\circ}$, $60^{\circ}$, and $90^{\circ}$ and support was added and resultant structure was sliced to a thickness of $100{\mu}m$. Processed restorations were printed with digital light processing type 3D printer using poly methyl meta acrylate-based resin. After washing and post-curing, compressive loading was applied at a speed of 1 mm/min on a metal jig fixed to a universal testing machine. The maximum pressure at which fracture occurred was measured. For the statistical analysis, build direction was set as the independent variable and fracture strength as the dependent variable. One-way analysis of variance and Tukey's post hoc analysis was conducted to compare fracture strength among groups (${\alpha}=0.05$). Result: The mean flexural strength of provisional restoration 3D printed with the build direction of $0^{\circ}$ was $1,053{\pm}168N$; it was $1,183{\pm}188N$ at $30^{\circ}$, $1,178{\pm}81N$ at $45^{\circ}$, $1,166{\pm}133N$ at $60^{\circ}$, and $949{\pm}170N$ at $90^{\circ}$. The group with a build direction of $90^{\circ}$ showed significantly lower flexural strength than other groups (P<0.05). The flexural strength was significantly higher when the build direction was $30^{\circ}$ than when it was $90^{\circ}$ (P<0.01). Conclusion: Among the build directions $0^{\circ}$, $30^{\circ}$, $45^{\circ}$, $60^{\circ}$, and $90^{\circ}$ set for 3D printing of fixed dental prosthesis, an orientation of $30^{\circ}$ is recommended as an effective build direction for 3D printing.

Comparative analysis of strain according to the deposition of a constant temperature water bath of a denture-base artificial tooth produced using three-dimensional printing ultraviolet-curing resin (3D 프린팅용 광경화 수지를 사용하여 제작한 의치상용 인공치아의 항온수조 침적에 따른 변형률 비교 분석)

  • Kim, Dong-Yeon;Lee, Gwang-Young;Kim, Jae-Hong;Yang, Cheon-Seung
    • Journal of Technologic Dentistry
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    • v.42 no.3
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    • pp.202-207
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    • 2020
  • Purpose: This study is a comparative analysis of the strain according to deposition in a constant temperature water bath after manufacturing ultraviolet (UV)-cured artificial teeth. Methods: As a control group, 10 ready-made artificial teeth were selected as the first molar on the right side of the maxilla (RT group). Silicone was used as a duplicate of the artificial denture teeth. Experimental teeth were prepared in two groups using the prepared silicone mold. In the first experimental group, the UV-cured resin was injected into the negative silicone, followed by irradiation with a UV-curing machine for 5 minutes (5M group). In the second experimental group, the UV-cured resin was injected into the negative silicone, and then irradiated for 30 minutes using a UV-curing machine (30M group). The one-way ANOVA was performed, and post-test was analyzed by Tukey. Results: When immersed in a water bath for 15 days, it was found to be -0.3% in the RT group, -0.6% in the 5M group, and -0.7% in the 30M group. The results revealed -0.2% in the RT group, 0.2% in the 5M group, and -0.2% in the 30M group when they were in the bath for 30 days. Conclusion: In the water bath, the swelling was greater when deposited for 1 to 15 days, but was less when deposited for 15 to 30 days.

Internal evaluation of provisional restorations according to the dental CAD/CAM manufacturing method : Three-dimensional superimpositional analysis (치과 CAD/CAM 가공방식에 따른 임시보철물의 내면 적합도 : 3차원 중첩 분석)

  • Kim, Jae-Hong;Kim, Ki-Baek
    • Journal of Technologic Dentistry
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    • v.41 no.2
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    • pp.81-86
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    • 2019
  • Purpose: The purpose of the present study was to compare the internal fit of two different temporary restorations fabricated by dental CAD/CAM system and to evaluate clinical effectiveness. Methods: Composite resin tooth of the maxillary first molar was prepared as occlusal reduction(2.0mm), axial reduction(1mm offset), vertical angle(6 degree) and chamfer margin for a temporary crown and duplicated epoxy die was fabricated. The epoxy dies were used to fabricate provisional restorations by CAD/CAM milling technique or 3D-printing technique. The inner data from all crowns were superimposed on the master die file in the 'best-fit alignment' method using 3D analysis software. Statistical analysis was performed using a Wilcoxon's rank sum test for differences between groups. Results: It showed that the internal RMS(Root Mean Square) values of the additive group were significantly larger than those of other group. No significant differences in internal discrepancies were observed in the temporary crowns among the 2 groups with different manufacturing method. Conclusion: All the groups had the internal fit within the clinical acceptable range (< $50{\mu}m$). The continuous research in the future to be applied clinically for the adaptation of additive manufacturing technique are needed.