• Title/Summary/Keyword: Thermal Cycling Test

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Development of Nanomodified Snow-Melting Concrete Using Low-Temperature Phase-Change Material Impregnated Lightweight Aggregate (저온 상변화 물질 함침 경량골재를 이용한 나노 개질 융설 콘크리트 개발)

  • Kyoung, Joo-Hyun;Kim, Sean-Mi;Hu, Jong-Wan
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.42 no.6
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    • pp.787-792
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    • 2022
  • In winter, the excessive use of deicing salt deteriorates concrete pavement durability. To reduce the amount of deicing salt used, phase-change materials (PCMs) potentially offer an alternative way to melt snow through their latent heat storage characteristics. In this research, thermal energy storage concrete was developed by using PCM-impregnated expanded clay as 50 % replacement to normal aggregate by volume. In addition, to improve the thermal efficiency of PCM lightweight aggregate (PCM-LWA)-incorporated concrete, multi-walled carbon nanotubes (MWCNTs) were incorporated in proportions of 0.10 %, 0.15 %, and 0.20 % by binder weight. Compressive strength testing and programmed thermal cycling were performed to evaluate the mechanical and thermal responses of the PCM-LWA concrete. Results showed a significant strength reduction of 54 % due to the PCM-LWA; however, the thermal performance of the PCM-LWA concrete was greatly improved with the addition of MWCNTs. Thermal test results showed that 0.10 % MWCNT-incorporated concrete had high thermal fatigue resistance as well as uniform heat flow, whereas specimens with 0.15 % and 0.20 % MWCNT content had a reduced thermal response due to supercooling when the ambient temperature was varied between -5℃ and 10℃.

The effect of temperature changes on force level of superelastic nickel-titanium archwires (온도 변화가 교정용 니켈-티타늄 호선의 하중값에 미치는 영향)

  • Chun, Kyoung-Ae;Kim, Kwang-Won;Lim, Sung-Hoon
    • The korean journal of orthodontics
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    • v.37 no.6
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    • pp.432-439
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    • 2007
  • The purpose of this study was to evaluate the influence of intraoral temperature changes on the orthodontic force level of a superelastic nickel-titanium alloy wire. Methods: Nickel-titanium archwires of $0.016"{\times}0.022"$ thickness were tested with a three point bending test setup, and temperature changes were applied. The force level changes according to temperature changes were measured at a 1.5 mm deflection during the loading phase and a 1.5 mm deflection during the unloading phase from a deflection to 3.1mm. Ten cycles of thermal cycling from baseline $(37^{\circ}C)$ to cold $(20^{\circ}C)$ or hot $(50^{\circ}C)$temperature were applied. Results: Alter thermal cycling, the force level during the loading phase decreased and the force level during the unloading phase increased even after the temperature was changed to the initial $37^{\circ}C$. Conclusions: The results suggest that the orthodontic force level can not return to the initial force level after temperature changes. When applying superelastic nickel-titanium archwires, we must consider that a lighter force than the loading force and a heavier force than the unloading force will be applied after intraoral temperature changes caused by eating and drinking.

Effect of Non-Conducting Filler Additions on Anisotropic Conductive Adhesives(ACAs) Properties and the Reliability of ACAs Flip Chip on Organic Substrates (이방성 전도 접착제 물성과 유기 기판 플립 칩의 신뢰성에 미치는 비전도성 충진재의 영향)

  • Im, Myeong-Jin;Baek, Gyeong-Uk
    • Korean Journal of Materials Research
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    • v.10 no.3
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    • pp.184-190
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    • 2000
  • We investigated the effect of filler content on the thermo-mechanical properties of modified ACA composite materials by incorporation of non-conducting fillers and the reliability of flip chip assembly on organic substrates using modified ACA composite materials. For the characterization of modified ACA s composites with different content of non-conducting fillers, differential scanning calorimeter (DSC), and thermo-gravimetric analyzer (TGA), dynamic mechanical analyzer (DMA), and thermo-mechnical analyzer (TMA) were utilized. As the non-conducting filler content increased, CTE values decreased and storage modulus at room temperature increased. In addition, the increase in the content of filler brought about the increase of Tg^{DSC}$ and $Tg^{TMA}$. However, the TGA behaviors stayed almost the same. Contact resistance changes were measured during reliability tests such as thermal cycling, high humidity and temperature, and high temperature at dry condition. It was observed that reliability results were significantly affected by CTEs of ACA materials especially at the thermal cycling test. Results showed that flip chip assembly using modified ACA composites with lower CTEs and higher modulus by loading non-conducting fillers exhibited better contact resistance behavior than conventional ACAs without non-conducting fillers.

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Repair bond strength of resin composite to three aged CAD/CAM blocks using different repair systems

  • Gul, Pinar;Altinok-Uygun, Latife
    • The Journal of Advanced Prosthodontics
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    • v.12 no.3
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    • pp.131-139
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    • 2020
  • PURPOSE. The purpose of this study is to evaluate the repair bond strength of a nanohybrid resin composite to three CAD/CAM blocks using different intraoral ceramic repair systems. MATERIALS AND METHODS. Three CAD/CAM blocks (Lava Ultimate, Cerasmart, and Vitablocks Mark II) were selected for the study. Thirty-two specimens were fabricated from each block. Specimens were randomly divided into eight groups for the following different intraoral repair systems: Group 1: control group (no treatment); Group 2: 34.5% phosphoric acid etching; Group 3: CoJet System; Group 4: Z-Prime Plus System; Group 5: GC Repair System; Group 6: Cimara System; Group 7: Porcelain Repair System; and Group 8: Clearfil Repair System. Then, nanohybrid resin composite (Tetric Evo Ceram) was packed onto treated blocks surfaces. The specimens were thermocycled before application of repair systems and after application of composite resin. After second thermal cycling, blocks were cut into bars (1 × 1 × 12 ㎣) for microtensile bond strength tests. Data were analyzed using two-way ANOVA and Tukey's HSD test (α=.05). RESULTS. Cimara System, Porcelain Repair, and Clearfil Repair systems significantly increased the bond strength of nanohybrid resin composite to all CAD/CAM blocks when compared with the other tested repair systems (P<.05). In terms of CAD/CAM blocks, the lowest values were observed in Vitablocks Mark II groups (P<.05). CONCLUSION. All repair systems used in the study exhibited clinically acceptable bond strength and can be recommended for clinical use.

Performance Analyses of the GPS Receiver for Satellite Launch Vehicles according to Temperature Variation (온도변화에 따른 위성발사체용 GPS 수신기의 성능분석)

  • Kwon, Byung-Moon;Moon, Ji-Hyeon;Choi, Hyung-Don;Cho, Gwang-Rae
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.33 no.12
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    • pp.101-108
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    • 2005
  • The GPS(Global Positioning System) receiver for satellite launch vehicles which will be mounted on a launch vehicle can be applied to the flight safety system with its accurately calculated position and velocity data during vehicle's flight. This paper analyzes the performance of the GPS receiver such as SNR(Signal to Noise Ratio), fix mode, position and velocity error, number of visible and tracking satellites, and PDOP(Position Dilution of Precision) under temperature variation which is changed from -34$^{\circ}C$ to +71$^{\circ}C$.

Repair bond strengths of non-aged and aged resin nanoceramics

  • Subasi, Meryem Gulce;Alp, Gulce
    • The Journal of Advanced Prosthodontics
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    • v.9 no.5
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    • pp.364-370
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    • 2017
  • PURPOSE. To explore the influence of different surface conditionings on surface changes and the influence of surface treatments and aging on the bond strengths of composites to non-aged and aged resin nanoceramics. MATERIALS AND METHODS. Rectangular-shaped non-aged and aged (5000 thermocycles) resin nanoceramic specimens (Lava Ultimate) (n=63, each) were divided into 3 groups according to surface treatments (untreated, air abrasion, or silica coating) (n=21). The surface roughness was measured and scanning electron microscopy was used to examine one specimen from each group. Afterwards, the specimens were repaired with a composite resin (Filtek Z550) and half were sent for aging (5000 thermocycles, n=10, each). Shear bond strengths and failure types were evaluated. Roughness and bond strength were investigated by two- and three-way analysis of variance, respectively. The correlation between the roughness and bond strength was investigated by Pearson's correlation test. RESULTS. Surface-treated samples had higher roughness compared with the untreated specimens (P=.000). For the non-aged resin nanoceramic groups, aging was a significant factor for bond strength; for the aged resin nanoceramic groups, surface treatment and aging were significant factors. The failures were mostly adhesive after thermal cycling, except in the non-aged untreated group and the aged air-abraded group, which had mostly mixed failures. Roughness and bond strength were positively correlated (P=.003). CONCLUSION. Surface treatment is not required for the repair of non-aged resin nanoceramic; for the repair of aged resin nanoceramic restorations, air abrasion is recommended.

Application and Verification Trend of Space Qualified Materials (우주용 자재의 적용 및 검증기술 동향)

  • Lee, Choon-Woo;Lee, Chang-Ho;Cho, Young-Jun;Hwang, Do-Soon
    • Current Industrial and Technological Trends in Aerospace
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    • v.6 no.2
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    • pp.60-68
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    • 2008
  • The characteristic and properties of materials are rapidly degraded when subjected to the synergistic effects of the space environment such as atomic oxygen, radiation, vacuum and thermal cycling. In order to understand the mechanism of material property variation in space environment and to develop new space materials applicable to the future space program, advanced space organizations such as NASA, ESA and JAXA have been continuing many researches on material test specimens used on ISSE(International Space Station Experiment) or LDEF(Long Duration Exposure Facility). In this paper, the selection requirements and verification trend of materials in space applications

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Fracture resistance and marginal fit of the zirconia crowns with varied occlusal thickness

  • Tekin, Yadel Hazir;Hayran, Yeliz
    • The Journal of Advanced Prosthodontics
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    • v.12 no.5
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    • pp.283-290
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    • 2020
  • PURPOSE. The present study aimed to evaluate the clinical applicability of monolithic zirconia (MZ) crowns of different thickness via determination of fracture resistance and marginal fit. MATERIALS AND METHODS. MZ crowns with 0.5, 0.8, 1.0, and 1.5 mm thickness and porcelain fused to metal (PFM) crowns were prepared, ten crowns in each group. Marginal gaps of the crowns were measured. All crowns were aged with thermal cycling (5 - 55℃/10000 cycle) and chewing simulator (50 N/1 Hz/lateral movement: 2 mm, mouth opening: 2 mm/240000 cycles). After aging, fracture resistance of crowns was determined. Statistical analysis was performed with one-way ANOVA and Tukey's HDS post hoc test. RESULTS. Fracture loads were higher in the PFM and 1 mm MZ crowns compared to 0.5 mm and 0.8 mm crowns. 1.5 mm MZ crowns were not broken even with the highest force applied (10 kN). All marginal gap values were below 86 ㎛ even in the PFM crowns, and PFM crowns had a higher marginal gap than the MZ crowns. CONCLUSION. The monolithic zirconia exhibited high fracture resistance and good marginal fit even with the 0.5 mm thickness, which might be used with reduced occlusal thickness and be beneficial in challengingly narrow interocclusal space.

Effects of Drying Temperature on the $LiCoO_2$ Thin Films Fabricated by Sol-gel Method

  • Kim, Mun-Kyu;Park, Kyu-Sung;Kim, Duk-Su;Son, Jong-Tae;Kim, Ho-Gi
    • Journal of the Korean Ceramic Society
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    • v.38 no.9
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    • pp.777-781
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    • 2001
  • $LiCoO_{2}$ thin films have received attention as cathodes of thin film microbatteries in these days. In this study, $LiCoO_{2}$ thin films are fabricated by a sol-gel spin coating method followed by a post-annealing process. The thermal decomposition behaviour of precursor is investigated by TG/DTA analysis. The change of crystallinity, microstructure and electrochemical properties of final films as the drying temperature changes are also studied by XRD, SEM and galvanostatic charge/discharge cycling test. The relationship between the discharge capacity and the drying temperature are intensively investigated in this work.

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A Study on the Improvement of Solder Joint Reliability for 153 FC-BGA (153 FC-BGA에서 솔더접합부의 신뢰성 향상에 관한 연구)

  • 장의구;김남훈;유정희;김경섭
    • Journal of the Microelectronics and Packaging Society
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    • v.9 no.3
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    • pp.31-36
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    • 2002
  • The 2nd level solder joint reliability of 153 FC-BGA for high-speed SRAM (Static Random Access Memory) with the large chip on laminate substrate comparing to PBGA(Plastic Ball Grid Array) was studied in this paper. This work has been done to understand an influence as the mounting with single side or double sides, structure of package, properties of underfill, properties and thickness of substrate and size of solder ball on the thermal cycling test. It was confirmed that thickness of BT(bismaleimide tiazine) substrate increased from 0.95 mm to 1.20 mm and solder joint fatigue life improved about 30% in the underfill with the low young's modulus. And resistance against the solder ball crack became twice with an increase of the solder ball size from 0.76 mm to 0.89 mm in solder joints.

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