• Bulletin of the Korean Chemical Society
• /
• v.30 no.2
• /
• pp.363-367
• /
• 2009

An isotope-dilution flow-injection electrospray/mass spectrometric method was developed for the accurate determination of glucosamine contents in pharmaceutical formulations. Samples were extracted by methanol. After spiking glucosamine-1-$^{13}C_1$ as an internal standard, the extracts were then analyzed by flow-injection ESI/MS in a selected ion monitoring (SIM) mode to detect [M+H]$^+$ ions of the analyte and its isotope analogue at m/z 180 and m/z 181, respectively. Confirmatory measurements were made by selectively monitoring the collisionally induced dissociation channels of m/z 180 $\rightarrow$ m/z 72 and m/z 181 $\rightarrow$73, respectively, to test the possibility of bias in the SIM method due to matrix interferences, but any significant bias in the SIM mode was not observed. Repeatability and reproducibility studies showed that the flow-injection ESI/MS method is a reliable and reproducible method which can provide a typical method precision of 1.0 %. Other results for the method validation are reported.

• Journal of the Korea Institute of Military Science and Technology
• /
• v.23 no.3
• /
• pp.229-236
• /
• 2020

A crush switch assembly(CSA) connected to an impact fuze provides electrical signal for detonation of the loaded main charge when an impact with the target is detected. Because the CSA experiences continuous changes in flight environment such as changes in velocity, vibration, and stresses, it is necessary to accurately predict the behavior of the fuze to maintain functionality during flight and to detonate when necessary. In this paper, random vibration analysis for flight environment and impact analysis on target hit are performed using FEA. Then, high speed impact tests are performed with the original and scaled down models to ensure operation validation of the manufactured products. The test results are then compared with M&S results to verify the capability of currently modeled CSA.

• Journal of the Korean Society for Aeronautical & Space Sciences
• /
• v.45 no.5
• /
• pp.401-408
• /
• 2017

This paper describes development and validation processes of a low-cost hardware based flight control computer designed for multi-rotor UAVs. The developed flight control computer controls multi-rotors stable and can handle complex flight missions using an integrated high-performance Linux computer. A complementary filter generates a navigation solution with 500 Hz, and a proposed observer significantly reduces measurement noise. A control algorithm utilizes a feed-forward term computed by a three-dimensional curve fitting method, and it increases tracking performance. The developed flight control system has been fully tested through several test flights, and it can apply to real flight environments.

• Journal of the Korea Academia-Industrial cooperation Society
• /
• v.10 no.3
• /
• pp.596-601
• /
• 2009

In this study, the rate-sensitive constitutive model, which was developed in the previous paper of this journal, was validated using the experimental results obtained from the well-calibrated triaxial compression test conducted with the Boston blue clay. The validation was performed for the various cases of the strain rate of 0.05%/hr, 0.5%/hr, 5.0%/hr and OCR of 1, 2, 4, 8. The developed model was validated for the normally and slightly overconsolidated cases; however, the cases of heavily overconsolidation needs further research.

• Korean Journal of Remote Sensing
• /
• v.22 no.5
• /
• pp.389-396
• /
• 2006

Surface Solar Insolation is important for vegetation productivity, hydrology, crop growth, etc. In this study, Surface Solar Insolation is estimated using Multi-functional Transport Satellite (MTSAT-1R) in clear and cloudy conditions. For the Cloudy sky cases, the surface solar insolation is estimated by taking into account the cloud transmittance and multiple scattering between cloud and surface. This model integrated Kawamura's model and SMAC code computes surface solar insolation with a $5\;km{\times}5\;km$ spatial resolution in hourly basis. The daily value is derived from the available hourly Surface Solar Insolation, independently for every pixel. To validation, this study uses ground truth data recorded from the pyranometer installed by the Korea Meteorological Agency (KMA). The validation of estimated value is performed through a match-up with ground truth. Various match-up with ground truth. Various match-up window sizes are tested with $3{\times}3,\;5{\times}5,\;7{\times}7,\;9{\times}9,\;10{\times}10,\;11{\times}11,\;13{\times}pixels to define the spatial representativity of pyranometer measurement, and to consider drifting clouds from adjacent pixels across the ground station during the averaging interval of 1 hour are taken into account.

• Smart Structures and Systems
• /
• v.18 no.3
• /
• pp.625-642
• /
• 2016

The rapid technology developments in smartphones have created a significant opportunity for their use in structural live load measurements. This paper presents extensive experiments conducted in two stages to investigate this opportunity. Shaking table tests were carried out in the first stage using selected popular smartphones to measure the sinusoidal waves of various frequencies, the sinusoidal sweeping, and earthquake waves. Comparison between smartphone measurements and real inputs showed that the smartphones used in this study gave reliable measurements for harmonic waves in both time and frequency domains. For complex waves, smartphone measurements should be used with caution. In the second stage, three-dimensional motion capture technology was employed to explore the capacity of smartphones for measuring the movement of individuals in walking, bouncing and jumping activities. In these tests, reflective markers were attached to the test subject. The markers' trajectories were recorded by the motion capture system and were taken as references. The smartphone measurements agreed well with the references when the phone was properly fixed. Encouraged by these experimental validation results, smartphones were attached to moving participants of this study. The phones measured the acceleration near the center-of-mass of his or her body. The human-induced loads were then reconstructed by the acceleration measurements in conjunction with a biomechanical model. Satisfactory agreement between the reconstructed forces and that measured by a force plate was observed in several instances, clearly demonstrating the capability of smartphones to accurately assist in obtaining human-induced load measurements.

• Wind and Structures
• /
• v.17 no.5
• /
• pp.495-513
• /
• 2013

Thin, high-strength steel roof cladding is widely used in residential and industrial low-rise buildings and is susceptible to failure during severe wind storms such as cyclones. Current cladding design is heavily reliant on experimental testing for the determination of roof cladding performance. Further study is necessary to evolve current design standards, and numerical modelling of roof cladding can provide an efficient and cost effective means of studying the response of cladding in great detail. This paper details the development of a numerical model that can simulate the static response of corrugated roof cladding. Finite element analysis (FEA) was utilised to determine the response of corrugated cladding subject to a static wind pressure, which included the anisotropic material properties and strain-hardening characteristics of the thin steel roof cladding. The model was then validated by comparing the numerical data with corresponding experimental test results. Based on this comparison, the model was found to successfully predict the fastener reaction, deflection and the characteristics in deformed shape of the cladding. The validated numerical model was then used to predict the response of the cladding subject to a design cyclone pressure trace, excluding fatigue effects, to demonstrate the potential of the model to investigate more complicated loading circumstances.

• Journal of the Korean Society of Propulsion Engineers
• /
• v.23 no.3
• /
• pp.96-103
• /
• 2019

In this study, a comparison was conducted to verify the propellant isolation assembly of the Korea Pathfinder Lunar Orbiter (KPLO). An engineering validation model (EVM) is being developed to simulate the flow of the flight model. Three factors were selected for comparison: the total pressure drop during propellant isolation assembly, the waterhammer by driving thruster valve, and the orifice set up for flow control and damping the waterhammer. The analysis results are compared with EVM test results. In the future, backup data to confirm the design will be established.

• International Journal of Internet, Broadcasting and Communication
• /
• v.13 no.4
• /
• pp.154-168
• /
• 2021

The purpose of this study is to develop and validate the disaster safety awareness scale for high school students. For this purpose, the previously developed disaster safety awareness scale and related prior research was analyzed. Questionnaire data was collected from March 22 to May 25, 2021 from 1054 students (male: 569, female: 485) in the first, second, and third grades of 5 high schools in 3 cities. Through the process of revising, supplementing, and reviewing the items extracted through preliminary research and preliminary test together with experts and students, a final disaster safety awareness scale consisting of 24 items was developed. This scale consists of four sub-factors: 'disaster prevention', 'disaster response A', 'disaster response B', and 'disaster recovery'. Good reliability and validity were secured through exploratory and confirmatory analyses. The significance of this study is that it laid a basic and objective foundation for high school students' disaster safety awareness research by developing a validated scale in a situation where the development of disaster safety awareness scales for high school students was still insufficient. It can be used as useful data for fire safety education as well as a psychological measurement tool for fostering fire safety awareness.

• Journal of the Korean Society of Systems Engineering
• /
• v.16 no.2
• /
• pp.1-15
• /
• 2020

Nuclear power plants in South Korea are operated to cover the baseload demand. Hence they are operated at 100% rated power and do not deploy power tracking control except for startup, shutdown, or during transients. However, as the contribution of renewable energy in the energy mix increases, load follow operation may be needed to cover the imbalance between consumption and production due to the intermittent nature of electricity produced from the conversion of wind or solar energy. Load follow operation may be quite challenging since the operators need to control the axial power distribution and core reactivity while simultaneously conducting the power maneuvering. In this paper, a systems engineering approach for multi-physics load follow simulation of APR1400 is performed. RELAP5/SCDAPSIM/MOD3.4/3DKIN multi-physics package is selected to simulate the Korean Advanced Power Reactor, APR1400, under load follow operation to reflect the impact of feedback signals on the system safety parameters. Furthermore, the systems engineering approach is adopted to identify the requirements, functions, and physical architecture to provide a set of verification and validation activities that guide this project development by linking each requirement to a validation or verification test with predefined success criteria.