• 제목/요약/키워드: Temperature Stabilizing

검색결과 123건 처리시간 0.023초

션트 저항체의 제작을 위한 Yarned CNT Fiber 저항에 대한 열처리의 영향 (Effect of Thermal Annealing on Resistance of Yarned Carbon Nanotube Fiber for the Use of Shunt Resistor)

  • 윤종현;이선우
    • 한국전기전자재료학회논문지
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    • 제32권5호
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    • pp.403-406
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    • 2019
  • We prepared yarned carbon nanotube (CNT) fibers from a CNT forest synthesized on a Si wafer by chemical vapor deposition (CVD). The yarned CNT fibers were thermally annealed to reduce their resistance by removing the amorphous carbonaceous impurities present in the fibers. The resistance of the yarned CNT fiber gradually decreased with an increase in the annealing temperature from $200^{\circ}C$ to $400^{\circ}C$ but increased again above $450^{\circ}C$. We carried out thermogravimetric analysis (TGA) to confirm the burning properties of the amorphous carbonaceous impurities and the crystalline CNTs present in the fibers. The pattern of the mass change of the sample CNT fibers was very similar to that of the resistance change. We conclude that CNT fibers should be thermally annealed at temperatures below $400^{\circ}C$ for reducing and stabilizing their resistance.

Experimental study on Microbially Induced Calcite Precipitation for expansive soil stabilization

  • Zheng Lu;Yu Qiu;Jie Liu;Chengcheng Yu; Hailin Yao
    • Geomechanics and Engineering
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    • 제32권1호
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    • pp.85-96
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    • 2023
  • Microbially induced carbonate precipitation (MICP) is extensively discussed as a promising topic for ground stabilization. The practical effect of stabilizing the expansive soil is presented in this paper with a logical process from the bacterial activity to the treatment technology. Temperature, pH, shaking frequency, and inoculation amount are discussed to evaluate the bacterial activity. The physic-mechanic properties are also evaluated to discuss the effect of the MICP process on expansive soil. Results indicate that the MICP method achieves the mitigation of expansion. The treated soil has a low proportion of fine particles (< 5 ㎛), the plasticity index significantly decreases, and strength values improve much. MICP process has a significant cementation effect on the soil matrix. Moreover, the infiltration model test presents the coating effect on the topsoil. According to the relation between the CaCO3 content and the treatment effect, the topsoil has better treatment than the deeper soil.

A Study on the widthwise thickness uniformity of HTS wire using thickness gradient deposition technology

  • Gwantae Kim;Insung Park;Jeongtae Kim;Hosup Kim;Jaehun Lee;Hongsoo Ha
    • 한국초전도ㆍ저온공학회논문지
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    • 제25권4호
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    • pp.24-27
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    • 2023
  • Until now, many research activities have been conducted to commercialize high-temperature superconducting (HTS) wires for electric applications. Most of all researchers have focused on enhancing the piece length, critical current density, mechanical strength, and throughput of HTS wires. Recently, HTS magnet for generating high magnetic field shows degraded performance due to the deformation of HTS wire by high electro-magnetic force. The deformation can be derived from widthwise thickness non-uniformity of HTS wire mainly caused by wet processes such as electro-polishing of metal substrate and electro-plating of copper. Gradient sputtering process is designed to improve the thickness uniformity of HTS wire along the width direction. Copper stabilizing layer is deposited on HTS wire covered with specially designed mask. In order to evaluate the thickness uniformity of HTS wire after gradient sputtering process, the thickness distribution across the width is measured by using the optical microscope. The results show that the gradient deposition process is an effective method for improving the thickness uniformity of HTS wire.

Technical Optimization of Culture Conditions for the Production of Exopolysaccharide (EPS) by Lactobacillus rhamnosus ATCC 9595

  • Kim, Young-Hoon;Kim, Ji-Uk;Oh, Se-Jong;Kim, Young-Jun;Kim, Myung-Hee;Kim, Sae-Hun
    • Food Science and Biotechnology
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    • 제17권3호
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    • pp.587-593
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    • 2008
  • Microbial exopolysaccharide (EPS) is a biothickener that can be added to a wide variety of food products, where it serves as a viscosifying, stabilizing, emulsifying, and gelling agent. The objective of this study was to investigate the optimum conditions of pH, incubation temperature, and whey protein concentration (WPC) for EPS production by Lactobacillus rhamnosus ATCC 9595. We found that maximal EPS production was achieved at a pH of 5.5 and temperature of $37^{\circ}C$. At the same fermentation conditions, EPS production was affected by the addition of L. rhamnosus GG (a weak-EPS producer). After growth for 24 hr, total EPS production was $583{\pm}15.4mg/L$ in the single culture system, and $865{\pm}22.6\;mg/L$ in the co-culture system with L. rhamnosus GG. Based on the presence of WPC, EPS production dramatically increased from $583{\pm}15.4$ (under no WPC supplementation) to $1,011{\pm}14.7\;mg/L$ (under supplementation with 1.0% WPC). These results suggest that WPC supplementation and the co-culture systems coupled with small portions of weak-EPS producing strain can play an important role in the enhancement of EPS production.

Investigation on Optical Properties of Natural Brown Diamonds with Various Types by High Pressure and High Temperature Treatment

  • Bai, Jong-Hyuck;Seo, Jin-Gyo;Shon, Shoo-Hack;Ahn, Yong-Kil;Park, Jong-Wan
    • 한국재료학회지
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    • 제20권5호
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    • pp.278-288
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    • 2010
  • High Pressure High Temperature (HPHT) treatment can significantly change the color of diamonds. We studied the variation of the optical properties according to the nitrogen arrangement in natural brown diamonds of various types (type IaAB, type IaB, type IaA > B, type IaA < B, IaA = B) after HPHT treatment. The diamonds with different arrangements of nitrogen were annealed at temperatures in the range $1700-1800^{\circ}C$ under a stabilizing pressure of 5 GPa. HPHT treated samples were analyzed using UV-Vis-NIR, FT-IR, and PL spectroscopy. The absorption and luminescence spectra were measured to compare the variations of nitrogen arrangement in the natural brown diamonds before and after HPHT treatment. After HPHT treatment, the brown coloration in all types of diamonds was reduced and a decrease in the peaks related to the A-aggregate of nitrogen was more predominant than the B-aggregate. Furthermore, the peaks related to N3 (415.4 nm), H4 (496.4 nm), and platelet decreased and the peaks related to H3 (503.2 nm) and G-band increased after HPHT treatment. In conclusion, spectroscopic analysis of natural brown diamonds after HPHT treatment showed that a yellow color was produced by absorption in the H3 centers and a green color was generated by interaction between absorptions of the H3 and H2 centers.

sII $SF_6+H_2$ 하이드레이트의 분자 거동 (Molecular Behavior of $SF_6+H_2$ Structure II Hydrates)

  • 박다혜;이보람;사정훈;;이건홍
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2011년도 추계학술대회 초록집
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    • pp.122.2-122.2
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    • 2011
  • Sulfur hexafluoride ($SF_6$), one of the most potent greenhouse gases, is known as a hydrate former and has been studied at the high pressure up to 1.3 GPa with gas mixtures and with aqueous surfactant. Since we regard $SF_6$ as a potential promoter molecule that can stabilize hydrate structure more effectively compare to the other promoters, further investigation is required to verify the stabilizing ability of $SF_6$ in the hydrate structure. However, the insoluble nature of $SF_6$ in water or gases hinders fine scale analyses. This work discusses the data obtained by using molecular dynamics simulations of structure II (sII) clathrate hydrates containing $SF_6$ and $H_2$. The simulations were performed using the TIP4P/Ice model for water molecule and a previously reported $SF_6$ molecular model (optimized at the pure $SF_6$ single phase system (Olivet and Vega, 2007)), and a $H_2$ molecular model (adapted from the THF+$H_2$ hydrate system (Alavi et al., 2006)). The simulations are performed to observe the stability of $SF_6$ and $H_2$ in the sII clathrate hydrate system with varying temperature and pressure conditions and occupancies of $SF_6$ and $H_2$, which cannot be easily tuned experimentally. We observe that stability of H2 enclathrated in the hydrate structure more affected by the occupancy of $SF_6$ molecules and temperature than pressure, which ranges from 1 to 100 bar.

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2단 다공성 매체버너에서 열교환기를 모사한 수관 유무에 따른 연소 특성 비교 (Comparison of Combustion Characteristics With and Without Water Tube Simulating Heat Exchanger in Two Sections Porous Media Burner)

  • 이희도;김재현;이기만
    • 한국가스학회지
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    • 제23권5호
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    • pp.24-34
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    • 2019
  • 본 연구에서는 수관식 보일러의 열교환기를 모사하기 위하여 수관의 존재 유무에 따른 화염의 안정화와 연소 특성을 당량비와 유속에 따라 비교하였다. 버너는 화염이 존재하는 SiC foam과 역화 방지를 위한 세라믹 보드, 균일한 유동장을 형성하는 알루미나 볼로 구성되며, 반경 반향의 열 손실을 최소화하기 위하여 단열재로 밀폐되어 있다. 결과적으로 수관이 존재하는 경우 낮은 당량비 구간에서 역화 및 날림 현상의 경계가 넓어지는 것을 안정화 영역에서 확인할 수 있었다. 또한, 수관이 존재하는 경우 NOx 배출량이 수관이 없는 경우보다 증가하는 것을 확인하였다. 이는 수관이 존재함으로써 열 손실을 억제하여 화염의 온도가 증가하는 것으로 판단하였으며, O2 배출량과 화염의 온도를 예측하여 입증하였다.

다결정 산화갈륨/다이아몬드 이종 박막 성장 및 열처리 효과 연구 (Growth and thermal annealing of polycrystalline Ga2O3/diamond thin films on Si substrates)

  • 서지연;김태규;신윤지;정성민;배시영
    • 한국결정성장학회지
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    • 제31권6호
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    • pp.233-239
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    • 2021
  • 본 연구에서는 산화갈륨의 방열 특성 향상을 위해 산화갈륨/다이아몬드 이종 박막 성장을 진행하였다. 먼저, 핫필라멘트 화학기상증착법을 이용하여 다결정 다이아몬드를 증착시킨 후, 미스트 화학기상증착법을 통해 450~600℃ 사이의 온도구간에서 산화갈륨 박막을 성장시켰다. 열처리 전후 비교를 통해 500℃에서 산화갈륨/다이아몬드 계면 분리 현상이 발생함을 확인하였다. 이는 비정질과 결정질이 혼재된 산화갈륨 박막이 성장된 후, 냉각 과정에서 열팽창계수의 차이로 인해 계면이 분리된 것으로 판단하였다. 따라서, 본 연구를 통한 산화갈륨/다이아몬드 계면의 물리적 안정성을 통해 산화갈륨의 열물성 보완및 고전력 반도체로의 활용이 기대된다.

전력변환장치 캐비넷에서의 내부발열 개선을 위한 열유동 분석 및 유통안전성 향상을 위한 진동특성 분석 (Theoretical Heat Flow Analysis and Vibration Characteristics During Transportation of PCS(Power Conversion System) for Reliability)

  • 주민정;서상욱;오재영;정현모;박종민
    • 한국포장학회지
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    • 제28권2호
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    • pp.143-149
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    • 2022
  • PCS needs to freely switch AC and DC to connect the battery, external AC loads and renewable energy in both directions for energy efficiency. Whenever converting happens, power loss inevitably occurs. Minimization of the power loss to save electricity and convert it for usage is a very critical function in PCS. PCS plays an important role in the ESS(Energy Storage System) but the importance of stabilizing semiconductors on PCB(Printed Circuit Board) should be empathized with a risk of failure such as a fire explosion. In this study, the temperature variation inside PCS was reviewed by cooling fan on top of PCS, and the vibration characteristics of PCS were analyzed during truck transportation for reliability of the product. In most cases, a cooling fan is mounted to control the inner temperature at the upper part of the PCS and components generating the heat placed on the internal aluminum cooling plate to apply the primary cooling and the secondary cooling system with inlet fans for the external air. Results of CFD showed slightly lack of circulating capacity but simulated temperatures were durable for components. The resonance points of PCS were various due to the complexity of components. Although they were less than 40 Hz which mostly occurs breakage, it was analyzed that the vibration displacement in the resonance frequency band was very insufficient. As a result of random-vibration simulation, the lower part was analyzed as the stress-concentrated point but no breakage was shown. The steel sheet could be stable for now, but for long-term domestic transportation, structural coupling may occur due to accumulation of fatigue strength. After the test completed, output voltage of the product had lost so that extra packaging such as bubble wrap should be considered.

방사면역치료용 $^{188}Re$ 표지 항체의 안정성과 안정제의 효과 (Stability of $^{188}Re$ Labeled Antibody for Radioimmunotherapy and the Effect of Stabilizing Agents)

  • 장영수;김보광;정재민;정준기;이승진;이동수;이명철
    • 대한핵의학회지
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    • 제36권3호
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    • pp.195-202
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    • 2002
  • 목적: 베타입자 방출 핵종을 표지한 항체를 임상적으로 이용하기 위해서는 높은 비방사능을 가지는 것이 중요하다. $^{188}W/^{188}Re$ 발생기를 사용하여 쉽게 얻을 수 있는 무담체 $^{188}Re$은 이런 목적에 이상적인 방사성 핵종이다. 하지만 높은 비방사능의 $^{188}Re$이 표지된 항체는 높은 베타 에너지(2.1 MeV)로 인한 불안정성이 문제가 된다. 우리는 $^{188}Re$이 표지된 항체의 안정성을 확보하기 위해 몇 가지 안정제가 미치는 영향에 대해서 조사하였다. 대상 및 방법: 환원시킨 단일클론항체(CEA79.4)에 stannous tartrate와 발생기에서 용출한 $^{188}Re-perrhenate$를 넣어 실온에서 2시간 반응시켰다. 각각의 방사화학적순도는 크로마토그라피를 써서 확인하였다. 표지된 항체에 사람 혈청 알부민(HSA)을 첨가(최종농도 2%)하고 ascorbic acid, ethanol, Tween 80 존재 하에서의 안정성을 각각 조사하였다. 결과: 표지된 항체의 비방사능은 $1.25{\sim}4.77MBq/{\mu}g$, 표지 효율은 $88{\pm}4%\;(n=12)$였다. 안정제로 ascorbic acid, ethanol, Tween 80을 첨가하였을 때 $N_2$ 존재 하에서 모든 경우에 10시간까지 안정하였으나, 공기와 접촉 시 10시간 후에 방사화학적순도는 각각 처음의 100, 45, 36%가 되었다. 과산화레늄(perrhenate)과 $^{188}Re-tartrate$의 증가가 주된 요인이었으며 콜로이드 형성은 모든 경우에 큰 영향을 끼치지 않았다. Ascorbic acid 첨가는 공기 중에서 perrhenate의 형성을 줄임으로서 항체의 안정성에 가장 많이 기여하였다. 결론: 높은 비방사능의 $^{188}Re$이 표지된 항체는 공기 중에 노출되었을 때 불안정하였으며, ascorbic acid 첨가시 안정성을 향상시킬 수 있었다.