• 제목/요약/키워드: Teflon

검색결과 527건 처리시간 0.026초

TiH2/camphene 슬러리의 동결건조 및 열처리에 의한 Ti 계 다공체의 제조 (Fabrication of Porous Ti by Freeze-Drying and Heat Treatment of TiH2/Camphene Slurries)

  • 서한길;김영도;석명진;오승탁
    • 한국재료학회지
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    • 제23권6호
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    • pp.339-343
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    • 2013
  • Porous Ti-systems with unidirectionally aligned channels were synthesized by freeze-drying and a heat treatment process. $TiH_2$ powder and camphene were used as the source materials of Ti and sublimable vehicles, respectively. Camphene slurries with $TiH_2$ content of 10 and 15 vol% were prepared by milling at $50^{\circ}C$ with a small amount of oligomeric polyester dispersant. Freezing of the slurry was done in a Teflon cylinder attached to a copper bottom plate cooled at $-25^{\circ}C$ while unidirectionally controlling the growth direction of the camphene. Pores were generated subsequently by sublimation of the camphene during drying in air for 48 h. The green body was heat-treated at $1100^{\circ}C$ for 1 h in a nitrogen and air atmosphere. XRD analysis revealed that the samples composed of TiN and $TiO_2$ phase were dependent on the heat-treatment atmosphere. The sintered samples showed large pores of about 120 mm which were aligned parallel to the camphene growth direction. The internal wall of the large pores had relatively small pores with a dendritic structure due to the growth of camphene dendrite depending on the degree of nucleation and powder rearrangement in the slurry. These results suggest that a porous body with an appropriate microstructure can be successfully fabricated by freeze-drying and a controlled sintering process of a camphene/$TiH_2$ slurry.

광중합(光重合) 레진의 경도측정(硬度測定)에 관(關)한 연구(硏究) (A STUDY ON THE HARDNESS IN VISIBLE LIGHT COMPOSITE RESIN)

  • 이명종
    • Restorative Dentistry and Endodontics
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    • 제14권1호
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    • pp.179-188
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    • 1989
  • The purpose of this study was to measure Micro vicker's hardness of 4 kinds of anterior Composite resins (Pyrofil light bond anterior, Lite-fil anterior, Photo clear fil anterior, Silux) and 6 kinds of posterior Composite resin (Pyrofil light bond posterior. Lite-fil posterior, Photo clear fil posterior, Occlusin posterior, Palfique light posterior, P-30, posterior) according to deference of depth and distance of light tip from surface of composite resin. Each composite resin was filled into Teflon tube of 5mm in diameter and 5mm in depth, celluloid matrix was covered and the light in accordance with each composite resin was irradiated in distance of zero millimeter and 1 cm from light tip to surface of composite resin for 30 seconds. Specimens were sectioned longitudinally with cutting device. Microvicker's hardness measurements ware made at the depth of surface, 1mm, 2mm, 3mm, 4mm and 5mm from the surface to deep portion. Vicker's hardness numbers were taken on each depth under 200gm load for 30 seconds with MVK-E. The following results were: 1. The highest hardness value was measured at 1 mm depth. Then the deeper the depth, the lesser the hardness was observed. 2. The hardness value of anterior composite resins is lower than one of posterior composite resins. 3. Hardness number of composite resin irradiated in distance of zero millimeter from surface of composite resin was higher than one of 1 cm from surface of composite resin. 4. The pattern of hardness change at varying depth was similar to all the experimental material with no relation to distance of light from specimen.

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흰쥐 족저에 Formalin 주입으로 유발된 통증반응에 대한 전침 효과 (Effects of Electroacupuncture on the Modulation of Formalin-induced Pain in the Rat)

  • 김재효;최동옥;김민선;박병림;손인철
    • 대한한의학회지
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    • 제23권2호
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    • pp.97-107
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    • 2002
  • Objective : Acupuncture is a method used to treat many kinds of pain in oriental cultural medicine. Especially when hetero-segmental area acu-points are stimulated, the therapeutic effects of pain control have more critical properties than other methods of acupuncture. However, the mechanism of pain control by acupuncture is contradictory so far. The present study examined the effects of electroacupuncture (EA) applied to the acu-point of the hetero-segmental area on modulation of formalin-induced pain in Sprague-Dawley rats. Methods : In order to apply EA to acu-points in the plantar area of right forepaws, a pair of Teflon-coated stainless steel wires were implanted in HT 7 (Shin-Moon) and PC 7 (Dae-Reung) 7 days before the behavioral test. A behavioral test was performed by means of video camera after injection of 5% formalin ($50{\;}\mu\textrm{l}$) into the lateral plantar region of the left hind paw. EA was delivered by a constant DC current stimulator at 4~5 mA, 2 ms, and 10 Hz for 30 min. c-Fos protein expression was measured in the lumbar spinal cord at 2 hr and 4 hr after formalin injection. Results : Behavioral responses including favoring, flinching and biting occurred in the biphasic pattern, such as the 1st phase (0~5 min) and the 2nd phase (20~45 min) after formalin injection. However, EA (4~5 mA, 2 ms, 10 Hz) significantly inhibited the behavioral responses. Injection of formalin expressed c-Fos protein on the ipsilateral dorsal horn neurons in L3 - L5 and the expression was sustained more than 4 hrs after formalin injection. However, EA decreased c-Fos protein expression at dorsal horn neurons in the lumbar spinal cord till 4hrs after formalin injection. Conclusions : These results suggest that EA modulates formalin-induced pain and this inhibitory action may be elicited by the descending inhibitory system.

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연마방법에 따른 복합레진의 활택도에 관한 연군 -Atomic Force Microscope를 이용한 연구 (A STUDY ON SURFACE ROUGHNESS OF COMPOSITE RESINS AFTER FINISHING AND POLISHING -an Atomic Force Microscope study)

  • 김형섭;우이형
    • 대한치과보철학회지
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    • 제35권4호
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    • pp.719-741
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    • 1997
  • This study was undertaken to compare by Atomic Force Microscope the effects of various finishing and polishing instruments on surface roughness of filling and veneering composite resins. Seven composite resins were studied : Silux Plus (3M Dental Products, U.S.A.), Charisma (Heraeus Kulzer, Germany), Prisma THP (L.D.Caulk, Dentsply, U.S.A.), Photoclearfil (Kuraray, Japan), Cesead (Kuraray, Japan), Thermoresin LC (GC, Japan), Artglass (Heraeus Kulzer, Germany). Samples were placed and polymerized in holes (2mm thick and 8.5mm in diameter) machined in Teflon mold under glass plate, ensuring excess of material and moulded to shape with polyester matrix strip. Except control group (Polyester matrix strip), all experimental groups were finished and polishied under manufacturer's instructions. The finishing and polishing procedure were : carbide bur (E.T carbide set 4159, Komet, Germany), diamond bur (composite resin polishing bur set, GC, Japan), aluminum-oxide disc (Sof-Lex Pop-On, 3M Dental Products, U.S.A.), diamond-particle disc (Dia-Finish, Renfert Germany), white stone bur & rubber point( composite finishing kit, EDENTA, Swiss), respectively. Each specimens were evaluated for the surface roughness with Atomic Force Microscope (AutoProbe CP, Park Scientific Instruments, U.S.A.) under contact mode and constant height mode. The results as follows : 1. Except Thermoresin LC, all experimental composite resin groups showed more rougher than control group after finishing and polishing(p<0.1). 2. A surface as smooth as control group was obtained by $Al_{2}O_{3}$ disc all filling composite resin groups except Charisma and all veneering composite resin groups except Thermoresin LC(p<0.05). 3. In case of Thermoresin LC, there were no statistically significant differences before and after finishing and polishing(p>0.1). 4. Carbide bur, diamond bur showed rough surfaces in all composite resin groups, so these were inappropriate for the final polishing instruments.

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축산관련차량 이동에 따른 도로의 에어로졸 발생량 분석 (Aerosol Emission from Road by Livestock Transport Vehicle Movement)

  • 서일환;이인복;황현섭;배연정;배승종;문운경
    • 농촌계획
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    • 제19권4호
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    • pp.137-147
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    • 2013
  • Most of livestock houses are concentrated in certain area with mass rearing system resulting in rapid spread of infectious diseases such as HPAI (highly pathogenic avian influenza). The livestock-related vehicles which frequently travel between farms could be a major factor for disease spread by means of transmission of airborne aerosol including pathogens. This study was focused on the quantitative measurement of aerosol concentration by field experiment while vehicles were passing through the road. The TSP (total suspended particle) and PM10 (particle matter) were measured using air sampler with teflon filter installed downward the road with consideration of weather forecast and the direction of road. And aerosol spectrometer and video recorders were also used to measure the real-time distribution of aerosol concentration by its size. The results showed that PM2.5 was not considerable for transmission of airborne aerosol from the livestock-related vehicle. The mass generated from the road during the vehicle movement was measured and calculated to 241.4 ${\mu}g/m^3$ by means of the difference between TSP and PM2.5. The dispersion distance was predicted by 79.6 m from the trend curve.

대혈관전위증 (S.D.D.) 치험 1례 (Complete Transposition of Great Arteries Combined with VSD and Pulmonic Stenosis (S.D.D.) -One Case Report-)

  • 강면식
    • Journal of Chest Surgery
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    • 제12권3호
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    • pp.207-214
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    • 1979
  • This 3-year-old girl was observed frequent exertional dyspnea and cyanosis at crying since birth. She was not premature baby and delivered at full term normally. On physical examination, she was underdeveloped-body weight 13.5 kg, height 99 cm.- and cyanotic. There was severe clubbing on fingers. There was grade II/VI ejection systolic murmur on left lateral border of the sternum. The preoperative examinations [EKG, echocardiogram, cardiac catheterization and biventriculogram] showed that complicated T.G.A. combined vena cava[S.D.D.]. Preoperatively, we decided the corrective surgery of Rastelli operation using a. pulmonary valved conduit. The operation was performed under total circulatory arrest using deep profound hypothermia combining with extracorporeal circulation. On operation, the anatomy of the heart showed that, 1. The subaortic conus was seen and subaortic muscles were hypertrophied. 2. The VSD[type II], behind the subaortic conus-about 1 cm. in diameter, was visible only through LV cavity and, 3. The pulmonary valve ring was hypoplastic and pulmonary valvular stenosis was seen also. The subpulmonic area [LV outflow tract] was obstructed with hypertrophied muscle and mitral valve. 4. Left superior vena cava was drained to RA via coronary sinus. 5. LAD coronary artery was originated from right coronary artery and ran anterior to the pulmonary artery. According to above anatomy, we performed the VSD closure with Teflon patch, and Mustard operation combined with LV-to-pulmonary artery bypass graft using the valve contained [Hancock 16 mm] conduit. Postoperatively, adequate blood pressure could be maintained under the state of using inotropic agent [epinephrine]. On the second postoperative day, the patient died of cardiac arrest due to low cardiac output syndrome, acute renal failure and pulmonary edema.

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우측 폐 하엽 절제술 후 발생한 기관지 이물질 (Bronchial Foreignbody after Right Lower Lobe Lobectomy)

  • 이형채;한일용;전희재;이양행;황윤호;조광현
    • Journal of Chest Surgery
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    • 제41권2호
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    • pp.281-284
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    • 2008
  • 기관지 내 이물은 대부분 흡입에 의해서 발생한다. 하지만 본 증례에서는 폐엽 절제술을 시행받은 5년 후, 기관지 내로 수술 시 사용한 비금속성 이물질이 배출된 드문 경우이다. 이 기관지 이물은 기관지 내시경으로 제거되었으며 수술 중 지혈 목적으로 사용된 테플론으로 밝혀졌다. 아직 수술 후 이러한 이물들이 기관지로 이주하여 배출되는 정확한 원인은 알 수 없으나 이번 증례는 일본에서 발표된 증례와 함께 비금속성의 물질들도 폐 실질에서 기관지로의 이주가 가능하다는 증거가 된다는 점에서 의미가 있겠다.

육계사 내 작업자의 미세먼지 노출량 현장모니터링 (Concentrations of Particulate Matter Exposed to Farm Workers in the Broiler Houses)

  • 서효재;오병욱;김효철;신소정;서일환
    • 한국농공학회논문집
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    • 제62권5호
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    • pp.27-37
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    • 2020
  • As domestic meat consumption increases, the broiler production industry has been larger and denser. The concentration of particulate matter (PM) and harmful gases generated is also increasing inside livestock house. However, the current research status of PM exposed to farm workers and the health effects are in the early stage. To understand PM concentration affecting workers in the broiler house, field monitoring was conducted according to its size distributions. Concentrations of PM10, PM2.5, and TD (Total Dust) were monitored using personal air samplers with teflon filter during working and moving periods considering the ventilation systems of 6 broiler houses. The purpose of this study is to monitor the PM concentration in the experimental broiler houses operated by forced ventilation system generally used in Korea and to evaluate the regional concentrations through airflow pattern. The PM concentrations were increased from inlet to outlet vents resulting in 1,872 of TD, 1,385 of PM10, and 209 ㎍/㎥ of PM2.5, respectively. The TD and PM10 concentrations were increased when the workers and broilers were moving. Among them, the particle size that occupied the largest amount of PM was 13.75 ㎛. These results suggest that personal protection equipments are important to reduce the health effect from PM inhalation.

ICP-OES를 이용한 우유의 Selenium 분석 (Determination of Selenium in Milk by ICP-OES)

  • 김효중;박종길;신정걸;백영진
    • 한국축산식품학회지
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    • 제23권4호
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    • pp.356-360
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    • 2003
  • 우유의 셀렌 함량을 측정하기 위하여 ICP-OES를 이용한 분석법을 확립하였다. 시료전처리는 우유의 수분을 제거한 후 질산과 과산화수소를 이용하여 유기성분을 제거하였고, 최종적으로 다시 과산화수소로 미량의 유기성분을 산화시켰다. 셀렌은 휘발성 무기성분이므로 전처리된 용액에 NaBH$_4$와 HCl을 이용하여 셀렌의 수소화(hydride)반응으로 끓는점을 높이고 분석감도를 향상시켰다. 수소화 반응 중 HCl 농도의 최적조건은 2 mol/L에서 최대 cps(counter per sec)로 나타났고, NaBH$_4$와 시료 유속의 최적조건은 각각 1.5%와 1.2mL/min인 것으로 나타났다. 따라서 위의 HG 조건이 시료 메트릭스에 따른 간섭효과를 제거하였으며, 최적의 정량조건임을 알 수 있었다. 이 조건으로 표준물질을 이용한 셀렌의 직선성 상관계수(R)는 0.98로서 우유에 함유된 셀렌 분석에 적용할 수 있었다. Standard addition method를 이용한 회수율은 10 ppb에서 88.0% 이었고, 첨가된 농도가 증가할수록 회수율 및 RSD는 정확성 및 정밀성을 확보할 수 있었다.

고도정수처리용 콘크리트 금속용사 피막의 내오존성 및 오존처리 후 부착강도 평가에 관한 실험적 연구 (Experimental Study on Evaluation of Bond Strength after Ozone Treatment and Ozone Resistance of Concrete Metal Spray Coating for Advanced Water Treatment)

  • 박진호;장현오;이한승
    • 한국구조물진단유지관리공학회 논문집
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    • 제22권4호
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    • pp.68-75
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    • 2018
  • 기존의 정수처리 방법으로는 제거되지 않는 물질이 발생함에 고도정수 처리 시설의 도입이 증가하고 있다. 그러나 오존을 이용한 고도정수처리 시설의 내부 방수 방식재는 오존의 산화력에 의해 열화되며 콘크리트까지 영향을 미쳐 내구성 저하의 원인이 된다. 본 연구에서는 내오존성 및 내화학성이 뛰어난 금속 패널을 기존의 시공법 보다 손쉬운 방법으로 시공하기 위한 방법으로 금속용사 공법을 이용하여 수처리 시설 콘크리트 구조물의 열화를 원천적으로 방지하기 위한 마감공법 개발 연구의 일원으로 용사금속 종류 및 피막의 표면처리 방법에 따른 내오존성 평가를 실시하였으며, 오존처리 후의 부착강도를 평가하였다. 실험결과 용사금속 Ti이 용사 후에도 내오존성이 뛰어난 것으로 나타났으며 표면처리 방법으로는 테프론계 봉공처리제를 사용하여 마감하는 것이 내오존성 및 부착성능 확보에 가장 적합한 방법이라 판단된다.