• Title/Summary/Keyword: Technical mixture

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A Study of Analytical Sensitivity on TDM Test Kit in Clinical Chemistry (약물검사 키트의 분석 민감도에 대한 연구)

  • Chang, Sang Wu;Kim, Nam Yong;Lee, Hee Gyung;Kim, Hyun Jung;Lee, Yun Jung;Jin, Ok Bae;Kim, Mi Gyung
    • Korean Journal of Clinical Laboratory Science
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    • v.36 no.2
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    • pp.127-130
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    • 2004
  • Analytical sensitivity on TDM test is the lowest concentration that can be distinguished from background noise. The aim of study was to evaluate analytical sensitivity that is also referred to as the lower limit of detection(LLD) about difference between zero calibrator and isotonic saline sample. We tested for 10 days with zero calibrators and 0.85% saline samples while running trilevel control samples under control. Raw data divided by two groups calculated mean and standard deviation from two sample populations and analytical sensitivity by ${\bar{X}}+2SD$. In comparison with isotonic saline samples and zero calibrators, there were significant differences in phenytoin, phenobarbital and vancomycin, etc. Especially analytical sensitivity on phenytoin is at the same level as the upper limit of analytical measurement range with $40{\mu}g/mL$. We think the cause of this is matrix interference. In conclusion, we were sure that standard protocol for analytical sensitivity as lower limit of analytical measurement range on TDM test must be measured with zero standard rather than an isotonic saline sample and type 1 reagent DW for reducing matrix effects within interactions between different materials in a mixture.

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Quality Characteristics of Pan Bread with Added Salt and Fat Content after Microwave Irradiation (Microwave 조사 시 소금 및 유지의 첨가량이 식빵의 품질 특성에 미치는 영향)

  • Park, Sang-Jun;An, Hye-Lyung;Lee, Kwang-Suck
    • Journal of the East Asian Society of Dietary Life
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    • v.20 no.5
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    • pp.687-696
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    • 2010
  • This study focused on microwave irradiation of dough, raising its temperature to monitor potential variations of dough properties and bread quality, and examined the optimum mixture ratio towards streamlining the bread-making process. According to comparison and analysis on dough properties and bread quality depending on mixture materials, it was found that Salt 2 had the highest dough temperature of all, and Salt 1 had the highest fermentation rate and specific volume but the lowest hardness (i.e. highest softness). Results of sensory evaluation, were that Salt 1.5 scored highest points in sweet taste, aftertaste, and overall acceptance, but there were significant differences among bread samples. Likewise, it was found that Fat 6 had the highest dough temperature, fermentation rate and specific volume of all. Texture analysis, showed that Fat 0 had the highest hardness of all. According to sensory characteristics, Fat 3 scored the highest points in overall acceptance. Based on these results, the optimum mixture ratio of salt and fat for microwave-irradiated bread was found to be 1.5% salt and 3% fat.

Freezing-thawing resistance evaluation of sandy soil, improved by polyvinyl acetate and ethylene glycol monobutyl ether mixture

  • Fard, Ata Rezaei;Moradi, Gholam;Ghalehjough, Babak Karimi;Abbasnejad, Alireza
    • Geomechanics and Engineering
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    • v.23 no.2
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    • pp.179-187
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    • 2020
  • Freezing-thawing cycles have significant effect on soils engineering behavior in frozen areas. This effect is more considerable in fine-graded than coarse-grained soils. The objective of this study is improving soil durability and strength in continues freezing-thawing cycles. For getting this purpose mixture of Polyvinyl Acetate (PVAc) and Ethylene Glycol Monobutyl Ether (EGBE) has been added to fine-grained soil and final prepared samples were tested at different freezing-thawing cycles. PVAc was mixed with 1%, 2% and 3% of soil weight. Half of PVAc weight was used as weight of EGBE. Freezing-Thawing cycles were exposed to samples and they were tested at different cycles. Results showed that adding mixture of PVAc+EGBE improved strength and durability of samples up to 10 freezing-thawing cycles. Unconfined compress strength tests were applied to samples and stress and strain of samples were tested on failure time. Behavior of samples was different at different percentages of mixture. Results showed that increasing amount of PVAc from 1% to 2% had more considerable effect on final stress than 2% to 3%. Using higher percentages of PVAc + EGBE mixture leaded to that samples carried more strain before collapsing. Another result gained from tests was that, freezing-thawing effect was more considerable after fourth cycles. It means differences between first and fourth cycles were more considerable than differences between fourth and tenth.

Composition, Source, and Regional Concentration of PBDEs in Pine Needles (소나무 잎 중 PBDEs의 조성, 발생원 및 지역적 농도)

  • Yeo, Hyun-Gu;Cho, Ki-Chul;Chun, Man-Young
    • Journal of Korean Society of Environmental Engineers
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    • v.28 no.8
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    • pp.829-835
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    • 2006
  • The composition, source, and regional concentration of polybrominated diphenyl ethers(PBDEs) were measured in pine needles with several sites in Korea. Homologs specific analysis confirmed that hepta-BDE(bromodiphenyl ethers) through deca-BDE were predictive indicator for total PBDEs concentration(Pearson's correlation coefficient r>0.96, p<0.001). Deca-BDE were detected in relatively very high concentration compared to other PBDE congeners in all samples. The similarity of between congeners profile to those of Bromkal 70-5DE and DE-71, the commercial mixture of PBDEs, indicates these mixtures are source of PBDEs observed in these sites. Also, BDE-47, -99, -100, -206, -207, and -209 were the dominant congeners in all samples, suggesting that the widely used commercial penta- and deca-BDE technical mixture were the original sources. However, Pearson's correlation coefficients of between BDE-209 and BDE-47, -99, -100 were insignificant, which implied that tetra-BDE and penta-BDE may originate from secondary sources such as air-plant partition in manner similar to that of the PCBs, while deca-BDE formulation still has primary sources.

Development of Hybrid Calcium Carbonate for High Loading Paper (I) - Manufacture and Application of Hybrid Calcium Carbonate - (고충전지 제조를 위한 하이브리드 탄산칼슘 충전제의 개발 (I) - 하이브리드 탄산칼슘의 제조 및 이용 -)

  • Jung, Jae Kwon;Seo, Yung Bum
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.47 no.4
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    • pp.30-37
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    • 2015
  • Needs for high ash loading in printing paper increase as green house gas (GHG) emission regulation becomes more stricter and pressure of lowering paper production cost increases. To meet the needs, a new type of filler was developed. The mixture of ground calcium carbonate (GCC) and calcium oxide was pre-floccuated with polyelectrolyte and further treated with carbon dioxide to form new calcium carbonate between GCCs. The final products were called as hybrid calcium carbonate (HCC), and its properties were compared to the GCC and the pre-flocculated GCC. Results showed increase in tensile, smoothness, opacity, and bulk for HCC.

Effect of Reductive Bleaching on Optical Properties of Color Ledger (색지 폐지의 광학적 특성에 미치는 환원 표백의 영향)

  • 안병준;백기현
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.33 no.2
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    • pp.68-73
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    • 2001
  • This experiment was executed to clarify the optimum condition of reductive bleaching for 100% color papers. The reductive bleaching of the color paper was desirable to be done under such conditions as high temperature over $60^{\circ}C$ and high consistency within possibly short time. The FAS bleaching like the sodium hydrosulfite required oxygen-free condition. Especially, as the mixture between pulps and chemicals was favored in case of the high consistency, it was actively recommended. Therefore, it is desirable to control the dosage with the type of the dyes, the nature, the dye content, the paper compositions, and the targeting initial and final brightness.

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Effect of Treatments with Flame-retardant on Flame-resistance and Tensile Strength of Paper (난연 처리가 종이의 난연성 및 인장강도에 미치는 영향)

  • Song, Han-Kyu;Lee, Myoung-Ku
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.38 no.4 s.117
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    • pp.61-67
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    • 2006
  • The effect of several inorganic flame-retardants such as ammonium phosphate, ammonium sulfate, aluminum hydroxide and antimony trioxide on the flame-retardant property and tensile strength of paper has been investigated. Flame-retardants were used preferably as a dry powdered mixture and added to the furnish. Both dipping and coating treatments were employed to apply flame-retardants to paper Flame-retardant paper was manufactured by treatment of $5{\sim}30%$ flame-retardants by weight of the paper on a dry weight. Paper's flame-retardant property and tensile strength were examined by comparison of char length and tensile index. As dosages of flame-retardant chemicals increased, flame-retardant property was improved but tensile index was decreased.

Energy Savings and Strength Improvement of Old Corrugated Container by Application of Wood Flour and Starch (목분과 전분을 이용한 골판지원지의 건조효율 및 물성향상)

  • Seo, Yung Bum;Jung, Jae Gwon;Ji, Sung Gil
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.48 no.2
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    • pp.99-105
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    • 2016
  • The increase of wet web solid content after wet press and dry compressive strength were observed in lab study by judicious application of wood flour and starch for the old corrugated container (OCC). Pearl starch was better than cationic starch in strength development, but cationic starch was better for drainage. Application of vacuum on the mixed solution of wood flour and starch helped strength development further without loss of other properties. The effect of wood flour addition on wet web solid content improved as the wet pressing pressure increased. The use of wood flour and starch mixture improved wet web solid contents further.

Assessment of swelling pressure of stabilized Bentonite

  • Angin, Zekai;Ikizler, Sabriye Banu
    • Geomechanics and Engineering
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    • v.15 no.6
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    • pp.1219-1225
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    • 2018
  • In this study, a comprehensive laboratory experimental programme was conducted on expansive soil with a high swelling potential to study the influence of different additive materials on swelling pressure and index properties. Lime, sand, multifilament fiber and fibrillated fiber were used for stabilization of expansive soil. Lime, sand and fibers were respectively added to the expansive soil at 0-7%, 0-80%, 0-0.5%. On each mixture that was prepared by the proportions mentioned above, Atterberg limits, compaction, and swelling pressure tests were conducted. From the result of these experiments, the swelling pressure-time relation could be replaced by a rectangular hyperbola established to facilitate the prediction of ultimate percent swelling with a few initial data points. The best type of additive and its optimum ratio for engineering purposes could be estimated rapidly by this approach.

Lightweight aggregates coated with colemanite

  • Bideci, Alper;Bideci, Ozlem Salli;Oymael, Sabit;Gultekin, Ali Haydar;Yildirim, Hasan
    • Computers and Concrete
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    • v.19 no.5
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    • pp.451-455
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    • 2017
  • Technological advancements in the field of building materials are achieved day by day. In this study, a new lightweight concrete aggregate is produced by mixing certain rates of colemanite (0%, 7.5%, 12.5%, 17.5%), cement and coating the surface of pumice aggregate with this mixture. Thin aggregate sections are analyzed with specific gravity, unit weight, water absorption, impact, and crushing experiments. In this way, the production of cement and cement+colemanite coated lightweight concrete aggregates is investigated and an opinion on the likely behavior of these concrete types is provided.