• 제목/요약/키워드: TL Analysis

검색결과 287건 처리시간 0.028초

Database of virtual spectrum of artificial radionuclides for education and training in in-situ gamma spectrometry

  • Yoomi Choi;Young-Yong Ji;Sungyeop Joung
    • Nuclear Engineering and Technology
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    • 제55권1호
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    • pp.190-200
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    • 2023
  • As the field of application of in-situ gamma spectroscopy is diversified, proficiency is required for consistent and accurate analysis. In this study, a program was developed to virtually create gamma energy spectra of artificial nuclides, which are difficult to obtain through actual measurements, for training. The virtual spectrum was created by synthesizing the spectra of the background radiation obtained through actual measurement and the theoretical spectra of the artificial radionuclides obtained by a Monte Carlo simulation. Since the theoretical spectrum can only be obtained for a given geometrical structure, representative major geometries for in-situ measurement (ground surface, concrete wall, radioactive waste drum) and the detectors (HPGe, NaI(Tl), LaBr3(Ce)) were predetermined. Generated virtual spectra were verified in terms of validity and harmonization by gamma spectrometry and energy calibration. As a result, it was confirmed that the energy calibration results including the peaks of the measured spectrum and the peaks of the theoretical spectrum showed differences of less than 1 keV from the actual energies, and that the calculated radioactivity showed a difference within 20% from the actual inputted radioactivity. The verified data were assembled into a database and a program that can generate a virtual spectrum of desired condition was developed.

Non-iterative pulse tail extrapolation algorithms for correcting nuclear pulse pile-up

  • Mohammad-Reza Mohammadian-Behbahani
    • Nuclear Engineering and Technology
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    • 제55권12호
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    • pp.4350-4356
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    • 2023
  • Radiation detection systems working at high count rates suffer from the overlapping of their output electric pulses, known as pulse pile-up phenomenon, resulting in spectrum distortion and degradation of the energy resolution. Pulse tail extrapolation is a pile-up correction method which tries to restore the shifted baseline of a piled-up pulse by extrapolating the overlapped part of its preceding pulse. This needs a mathematical model which is almost always nonlinear, fitted usually by a nonlinear least squares (NLS) technique. NLS is an iterative, potentially time-consuming method. The main idea of the present study is to replace the NLS technique by an integration-based non-iterative method (NIM) for pulse tail extrapolation by an exponential model. The idea of linear extrapolation, as another non-iterative method, is also investigated. Analysis of experimental data of a NaI(Tl) radiation detector shows that the proposed non-iterative method is able to provide a corrected spectrum quite similar with the NLS method, with a dramatically reduced computation time and complexity of the algorithm. The linear extrapolation approach suffers from a poor energy resolution and throughput rate in comparison with NIM and NLS techniques, but provides the shortest computation time.

Principal Component Analysis and Molecular Characterization of Reniform Nematode Populations in Alabama

  • Nyaku, Seloame T.;Kantety, Ramesh V.;Cebert, Ernst;Lawrence, Kathy S.;Honger, Joseph O.;Sharma, Govind C.
    • The Plant Pathology Journal
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    • 제32권2호
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    • pp.123-135
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    • 2016
  • U.S. cotton production is suffering from the yield loss caused by the reniform nematode (RN), Rotylenchulus reniformis. Management of this devastating pest is of utmost importance because, no upland cotton cultivar exhibits adequate resistance to RN. Nine populations of RN from distinct regions in Alabama and one population from Mississippi were studied and thirteen morphometric features were measured on 20 male and 20 female nematodes from each population. Highly correlated variables (positive) in female and male RN morphometric parameters were observed for body length (L) and distance of vulva from the lip region (V) (r = 0.7) and tail length (TL) and c' (r = 0.8), respectively. The first and second principal components for the female and male populations showed distinct clustering into three groups. These results show pattern of sub-groups within the RN populations in Alabama. A one-way ANOVA on female and male RN populations showed significant differences ($p{\leq}0.05$) among the variables. Multiple sequence alignment (MSA) of 18S rRNA sequences (421) showed lengths of 653 bp. Sites within the aligned sequences were conserved (53%), parsimony-informative (17%), singletons (28%), and indels (2%), respectively. Neighbor-Joining analysis showed intra and inter-nematodal variations within the populations as clone sequences from different nematodes irrespective of the sex of nematode isolate clustered together. Morphologically, the three groups (I, II and III) could not be distinctly associated with the molecular data from the 18S rRNA sequences. The three groups may be identified as being non-geographically contiguous.

Alkaline Protease를 이용한 Corn Gluten Meal의 효소가수분해 반응특성 및 반응속도론적 분석 (Reaction Characteristics and Kinetic Analysis of Enzymatic Hydrolysis of Corn Gluten Meal Using Alkaline Protease)

  • 김성진;이은규남충희
    • KSBB Journal
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    • 제10권5호
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    • pp.540-546
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    • 1995
  • bacterial alkaline protease를 이 용한 corn glu ten meal의 효소가수분해시 pH, 온도, 효소대 기질의 질량비율 등에 따른 반응특성 및 반응의 적정화 를 꾀하였고, 효소의 deactivation여부에 초점을 맞추어 효소반응속도론적 방정식을 제안조사하였다. 그 결과,$50^{\circ}C$, pH 9~10에서 가장 높은 가수분해 도를 나타내었고 $e_0/s_o$가 높을수록 반응속도 빛 최종 가수분해도가 증가하였다. 최종가수분해도는 gluten meal전체질량기준으로 17~20%, gluten meal내의 단백질질량기준으로 25 ~ 28 % 였다. 반응후반에서의 반응속도감소의 주된 원인은 기 질소진 (substrate de pletion) 이며 이때 enzyme deactivation 및 product inhibition의 영향은 미미한 것으로 확인되었다. 효소 deactivation항을 무시하여 변형시킨 model equa-tlOn에 의해 이 효소반응에 해당하는 여러 kinetic parameter들의 값을 계산분석한 결과 product inhi bition효과가 미미함을 확인하였다. 변형된 kinetic equation과 실험적으로 얻은 가수분해 데이타는 거 의 완벽하게 일치하였다. 효소반응을 $100\times$scale­u up한 결과 가수분해 profile 및 가수분해도는 $1\times$ 와 비교시 거의 일치하였으므로 이 효소반응이 용이하 게 scale-up될 수 있음을 확인하였고, 아미노산분석 결과 가수분해액을 미생물발효기질용 질소원으로 사 용할 수 있음을 제시하였다.

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한국 전통 양념을 이용한 발효 돼지고기의 품질 특성 (Quality Characteristics of Fermented Pork with Korean Traditional Seasonings)

  • 진상근;김철욱;이상욱;송영민;김일석;박석규;하경희;배대순
    • Journal of Animal Science and Technology
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    • 제46권2호
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    • pp.217-226
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    • 2004
  • 이 연구는 한국 전통 양념을 이용한 발효 돼지고기의 품질 특성에 관한 것으로 돼지고기의 바깥 볼깃살을 채취하여 7${\times}$12${\times}$2cm 크기로 자른 후 육을 동일한 비율의 양념액에 침지하여 -1${\pm}$1$^{\circ}C$에서 20일간 숙성한 발효육[T1(마늘소스 돼지고기), T2(제육김치 돼지고기), T3(김치소스 돼지고기), T4(된장소스 돼지고기), T5(고추장소스 돼지고기)]의 품질 특성을 측정한 결과는 다음과 같다. T1은 수분이 가장 높은 반면 조단백질 함량이 가장 낮았으며, T5는 수분이 가장 낮은 반면 조단백질과 조지방 함량이 가장 높았다. 양념 페이스트와 발효육의 pH는 T1이 가장 높았으며, T3가 가당 낮게 나타났다. 보수력은 T4와 T5가 매우 높고, T3는 가장 낮았다. 전단력은 T5가 가장 높고, T4가 가장 낮게 나타났다. 지방산패도는 T3가 가장 높았으며, T4가 가장 낮았다. 휘발성염기태질소화합물은 T4가 가장 높았으며, T1이 가장 낮았다. 당도는 T5가 가장 높았으며, T3가 가장 낮았다. 염도는 T2가 가장 높았으며, T5가 가장 낮았다. 표면육색과 심부육색 모두 $L^*$값, $a^*$값, $b^*$값은 각각 T4, T2, T2가 가장 높았으며, $L^*$값은 T5가 가장 낮았다. 가열육의 관능평가 결과 전 항목 및 전체적인 기호도는 T5가 가장 높았으며, T4가 가장 낮았다. 불포화지방산 비율은 T5가 많고 T2는 적었다. 불포화지방산/포화지방산 비율은 T5, T4, T3, T1, T$, T3순이었다. 이상의 결과를 요약하여 볼 때, 소비자가 구입을 꺼려하는 뒷다리살을 한국 전통양념류를 이용하여 제품을 만들었을 때, 제품의 맛과 품질을 개선시켜 그 소비를 촉진 시킬 수 있을 것으로 사료되며 앞으로 포장방법과 유통기간 설정 등 이에 대한 더욱더 많은 연구가 이루어져야 하겠다.

바이오모니터링 프로그램을 위한 혈중 금속류 동시분석법 개발 및 확인 평가 (Development and Verification of a Simultaneous Analytical Method for Whole Blood Metals and Metalloids for Biomonitoring Programs)

  • 차상원;오은하;오세림;한상범;임호섭
    • 한국환경보건학회지
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    • 제47권1호
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    • pp.64-77
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    • 2021
  • Objective: Biological monitoring of trace elements in human blood samples has become an important indicator of the health environment. The purpose of this study was to detect and evaluate multiple metal items in blood samples based on ICP-MS, to perform comparative evaluation with the existing analysis method, and to develop and verify a new method. Methods: 100 μL of whole blood from 80 healthy subjects was used to analyze ten metals (Sb, tAs, Cd, Pb, Mn, Hg, Mo, Ni, Se, Tl) using ICP-MS. Verification of the analysis method included calculation of linearity, accuracy, precision and detection limits. In addition, a comparative test with the conventional graphite furnace atomic absorption spectroscopy (GF-AAS) method was performed. In the case of Pb, Cd, and Hg in whole blood, cross-analysis between Pb, Cd, and Hg analysis methods was performed to confirm the difference between the existing method and the new method (ICP-MS). Results: The coefficient of determination (R2) was 0.999 or higher in seven items and 0.995 or higher in three items. The Pb result showed that Pearson's correlation coefficient was very high at 0.983, and the intraclass correlation coefficient was 0.966. The Cd result showed that Pearson's correlation coefficient was 0.917 between the existing method and the new analysis concentration value. Its intraclass correlation coefficient was 0.960, and there was no significant difference between the two groups. Hg had a low correlation at 0.687, and the intraclass correlation coefficient was 0.761, which was lower than that of Pb and Cd. The intra-day and inter-day accuracy of Pd and Cd were satisfactory, but Hg did not meet the criteria for both accuracy and precision when compared with the conventional analysis method. Conclusion: This study can be meaningful in that it proposes a more efficient and feasible analysis method by verifying a blood heavy metal concentration experiment using multiple simultaneous analyses. All samples were processed and analyzed using the new ICP-MS. It was confirmed that the agreement between the two methods was very high, with the agreement between the current and new methods being 0.769 to 0.998. This study proposes an efficient simultaneous methodology capable of analyzing multiple elements with small samples. In the future, studies of various applications and the reliability of ICP-MS analysis methods are required, and research on the verification of accurate, precise, and continuous analysis methods is required.

Isotope Measurement of Uranium at Ultratrace Levels Using Multicollector Inductively Coupled Plasma Mass Spectrometry

  • Oh, Seong-Y.;Lee, Seon-A.;Park, Jong-Ho;Lee, Myung-Ho;Song, Kyu-Seok
    • Mass Spectrometry Letters
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    • 제3권2호
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    • pp.54-57
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    • 2012
  • Mass spectrometric analysis was carried out using multicollector inductively coupled plasma mass spectrometry (MC-ICP-MS) for the precise and accurate determination of the isotope ratios of ultratrace levels of uranium dissolved in 3% $HNO_3$. We used the certified reference material (CRM) 112-A at a trace level of 100 pg/mL for the uranium isotopic measurement. Multiple collectors were utilized for the simultaneous measurement of uranium isotopes to reduce the signal uncertainty due to variations in the ion beam intensity over time. Mass bias correction was applied to the measured U isotopes to improve the precision and accuracy. Furthermore, elemental standard solution with certified values of platinum, iridium, gold, and thallium dissolved in 3% $HNO_3$ were analyzed to investigate the formation rates of the polyatomic ions of $Ir^{40}$ $Ar^+$, $Pt^{40}$ $Ar^+$, $Tl^{40}$ $Ar^+$, $Au^{40}$ $Ar^+$ for the concentration range of 50-400 pg/mL. Those polyatomic ions have mass-to-charge ratios in the 230-245 m/z region that it would contribute to the increase of background intensity of uranium, thorium, plutonium, and americium isotopes. The effect of the polyatomic ion interference on uranium isotope measurement has been estimated.

변화된 업무환경에서 인식하는 항공사 서비스품질이 글로벌 브랜드 (항공사 조인트벤쳐) 이미지 형성에 미치는 영향 연구 (A Study of the Effect of Perceived Service Quality under the New Service Environment on Formulating Airline's Global Brand(Joint Venture) Image)

  • 김태준;김기웅;박성식;이수미
    • 한국항공운항학회지
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    • 제26권3호
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    • pp.66-76
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    • 2018
  • Terminal 2 of Incheon in'tl airport had made a grand opening since January 2018. Terminal 2 is currently operated by mainly Korean airline in cooperation with such skyteam members as Delta airline, Air France and Royal Dutch KLM. It is expected another three skyteam member airlines join the separate operation at terminal 2 since this coming winter. It is believed very meaningful research to analyze how separate operation of Global alliance of airlines affects the global brand image of an organization. To find out such effect, researchers have made an empirical analysis of perception of airline staffs working at terminal 2. This paper has focused on how the staffs perceive airline service quality in the changed working environment and on how significantly their perception on service has an effect on airline's global brand image with such moderating variables as organizational efficacy and organizational trust. According to empirical analysis using structural equation modeling, it was proven the variable of responsiveness among perceived airline service qualities had a direct significant effect on formulating airline's global brand image associated with joint venture between Korean airline and Delta airline. However, the other variables had a indirect significant effect on global brand image with moderating effects.

Is Mathematics Teaching in East Asia Conducive to Creativity Development? - Results from the TIMSS 1999 Video Study and the Learners' Perspective Study

  • Leung Frederick K. S.;Park Kyungmee
    • 한국수학교육학회지시리즈D:수학교육연구
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    • 제9권3호
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    • pp.203-231
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    • 2005
  • Students in East Asia have consistently out-performed their counterparts in the West in recent international studies of mathematics achievement. But some studies also show that East Asian students are more rigid in thought, and lack originality and creativity. While different theories have been proposed to account for these student performances, relatively few research studies have been done on classroom practices, potentially a major variable for explaining student performances. This paper will report on the results of two classroom studies: the TIMSS 1999 Video Study and the Learners' Perspective Study (LPS). Results the quantitative analysis of the TlMSS 1999 Video Study data show that the East Asian classrooms were dominated by teacher talk, and the mathematics content learned was abstract and unrelated to the real life. On the other hand, the characteristics of the instructional practices in Hong Kong as judged by an expert panel are that student learned relatively advanced mathematics content; the components of the lessons were more coherent, and the presentation of the lessons was more fully developed. Hong Kong students seemed to be more engaged in the mathematics lessons, and the. overall quality of the lessons was judged to be high. Results of the analysis of the LPS data also show that the classrooms in the East Asian city of Seoul were in general teacher dominated, but students were usually actively engaged in the mathematics learning. Emphasis on exploration of mathematics and practicing exercises with variation was common. It is argued that the quality teaching in the East Asian classrooms laid a firm foundation in mathematics for students, and that constitutes a necessary condition for the development of students' creativity. In order to fully develop the creativity of East Asian students, they need to be given the right environment and encouragement.

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Suggestion of Model Change Work Improvement by REBA and Therblig

  • Lee, Sung-Koon;Park, Peom
    • 대한인간공학회지
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    • 제30권6호
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    • pp.757-764
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    • 2011
  • Objective: The aim of this study was to provide a method to improve the compliance and reduce the time by reducing the workload during the model change work. Background: The enterprises are constructing the small quantity batch production system by increasing the number of model change and reducing model-changing. However, the compliance is low because the work is strenuous and high skills are needed, so the system management is facing with many difficulties. Method: After classifying the model change work according to the purposes(preparation, change and adjustment) with the target of mascara filling machine, element tasks time were measured and the motion analysis(therblig symbol) and REBA analysis were performed. The study incorporated 3 independent variables as the number of motion, REBA score and the element time. The dependent variable is the type of element work as preparation, change and adjustment. The statistical test was performed by one-way ANOVA(${\alpha}$ < 0.05). Results: For the preparation, the number of motions appeared in the order of Use(U), Transport Loaded(TL), and Position(P). The order appeared in change is Use(U), Release Load(RL), and Grasp (G). The adjustment appeared in the order of Position(P) and Use(U). The results of average motion time as the element work times divided by the number of motion appeared in the order of adjustment(1.85sec/motion), preparation(1.11sec/motion), and change(0.62sec/motion). The results of REBA showed that the average risk level of change and adjustment were medium, but 53.1% of change and 42.9% of adjustment were evaluated as high. Conclusion: Reducing the avoidance and improving the compliance of work could be expected if the job autonomy were improved by improving the working postures with high risk level. Application: It is expected to solve the problem of reducing the time of model change work in the small quantity batch production system. The future work is to carry out the improvement directions found in the results and compare the results after improvement.