• Journal of Industrial and Engineering Chemistry
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• v.68
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• pp.153-160
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• 2018

An environmentally favorable (chlorine-free) solid oxidizer, guanidinium dinitramide [GDN; $NH_2C(NH_2)NH_2N(NO_2)_2$], was newly synthesized from guanidine carbonate [$NH_2C(=NH)NH_2{\cdot}1/2H_2CO_3$]. Two different crystalline forms (${\alpha}-type$ and ${\beta}-type$) appeared according to the applied solvents and synthesis conditions. Moisture, during extraction, might become trapped in a crystal between inner molecules. Therefore, despite having the same chemical composition, Raman-IR and TGA-DSC revealed different physical characteristics of the two forms. Peaks of Raman shift near $1000cm^{-1}$ implied different chemical structures. Thermal analysis revealed an exothermic temperature $155.7^{\circ}C$ for ${\alpha}-type$ but one of $191.6^{\circ}C$ for ${\beta}-type$. The caloric value of ${\alpha}-type$ was 536.4 J/g, which was 2.5 times larger than that of the ${\beta}-type$, which was 1310 J/g. While the synthesized GDN of ${\alpha}-type$ showed a steep exothermic decomposition, the ${\beta}-type$ was slowly decomposed after melting through an endothermic process. This work implied that despite of the same molecular formula some different core thermal properties would appear depending on synthesis conditions.

• 한국정보디스플레이학회:학술대회논문집
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• 2006.08a
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• pp.1409-1411
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• 2006

A new rod-like liquid crystalline monomer having divinyl terminal groups was synthesized and polymerized by using thiol-ene UV polymerization technique. High quality thin film with good retardation value was prepared on a rubbed alignment layer without the inert gas purging. The retardation value of the resulting film was controlled by experimental conditions such as spin speed, concentration, and spin time. From the retardation value and thickness measurement, ${\bigtriangleup}n$ was calculated to be 0.169 for the resulting film having thickness of 815.1 nm.

• Proceedings of the IEEK Conference
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• 2001.06b
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• pp.121-124
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• 2001

This paper proposed resource allocation algorithm for the minimum switching activity of functional unit in high level synthesis process as like DSP which is circuit to give many functional unit. The resource allocation method after scheduling use the power function calculating average hamming distance and switching activity of the between two input. First of all, the switching activity is calculated by the input value after calculating the average hamming distance between operation. In this paper, the proposed method though high If level simulation find switching activity in circuit each functional unit exchange for binary sequence length and value bit are logic one value. To use the switching activity find the allocation with minimal power consumption, the proposed method visits all control steps one by one and determines the allocation with minimal power consumption at each control step. As the existing method, the execution time can be fast according to use the number of operator and max control step. And it is the reduction effect from 6% to 8%.

• Publications of The Korean Astronomical Society
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• v.30 no.2
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• pp.381-383
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• 2015

MOdified Newtonian Dynamics (MOND) is an alternative to the dark matter paradigm. MOND asserts that when the magnitude of acceleration is smaller than the acceleration parameter $a_0$, the response of the system to gravity is stronger (larger acceleration) than the one given by Newtonian dynamics. The current value of $a_0$ is obtained mostly by observations of spiral galaxies (rotation curves and the Tully-Fisher relation). We attempt to estimate $a_0$ from the dynamics of elliptical galaxies. We seek elliptical galaxies that act as the lens of gravitational lensing systems and have velocity dispersion data available. We analysed 65 Einstein rings from the Sloan Len ACS survey (SLACS). The mass estimates from gravitation lensing and velocity dispersion agree well with each other, and are consistent with the estimates from population synthesis with a Salpeter IMF. The value of $a_0$ obtained from this analysis agrees with the current value.

• Journal of the Korean GEO-environmental Society
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• v.21 no.5
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• pp.5-11
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• 2020

Outliers detection and elimination included in field monitoring datum are essential for effective foundation of unusual movement, long and short range forecast of stability and future behavior to various structures. Integrated outlier analysis system for assessing long term time series data was developed in this study. Outlier analysis could be conducted in two step of primary analysis targeted at single dataset and second multi datasets analysis using synthesis value. Integrated outlier analysis system presents basic information for evaluating stability and predicting movement of structure combined with real-time safety management platform. Field application results showed increased correlation between synthesis value including similar sort of sensor showing constant trend and each single dataset. Various monitoring data in case of showing different trend can be used to analyse outlier through correlation-weighted value.

• Archives of Pharmacal Research
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• v.19 no.4
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• pp.307-311
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• 1996

The activity of fucosidase shows different value depending on disease, eg) fucosidosis and I cell disease are characterized by the absence or deficiences of .alpha.-fucosidase, and sera of ovarian cancer patients exhibited a statistically significant deficiency of .alpha.-L-fucosidase activity (Zielke et al., 1972; Kress et al., 1980; Barlow et al., 1981). For the purpose of diagnosis of these disease easily, the manual of test can be developed by preparing kits of hydrophobic-binding substrate of fucosidase that bind C18-column.

• Biotechnology and Bioprocess Engineering:BBE
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• v.4 no.1
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• pp.17-20
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• 1999

Facile synthetic methods of 2',5'-dideoxy-, 2',3'-dideoxy- and 3'-deoxy-1, N6-ethenoadenosine nucleosides by either an enzymatic dideoxyribosyl transfer reaction or a simple chemical reaction were proposed. The synthesis products were isolated and purified by preparative HPLC and their structures were confirmed by 1H NMR (500 MHz) and FAB-MS including high resolution mass measurement. These modified nucleoside analogs have not been reported yet. Therefore, these modified nucleoside analogs are of potential value to be studied further for biological activity such as anticancer or antiviral.

• Journal of the Korean Institute of Telematics and Electronics
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• v.4 no.1
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• pp.13-21
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• 1967

A low pass filter is synthesized with R, C and negative impedance converters(NIC). The filter has a 4-th order elliptic function, which gives best magnitude approximation with equi-ripple characteristics both in pass and stop band. And experimental investigations have been made on the effect of the anticipated deviation of the NIC conversion factor and of possible loaded operation. Through the study, it has been cocluded that: 1. For minimum pole-zero sensitivity with respect to the NIC conversion factor, the network of a parallel RC-NIC configuration is preferable and the Horowitz polynomial decomposition method is applied in the synthesis procedure. 2. A few percentage variation of the NIC conversion factor changes the frequency and amplitude characteristics of the filter by nearly negligible amount. 3. With a load resistance below the critical value, the filter turns into an oscillator.

• Proceedings of the Korean Institute of Intelligent Systems Conference
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• 2003.09b
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• pp.141-144
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• 2003

A composite adaptive dual fuzzy controller combining the approximate mathematical model, linguistic model description, linguistic control rules and identification modeling error into a single adaptive fuzzy controller is developed for a nonlinear system. It ensures the system output tracks the desired reference value and excites the plant sufficiently for accelerating the parameter estimation process so that the control performances are greatly improved. Using the Lyapunov synthesis approach, proposed controller is analyzed and simulation results verify the effectiveness of the proposed control algorithm.

• Biotechnology and Bioprocess Engineering:BBE
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• v.10 no.3
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• pp.167-179
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• 2005

Chiral epoxides are highly valuable intermediates, used for the synthesis of pharmaceutical drugs and agrochemicals. They have broad scope of market demand because of their applications. A major challenge in modern organic chemistry is to generate such compounds in high yields, with high stereo- and regio-selectivities. Epoxide hydrolases (EH) are promising biocatalysts for the preparation of chiral epoxides and vicinal diols. They exhibit high enantioselectivity for their substrates, and can be effectively used in the resolution of racemic epoxides through enantioselective hydrolysis. The selective hydrolysis of a racemic epoxide can produce both the corresponding diols and the unreacted epoxides with high enantiomeric excess (ee) value. The potential of microbial EH to produce chiral epoxides and vicinal diol has prompted researchers to explore their use in the synthesis of epoxides and diols with high ee values.