• Title/Summary/Keyword: Surface extraction

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Monitoring of Extraction Yields and Functional Properties of Ginger (Zingiber officinale) Extracts Using Response Surface Methodology (반응표면분석을 이용한 생강의 추출효율 및 기능성에 대한 모니터링)

  • Lim, Tae-Soo;Kwon, O-Jun;Kwon, Joong-Ho;Kim, Hyun-Ku
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.36 no.3
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    • pp.348-354
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    • 2007
  • Extraction characteristics of ginger (Zingiber officinale) and the functional properties of the corresponding extracts were monitored by the response surface methodology (RSM). The maximum extraction yield of 38.83% was obtained under the specific extraction conditions, such as microwave power of 126.68 W, ethanol concentration of 53.39% and extraction time of 8.15 min. The maximum electron donating ability (EDA) was found as 77.92% at the conditions of 58.25 W microwave power, 91.87% ethanol concentration and 5.54 min extraction time. The maximum inhibitory effect on tyrosinase was 79.39% at 106.08 W, 2.06% and 5.61 min. The maximum polyphenol content was 105.59% under the extraction conditions of 81.82 W, 99.52% and 4.06 min. Based on superimposition of four dimensional RSM with respect to extraction yield and electron donating ability and polyphenol content obtained under the various extraction conditions, the optimum ranges of extraction conditions were found to be microwave power of $0{\sim}80\;W$, ethanol concentration of $0{\sim}40%$ and extraction time of $3{\sim}7$ min.

Optimization of Extraction Conditions of Sarcodon aspratus by Response Surface Methodology (반응표면분석에 의한 능이버섯 추출물의 추출조건 최적화)

  • Lee, Hye-Jin;Jung, Sung-Keun;Do, Jeong-Ryong;Kim, Hyun-Ku
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.44 no.3
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    • pp.464-469
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    • 2015
  • Response surface methodology (RSM) was used to monitor extraction characteristics of extracts from Sarcodon aspratus. Based on a central composite design, independent variables were microwave power (30~150 W), ethanol concentration (0~100%), and extraction time (1~9 min). Dependent variables were yield, electron-donating ability, total phenol contents, and SOD-like activity. Coefficients of determination ($R^2$) for dependent variables ranged from 0.80 at 0.97. The maximum extraction yield was 50.28% under conditions of 125.1 W microwave power, 18.67% ethanolic concentration, and 7.06 min extraction time. The maximum extraction electron-donating ability was 22.14% under conditions of 31.09 W, 45.76%, and 4.32 min. The maximum extraction total polyphenol content was 30.54 mg tannic acid equivalent/g at 122.54 W, 48.05%, and 8.36 min. The maximum extraction SOD-like activity was 33.44% at 121.17 W, 47.42%, and 8.41 min. Based on superimposition of four dimensional RSM with respect to extraction yield, electron-donating ability, total polyphenol content, and SOD-like activity obtained under various extraction conditions, optimum ranges of extraction conditions were found to be microwave power of 78~88 W, ethanol concentration of 39~57%, and extraction time of 3.5~9 min.

Optimization of Extraction of Marker Compounds from Red Ginsengs by Accelerated Solvent Extraction Using Response Surface Methodology (반응표면분석법을 사용한 가속 용매 추출에 의한 홍삼 지표성분의 추출 최적화)

  • Kim, Eun Ok;Xu, Jiu Liang;Um, Byung Hun
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.45 no.8
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    • pp.1162-1169
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    • 2016
  • A new method based on accelerated solvent extraction (ASE) combined with response surface methodology (RSM) has been developed for optimization of the extraction of ginsenoside [Rb1, Rg1, and Rg3(20S)], total phenolics, and benzopyrene in red ginseng. The RSM method, based on a five level and two variable central composite design, was employed to obtain the optimal combination of extraction conditions. In brief, ginsenosides Rb1, Rg1, and Rg3(20S) and total phenolics with undetectable benzopyrene were optimally extracted with 50% ethanol as an extraction solvent, extraction temperature of $158^{\circ}C$, extraction time of 20 min, extraction pressure of 2,500 psi, flush volume of 60%, and one extraction cycle. The contents of ginsenosides and total phenolics in red ginseng extracted by ASE under optimum conditions were significantly higher than those extracted by sonication and reflux extraction.

Optimization of Extraction Conditions for Active Compounds of Herbal Medicinal Formula, DF, by Response Surface Methodology

  • Jeong, Birang;Choi, Seong Yeon;Jang, Hyeon Seok;Yoo, Guijae;Kim, Seung Hyun;Kim, Jung-Hwan;Kwon, Yong Soo;Roh, Jong Seong;Yoon, Yoosik;Shin, Soon Shik;Yang, Heejung
    • Natural Product Sciences
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    • v.23 no.1
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    • pp.9-15
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    • 2017
  • DF formula is comprised of three traditional herbs, Ephedra intermedia, Rheum palmatum and Lithospermum erythrorhizon, and locally used for treating of the metabolic diseases, such as obesity and diabetes in Korea. We tried to optimize the extraction conditions of two major components, (-)-ephedrine and (+)-pseudoephedrine, in DF formula using response surface methodology with Box-Behnken design (BBD). The experimental conditions with 70% for EtOH concentrations, 4.8 hour for extraction hours and 8.7 times for the solvent to material ratio were suggested for the optimized extraction of DF formula with the highest amounts of (-)-ephedrine and (+)-pseudoephedrine in the designed model.

Optimization of the Extraction of Polyphenols and Flavonoids from Argania spinosa Leaves using Response Surface Methodology

  • Rajaa Moundib;Hamadou Sita;Ismail Guenaou;Fouzia Hmimid
    • Natural Product Sciences
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    • v.29 no.2
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    • pp.83-90
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    • 2023
  • To our knowledge, this is the first study aiming to optimize the extraction conditions of total phenolic compounds (TPC) and total flavonoids contents (TFC) from Argania spinosa leaves using Response Surface Methodology (RSM) with a Box-Behnken design (BBD). The optimal conditions obtained were 5% (w/v) solvent-to-solid ratio, 72.33% ethanol concentration, and 10h ours as an extraction time, which resulted in an extract with maximum TPC (131.63 mg GAE/g dw) and TFC (10.66 mg QE/g dw). Under the optimal extraction conditions, the antioxidant activity of the extracts of leaves of argan tree showed a moderate antiradical capacity of DPPH (IC50 = 0,130 mg/mL) and ABTS (IC50 = 0.198 mg/mL). However, the leaves of argan tree showed a very interesting reducing power of Iron (IC50 = 0.448 mg/ml) which is similar to that of the ascorbic acid (IC50 = 0.371 mg/mL).

Extraction of the Surface Roughness in Grinding Operation by Acoustic Emission Signal (AE 신호에 의한 연삭가공 표면거칠기 검출)

  • Chung, Sung-Won
    • Journal of the Korean Society of Industry Convergence
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    • v.2 no.2
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    • pp.147-153
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    • 1999
  • An in-process extraction method of the ground surface roughness is a bottle-neck and essential field in conventional machining process. We define the D.A.R.F(Dimensionless Average Roughness Factor) that has a roughness characteristic of ground surface. D.A.R.F include the absolute average and the standard deviation values which are the analytic parameters of the AE(Acoustic Emission) signal generated during the grinding operation. The theoretical equation between the surface roughness and the D.A.R.F has been derived from the linear regressive analysis and verified its availability through the experimentation on the surface grinding machine.

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A Study on Medial Surface Extraction from Point Samples on 3D Closed Surfaces in Shell Shapes (셸 형상의 3차원 폐곡면상에서 추출된 점데이터군으로부터 중립곡면 계산에 관한 연구)

  • Woo, Hyuck-Je
    • Korean Journal of Computational Design and Engineering
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    • v.15 no.1
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    • pp.33-42
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    • 2010
  • In this study, new medial surface calculation methods using Voronoi diagrams are investigated for the point samples extracted on closed surface models. The medial surface is defined by the closure of all points having more than one closest point on the shape boundary. It is a one of essential geometric information in 3D and can be used in many areas such as 3D shape analysis, dimension reduction, freeform shape deformation, image processing, computer vision, FEM analysis, etc. In industrial parts, the idealized solid parts and shell shapes including sharp edges and vertices are frequently used. Other medial surface extraction methods using Voronoi diagram have inherent separation and branch problems, so that they are not appropriate to the sharp edged objects and have difficulties to be applied to industrial parts. In addition, the branched surfaces on sharp edges in shell shapes should be eliminated to obtain representative medial shapes. In order to avoid separation and branch problems, the new approach by analyzing the shapes and specially sampling on surfaces has been developed.

Monitoring of Extraction Properties of Ginseng Components during Pressurized Micorwave-Assisted Extraction (가압조건의 마이크로웨이브 추출에서 몇가지 인삼성분의 추출특성 모니터링)

  • 권중호;이새봄;이기동;정용진;김정숙
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.28 no.5
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    • pp.1087-1091
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    • 1999
  • Microwave extraction system equipped with closed vessels, which is known to rapidly extract target compounds from natural products, was applied to monitor the changes in phenolic compounds, browning color intensity and electron donating ability by using response surface methodology(RSM). Maximum content of phenolic compound was 21.65mg/100ml in 67.88% of ethanol concentration, 145oC of extraction temperature, and 6.24min of extraction time. The phenolic compounds in extracts are dependent on the increase of the extraction temperature and the ethanol concentration. Browning color intensity, which was maximized in 67.21%, 147oC, and 6.02min, was proportional to the increase of the extraction temperature. Maximum value of electron donating ability was 24.50units in 54.33%, 147oC, and 6.11 min. The electron donating ability of extracts was dependent on the increase of extraction temperature and maximized in the range from 50 to 65% of ethanol concentration.

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Analysis and Implementation of Traveling Surface Characteristics Test Equipment Using Optical Mice (광 마우스 기반 주행 표면 특성 시험 장치의 분석 및 구현)

  • Kim, Sungbok
    • Journal of Institute of Control, Robotics and Systems
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    • v.22 no.7
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    • pp.543-551
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    • 2016
  • This paper presents the analysis and implementation of traveling surface characteristics test equipment using optical mice in connection with the velocity estimation of a mobile robot equipped with optical mice. In the traveling surface characteristics test equipment, a traveling surface sample is made to rotate toward stationary optical mice instead of a mobile robot equipped with optical mice moving over a traveling surface. First, the conceptual design and operational principle of the traveling surface characteristics test equipment is explained. Second, the velocity kinematics of the traveling surface characteristics test equipment is formulated; based on this, the parameter setting of the traveling surface characteristics test equipment is described. Third, the implementation of the traveling surface characteristics test equipment is described in detail, including the mechanical design and construction and the hardware and software development. Fourth, using the prototype of the traveling surface characteristics test equipment, the experimental results of the statistical parameter extraction for different traveling surface samples are given. Finally, some potential usages of the traveling surface characteristics test equipment are discussed.

Automated Silhouette Extraction Method for Generating a Blueprint from 3D Scan Data of Cultural Asset (문화재의 3D 스캔 데이터로부터 도면을 생성하기 위한 자동화된 실루엣 추출 방법)

  • Jung, Jung-Il;Cho, Jin-Soo;WhangBo, Tae-Keun
    • The Journal of the Korea Contents Association
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    • v.8 no.12
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    • pp.10-19
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    • 2008
  • In this paper, we propose an automated silhouette extraction method that can effectively extract inner-patterns and silhouettes from 3D scan data of cultural asset. First of all, after creating the edge list of 3D vector data, we decide contour edge and crease edge according to viewpoint. In the next step, after extracting surface silhouette by investigating the vector variation of adjacent faces in crease edge, we finally extract the contour silhouette and surface silhouette for generating the blueprint of cultural asset. To evaluate the performance of the proposed silhouette extraction method, we performed experiments of silhouette extraction using a traditional tile model, a car model and a stone monument model. Comparing with the conventional threshold-based silhouette extraction method, the proposed method extracted more distinct and clear surface silhouettes and inner-patterns by effectively removing meaningless edges, such as noise.