• 한국전기전자재료학회논문지
• /
• 제14권7호
• /
• pp.606-610
• /
• 2001

Bi-2212 HTS tube was fabricated by centrifugal forming and partial melting processes. Bi-2212 bulk tube has been optimized to achieve smooth surface and uniform thickness. The slurry was prepared in the mixing ratio of 10:1 between Bi-2212 powder and binder and initially charged into the rotating mold under the speed of 300~450 rpm. Heat-treatment was performed at the temperature ranges of 860~89$0^{\circ}C$ in air for partial melting. the HTS tube fabricated by centrifugal forming process at 89$0^{\circ}C$ under the rotating speed of 450 rpm was highly densified and the plate-like grains with more than 20${\mu}{\textrm}{m}$ were well oriented along the rotating axis. The measured Tc and J$_{c}$ at 10K on specimen heat treated at 89$0^{\circ}C$ was around 85 K and 1,200 A/$\textrm{cm}^2$ respectively.y.

• 한국초전도학회:학술대회논문집
• /
• 한국초전도학회 2000년도 High Temperature Superconductivity Vol.X
• /
• pp.211-215
• /
• 2000

Bi-2212 HTS tube was fabricated by CFP(Centrifugal Forming Process). Slury was prepared in the mixing ratio of 8:2 between powder and binder and ball-milled for 24 hrs. Slurry was initially charged into the rotating mold with 300${\sim}$450 rpm and heated at the temperature ranges of 840${\sim}$860$^{\circ}$C for partial melting to finally obtain a uniformly textured tube shape. It was observed the plate-like grains with more than 20 ${\mu}$m were well oriented along the rotating axis and the measured T$_c$ was around 67K. In this paper we will discuss and analyze the tube characteristics depending on many different processing parameters such as, powder composition, binder mixing ratio between powder and binder, motor speed, heating temperature and etc.

• Progress in Superconductivity
• /
• 제2권1호
• /
• pp.6-10
• /
• 2000

New cuprates with the nominal composition $(Pb_{0.75}Sn_{0.25})Sr_2(Ca_{1-x}Lu_x)Cu_2O_z(x=0.4{\sim}1.0)$ have been synthesized. These materials exhibit superconducting properties for 0.4 $\leq$ x $\leq$ 0.7. It is also observed that the superconductivity of the as-prepared sample is enhanced by post-annealing at high temperature followed by quenching. X-ray diffraction analysis reveals that the c lattice parameter decreases as x increases whereas the a lattice parameter is nearly independent of the value of x for both the as-prepared and the post-treated samples. The thermoelectric power measurements indicate that the post-heat-treatments result in an increase in the hole carrier density which account for the observed increase of $T_c$. Bulk superconductivity with a $T_c$ value of 60 K is observed in this system.

• 한국초전도학회:학술대회논문집
• /
• 한국초전도학회 2009년도 Korea Superconductivity Society Meeting 2009
• /
• pp.39-39
• /
• 2009

• 한국초전도학회:학술대회논문집
• /
• 한국초전도학회 2009년도 Korea Superconductivity Society Meeting 2009
• /
• pp.54-54
• /
• 2009

• 한국전기전자재료학회논문지
• /
• 제29권2호
• /
• pp.106-109
• /
• 2016

The YBaCuO superconducting bulks were prepared by the thermal diffusion process involving the peritectic reaction to investigate the effect on microstructure and superconductivity. All the diffused YBaCuO could be successively separated from superconducting 123 phase by applying the thermal diffusion process. Electromagnetic properties of treated and untreated YBaCuO superconductor were evaluated to investigate the pinning effect. It was confirmed experimentally that a large amount of magnetic flux was trapped in the thermal treated superconducting bulk than that in the untreated one, indicating that the pinning centers of magnetic flux are related closely to the occurrence mechanism of the magnetic effect.

• 대한전기학회논문지:전기기기및에너지변환시스템부문B
• /
• 제52권9호
• /
• pp.442-447
• /
• 2003

Motors with HTS wires or bulks have been developing recently. Those are large synchronous motor with HTS wires at the field winding in the rotor, hysteresis and reluctance motors with HTS bulk in the rotor. This paper presents the fabrication and test results of an HTS induction motor. Conventional end rings and short bars were replaced with HTS wires in the motor. Stator of the conventional induction motor was used as the stator of the HTS motor. Rated capacity and rpm at full rotor of the conventional motor were 0.75[kW] and 1,710[rpm]. Two, HTS wires are used in parallel to make the end rings and bars. The critical current of the BSCCO-2223 HTS wire which was used in the bars and end rings were 115[A]. Electrodynamometer was coupled directly to the shaft of the rotor with HTS wires.

• 한국전기전자재료학회논문지
• /
• 제20권6호
• /
• pp.550-554
• /
• 2007

Large and single-grain Y-Ba-Cu-O(YBCO) bulk superconductors have been fabricated by using a seeded infiltration and growth method. $Y_2BaCuO_5$(Y211) precursor pellets and $YBa_2Cu_3O_x$(Y123) liquid source pellets were prepared using commercial powder and were processed by infiltration and growth method to achieve low pore and high trapped field property. The superconductor properties of the single crystal are measured and analyzed in relation with the density and size of the Y211 particle in the Y123 matrix. An optimum processing condition is suggested based on the analyzed results.

• 한국재료학회지
• /
• 제24권9호
• /
• pp.465-468
• /
• 2014

The crystallization effects of boron (B) powder on the phase, full width at half maximum (FWHM) values, and critical properties were investigated for in-situ reacted $MgB_2$ bulk superconductors. The semi-crystalline B powder was heat-treated at different temperatures of 1000, 1300 and $1500^{\circ}C$ for 5 hours in an Ar atmosphere. Then, using as-received and heat-treated B powders, the $MgB_2$ samples were prepared at $600^{\circ}C$ for 40 hours in an Ar atmosphere. As the heat-treatment temperature of the B powder increased, both the particle size of the B powder and crystalline phase increased. In the case of $MgB_2$ samples using B powders heat-treated at above $1300^{\circ}C$, unreacted magnesium (Mg) and B remained due to the improved crystallinity of the B powder. As the heat-treatment temperature of B powder increased, the critical current density of $MgB_2$ decreased continuously due to the reduction of grain boundary density and superconducting volume caused by unreacted Mg and B.

• 한국세라믹학회지
• /
• 제42권6호
• /
• pp.437-442
• /
• 2005

We fabricated BSCCO-2212 (2212) bulk superconductor by melt casting process, and evaluated the dependence of the critical properties on the temperature and cooling .ate of mold and the pouring methods of melt. It was observed that the critical current (Ic) of 2212 was significantly dependent on the pre-heating temperature of the mold. At the pre-heating temperature of $500^{\circ}C$ followed by air cooling condition, Ic of 48 A at 77 K was obtained which was higher than others processed at different temperatures. In addition, the Ic improved to 132 A when tilt casting method was applied. The improved Ic is probably due to the fact that the tilt casting reduced a turbulent flow of the melt during casting causing less porosity and more homogeneous microsructure. Critical temperature was measured to be 87-89 K after the first heat treatment and it improved to 90-91 K when subsequently heat treated at $650^{\circ}C$ in a nitrogen atmosphere. This improvement was considered to be due to an optimization of the oxygen content in the range of 8.16-8.2.