• Title/Summary/Keyword: Sub-50nm

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The Electric and Ferroelectric of Pb(Zr0.52Ti0.48)O3 Thin Films Deposited on Ruthenium Electrodes (루테늄 전극위에 증착된 PZT 박막의 전기적 및 강유전 특성)

  • Hwang, Hyun Suk;Yu, Yougn Sik;Lim, Yun-Sik;Kang, Hyun-Il
    • The Transactions of the Korean Institute of Electrical Engineers P
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    • v.63 no.1
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    • pp.46-49
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    • 2014
  • $Pb(Zr_{0.52}Ti_{0.48})O_3(PZT)$ thin films deposited on $Ru/RuO_2$ bottom electrode that grown for in-situ progress used rf magnetron sputtering method. We investigated the dependence of the crystalline and electrical properties in the way of capacitors PZT thin films. Our results show that all PZT films indicated polycrystalline perovskite structure with preferred orientation (110) and no pyrochlore phase is observed. The electric properties of the Ru improved with increasing Ru thin films thickness. A well-fabricated Ru/PZT/Ru (100 nm) /$RuO_2$ capacitor showed a leakage current density in the order of $2.03{\times}10^{-7}$ $A/cm^2$ as a 50 kV/cm, a remnant polarization (Pr) of 9.22 ${\mu}C/cm^2$, and a coercive field (-EC) of -32.22 kV/cm. The results show that $Ru/Ru/RuO_2$ bottom electrodes are expected to reduce the degradation ferroelectric fatigue and excellent ferroelectric properties.

Preparation of Y3Al5O12 Nanocrystals by a Glycol Route

  • Bartwal, Kunwar Singh;Kar, Sujan;Kaithwas, Nanda;Deshmukh, Monica;Dave, Mangla;Ryu, Ho-Jin
    • Journal of the Korean Ceramic Society
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    • v.44 no.5 s.300
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    • pp.151-154
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    • 2007
  • Yttrium aluminum garnet, $Y_3Al_5O_{12}$ (YAG) is an extensively used solid-state laser host material. YAG nanocrystals were synthesized using low-temperature glycol method, a modified sol-gel method performed at low temperature that consists of a mixture of salts that are mostly nitrates in an aqueous media. Single-phase nanocrystalline YAG was obtained at $850^{\circ}C$, which is a much lower temperature than with other techniques such as a wet-chemical technique. The structural characterization is done by powder X-ray diffraction, scanning electron microscopy and transmission electron microscopy. A crystallite size range of 20-50 nm was observed for the materials prepared at $850-950^{\circ}C$.

Characteristics of Micro Groove grinding for the Mold of PDP Barrier Ribs (PDP 격벽용 금형의 마이크로 홈 연삭 특성)

  • 조인호;정상철;박준민;정해도
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2000.05a
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    • pp.963-966
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    • 2000
  • Plasma display panel (PDP) is a type of flat panel display utilizing the light emission that is produced by gas discharge. Barrier Ribs of PDP separating each sub-pixel prevents optical and electrical crosstalk from adjacent sub-pixels. Mold for forming barrier ribs has been newly researched to overcome the disadvantages of conventional manufacturing process such as screen printing, sand-blasting and photosensitive glass methods. Mold for PDP barrier ribs have stripes of micro grooves transferring stripes of glass-material wall. In this paper. Stripes of grooves of which width 48 um, depth 124um, pitch 274um was acquired by machining the material of WC with dicing saw blade. Maximum roughness of the bottom and sidewall of the grooves was respectively 120 nm, 287 nm. Maximum tilt angle caused by difference between upper-most width and lower-most width was 2$^{\circ}$. Maximum Radius of curvature of bottom was 7.75 ${\mu}{\textrm}{m}$. This results meets the specification for barrier ribs of 50 inch XGA PDP. Forming the glass paste will be followed by using mold in the near future.

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Texture, Morphology and Photovoltaic Characteristics of Nanoporous F:SnO2 Films

  • Han, Deok-Woo;Heo, Jong-Hyun;Kwak, Dong-Joo;Han, Chi-Hwan;Sung, Youl-Moon
    • Journal of Electrical Engineering and Technology
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    • v.4 no.1
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    • pp.93-97
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    • 2009
  • The nanoporous $F:SnO_2$ materials have been prepared through the controlled hydrolysis of fluoro(2-methylbutan-2-oxy)di(pentan-2,4-dionato)tin followed by thermal treatment at $400-550^{\circ}C$. The main IR features include resonances at 660, 620 and 540 cm-1. From the TG-DTG result, three main mass losses of 6.5, 13.3 and 3.8 at 81, 289 and $490^{\circ}C$ are observed between 50 and $650^{\circ}C$ yielding a final residue of 76.0%. The size of Sn $O_2$ nanoparticles rose from 5 nm to 10-12 nm as the temperature of thermal treatment is increased from 400 to $550^{\circ}C$.

Investigation of the Combustion and Emission Characteristics of 1-Octanol/Diesel Fuel Blends in a Direct Injection Diesel Engine (직분사 디젤 엔진에서 1-옥탄올/경유 혼합 연료의 연소 및 배기 특성 연구)

  • CHEOL-OH PARK;JEONGHYEON YANG;BEOMSOO KIM;JAESUNG KWON
    • Transactions of the Korean hydrogen and new energy society
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    • v.34 no.1
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    • pp.69-76
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    • 2023
  • An experimental study was conducted on a 4-stroke direct injection diesel engine to examine the combustion and emission characteristics of 1-octanol/diesel fuel blends. The concentration of 1-octanol in the fuel blends was 10%, 30%, and 50% by volume. Experiments were conducted by varying the engine torque from 6 Nm to 12 Nm at the same engine speed of 2,700 rpm. Results showed that the fuel conversion efficiency increased as the 1-octanol proportion increased under most experimental conditions. However, the brake specific fuel consumption increased due to the relatively low lower heating value of 1-octanol. The smoke opacity and the concentrations of NOx and CO emissions generally decreased with brake mean effective pressure as the 1-octanol proportion increased. On the other hand, the unburned hydrocarbon concentration increased with an ascending ratio of 1-octanol.

Synthesis and Compaction Behavior of Monodispersed 3Y-ZrO2 Spherical Agglomerates

  • Choi, Hong-Goo;Yong, Seok-Min;Kim, Do Kyung
    • Journal of the Korean Ceramic Society
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    • v.50 no.6
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    • pp.434-438
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    • 2013
  • Monodispersed 3Y-$ZrO_2$ spherical agglomerates were synthesized by thermal hydrolysis process followed by crystallization processes (hydrothermal treatment and calcination). The crystallization process affected the properties of the final particles, such as the primary particle size, the agglomeration state, and the fraction of $ZrO_2$ monoclinic phase. The hydrothermal treated spherical particles were porous microstructures (weak agglomerates) composed of small primary particles with a size of 14 nm, but the calcined spherical particles had a dense microstructure due to the hard aggregation between primary particles. While the calcined particles had a low green density due to the hard aggregation, hydrothermal treated ones were soft agglomerates and had a deflection point at 50 MPa due to the rearrangement of secondary spherical particles and the filling of the interstices with the primary particles. Finally, the green density of hydrothermally treated $ZrO_2$ particles was 58% at 200 MPa.

Block Copolymer (BCP) 를 이용한 sub-50 nm 3차원 구조물 제작에 관한 연구

  • Sin, Jae-Hui;O, Jong-Sik;Yeom, Geun-Yeong
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2014.11a
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    • pp.15-15
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    • 2014
  • Block Copolymer(BCP) 는 self assembly 현상을 이용하여 다양한 pattern을 형성하는데 용이한 물질로써 이를 이용한 다양한 구조물 제작에 대한 연구가 활발히 진행되고 있다. 본 연구에서는 hoe pattern 모양을 갖는 BCP 패턴을 이용하여 Atomic Layer Deposition(ALD) 및 Reactive Ion Etching(RIE) 공정을 이용한 3차원 quantum tube 구조물을 제작하였다.

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Eine Structure of Cerebral Ganglion in the Korean Planaria, Dugesia japonica (한국산 플라나리아(Dugesia japonica) 뇌신경절의 미세구조)

  • Chang, Nam-Sub
    • Applied Microscopy
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    • v.29 no.1
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    • pp.57-66
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    • 1999
  • The nervous tissue in the cerebral ganglion of Korean planaria was observed using electron microscope. The obtained results are as follows: A cerebral ganglion is composed of the nerve cells, neurosecretory cells, neuroglial cells and neuropils. The nerve cells are round or ovoidal-shaped cells (diameter, $5{\mu}m$), which has a large ellipsoidal nucleus containing the evenly developed heterochromatin. Their cytoplasms were found to be relatively simple, because of their undeveloped cell organelles. The neurosecretory cells are long and ellipsoid or spindle-shaped cells, where there were found a large ellipsoidal nucleus and cytoplasm filled with secretory granules (diameter, 60 nm). The neuroglial cells were seldom observed. They are spindle-shaped cells (size, $6\times0.8{\mu}m$), which were observed mainly among the nerve fibers. The neuropils are formed by the nerve fibers and nerve endings which are filled with mitochondria, neurotubules and secretory granules of four kinds (high electron dense granules of sizes 75 nm, 50 nm and 37 nm, and electron lucent granule of size 30 nm etc.). These granular vesicles are divided into single vesicle type and compound vesicle type in the nerve terminals, and neuronal synapses were observed to be the axo-dendritic and dendro-dendritic synapse type.

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Synthesis of TiN-Coated cBN Powder by Sol-Gel Method Using Titanium (IV) Isopropoxide (티타늄 이소프로폭사이드를 이용한 졸-겔법에 의한 TiN 코팅 cBN 분말 합성)

  • Lee, Youn Seong;Kim, Sun Woog;Lee, Young Jin;Lee, Ji Sun;Shin, Dongwook;Kim, Sae-Hoon;Kim, Jin Ho
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.33 no.5
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    • pp.373-379
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    • 2020
  • In this study, TiN-coated cBN (cubic-structure boron nitride) powders were successfully synthesized by a sol-gel method using titanium (IV) isopropoxide (TTIP) and by controlling the heat treatment conditions. After the sol-gel process, amorphous nano-sized TiOx was uniformly coated on the surface of cBN powder particles. The obtained TiOx-coated cBN powders were heated at 1,000~1,300℃ for 1 or 6 h in a flow of 95%N2-5%H2 mixed gas. With increasing temperature, the chemical composition of the TiOx coating layer changed in the order of TiO2→Ti6O11→Ti4O7→TiN due to reduction of the Ti ions. The TiN coating layer was observable in the samples heated at 1,200℃ and appeared as the main phase in the sample heated at 1,300℃. The resulting thickness of the TiN coating layer of the sample heated at 1,300℃ was approximately 45~50 nm.

Development of an Axially Viewed Inductively Coupled Plasma for Atomic Emission Spectrometry and Comparison between the Detection Limits of Lead (원자방출 분광분석을 위한 수평형 유도결합 플라스마의 개발과 납 검출한계 비교)

  • Cho, Sung Il;Han, Myung Sub;Lee, Sang Hwa;Lee, Joung Hae;Woo, Jin Chun
    • Journal of the Korean Chemical Society
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    • v.41 no.6
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    • pp.292-298
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    • 1997
  • An ICP(Inductively Coupled Plasma) emission spectrometer was developed with an axially viewed ICP source incorporated by a 5-turned induction coil and a torch, outer quartz tube of which was 50 mm longer than that used in conventional ICP/AES(Inductively Coupled Plasma Atomic Emission Spectrometry). The Optimization of the system has been performed in terms of the determination of signal-to-noise ratio and background intensity at various rf powers, sample flow rates, argon gas flow rates and cut-off gas flow rates. The spectro-analytical characteristics of the spectrum obtained between 200 and 500 nm was revealed to be similar compared with a vertically viewed ICP source. The detection limit of Pb(Ⅱ) at 220.35 nm was 11 ppb which was 5 times lower than that obtained with a vertically viewed ICP source.

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