• Transactions of Materials Processing
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• v.14 no.1 s.73
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• pp.65-70
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• 2005

A phase mixture model was employed to simulate the deformation behaviour of metallic materials covering a wide grain size range from micrometer to nanometer scale. In this model a polycrystalline material is treated as a mixture of two phases: grain interior phase whose plastic deformation is governed by dislocation and diffusion mechanisms and grain boundary 'phase' whose plastic flow is controlled by a boundary diffusion mechanism. The main target of this study was the effect of grain size on stress and its strain rate sensitivity as well as on the strain hardening. Conventional Hall-Petch behaviour in coarse grained materials at high strain rates governed by the dislocation glide mechanism was shown to be replaced with inverse Hall-Petch behaviour in ultrafine grained materials at low strain rates, when both phases deform predominantly by diffusion controlled mechanisms. The model predictions are illustrated by examples from literature.

• Journal of the Optical Society of Korea
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• v.3 no.2
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• pp.64-68
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• 1999

The performance of a fiber Bragg grating strain sensor constructed with 3$\times$3 coupler is investigated. A 3$\times$3 coupler Mach-Zehnder (M/Z) interferometer is used as wavelength discriminator, interrogating strain-induced Bragg wavelength shifts. Two quadrature-phase-shifted intensities are synthesized from the as-coupled interferometer outputs, and digital arctangent demodulation and phase unwrapping algorithm are applied to extract the phase information proportional to strain. Due to the linear relation between the input strain and the output of quadrature signal processing, signal-fading problems eliminated. In the experiment, a fiber grating that was surface adhered on an aluminum beam was strained in different ways, and the photodetector signals were transferred and processed in a computer-controlled processing unit. A phase recovery fo 7.8$\pi$ pk-pk excursion, which corresponds to ~650$\mu$strain pk-pk of applied strain, was demonstrated. The sensor system was stable over the environmental intensi쇼 perturbations because of the self-referencing effect in the demodulation process.

• Transactions of the Korean Society of Automotive Engineers
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• v.3 no.1
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• pp.1-12
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• 1995

Isothermal and thermal-mechanical fatigue characteristics of 12Cr heat resisting steel used for high temperature applications were investigated including hold time effects. Isothermal low cycle fatigue test at $600^{\circ}C$ and in-phase, out-of-phase thermal-mechanical fatigue test at 350 to $600^{\circ}C$ were conducted using smooth cylindrical hollow specimen under strain-control with total strain ranges from 0.006 to 0.015. Regardless of thermal-mechanical and isothermal fatigue tests, cyclic softening behavior was observed and much more pronounced in the thermal-mechanical fatigue tests with hold times due to the stress relaxation during the hold time. The phase difference between temperature and strain in thermal-mechanical fatigue tests resulted in significantly shorter fatigue life for out-of-phase compared to in-phase. The differences in fatigue lives were dependent upon the magnitudes of plastic strain ranges and mean stresses. During the hold time in the strain-controlled fatigue tests, the increase in the plastic strain range and the stress relaxation were observed. It appeared that the increase in plastic strain range per cycle and the introduction of creep damage made important contributions to the reduction of thermal-mechanical fatigue life with hold time, and the life reduction tendency was more remarkable in the in-phase than in the out-of-phase thermal-mechanical fatigue. Isothermal fatigue tests performed under the combination of fast and slow strain rates at $600^{\circ}C$ showed that the fatigue life decreased as the strain rate and frequency decreased,especially for the low strain ranges.

• Proceedings of the Korean Vacuum Society Conference
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• 2012.02a
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• pp.572-572
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• 2012

Growth of metal oxides on graphene may lead to a better understanding of delicate effects of their growth habits on their underlying physics. The vanadium dioxide ($VO_2$) is well known for its metal-to-insulator transition accompanied by a reversible first order structural phase transition at 340 K. This transition makes $VO_2$ a potentially useful material for applications in electrical and optical devices. We report a successful growth of $VO_2$ nanostructures on a graphene substrate via a vapor-solid transport route. As-grown $VO_2$ nanostructures on graphene were systematically characterized by field emission scanning electron microscopy, x-ray diffraction, Raman spectroscopy, FT-IR spectroscopy and high resolution transmission electron microscopy. These results indicate that the strain between $VO_2$ and graphene layers may be easily controlled by the number of underlying graphene layer. We also found that the strain in-between $VO_2$ and graphene layer affected its metal-to-insulator transition characteristics. This study demonstrates a new way for synthesizing $VO_2$ in a desired phase on the transparent conducting graphene substrate and an easy pathway for controlling metal-to-insulator phase transition via strain.

• Journal of Industrial Technology
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• v.21 no.B
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• pp.331-339
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• 2001

Zero to tension fatigue tests and strain controlled fatigue tests were carried out to find how initial strain induced martensite, ${\alpha}^{\prime}$ affects low and high cycle fatigue behavior and fatigue crack growth mechanisms. Microscopic study and phase analysis were carried out with TEM, SEM, EDAX, Optical Microscope, Ferriscope, and X-ray diffractometry. The amount of Initial ${\alpha}^{\prime}$ was controlled from 0% to 33% by controlling the temperatures for cold working and heat treatment. Lower contents of initial ${\alpha}^{\prime}$ showed higher fatigue resistance in low cycle fatigue but lower fatigue resistance in high cycle fatigue because it is ascribed to the more transformation of ${\alpha}^{\prime}$ martensite during low cycle fatigue and higher ductility. In high cycle fatigue, fatigue life is attributed to the strength and phase transformation of austenite into ${\alpha}^{\prime}$ during fatigue was negligible. ${\gamma}$ boundary, ${\gamma}/twin$ boundary, and ${\gamma}/{\alpha}^{\prime}$ boundary were found to be the preferred site of fatigue crack initiation.

• Nuclear Engineering and Technology
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• v.51 no.6
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• pp.1525-1531
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• 2019

The indigenous nuclear power program of India is based mainly on a series of Pressurised Heavy Water Reactors (PHWRs). A burst correlation for Indian PHWR fuel claddings has been developed and empirical burst parameters are determined. The burst correlation is developed from data available in literature for single-rod transient burst tests performed on Indian PHWR claddings in inert environment. The heating rate and internal overpressure were in the range of 7 K/s-73 K/s and 3 bar-80 bar, respectively, during the burst tests. A burst criterion for inert environment, which assumes that deformation is controlled by steady state creep, has been developed using the empirical burst parameters. The burst criterion has been validated with experimental data reported in literature and the prediction of burst parameters is in a fairly good agreement with the experimental data. The burst criterion model reveals that increasing the heating rate increases the burst temperature. However, at higher heating rates, burst strain is decreased considerably and an early rupture of the claddings without undergoing considerable ballooning is observed. It is also found that the degree of anisotropy has significant influence on the burst temperature and burst strain. With increasing degree of anisotropy, the burst temperature for claddings increases but there is a decrease in the burst strain. The effect of anisotropy in the ${\alpha}$-phase is carried over to ${\alpha}+{\beta}$-phase and its effect on the burst strain in the ${\alpha}+{\beta}$-phase too can be observed.

• Proceedings of the KSME Conference
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• 2007.05a
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• pp.1807-1812
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• 2007

A bulge testing system was developed to measure mechanical properties of thin film materials. A bulge pressure test system for pressurizing the bulge window of the film and a micro out-of-plane ESPI(Electronic Speckle Pattern Interferometric) system for measuring deflection of the film were included in the testing system developed. For the out-of-plane ESPI system, whole field speckle fringe pattern, corresponding to the out-of-plane deflection of the bulged film, was 3-dimensionally visualized using 4-bucket phase shifting algorithm and least square phase unwrapping algorithm. The bulge pressure for loading and unloading was controlled at a constant rate. From the pressure-deflection curve measured by this testing system, ain-plane stress-strain curve could be determined. In this study, elastic modulus of an electrolytic copper film 18 ${\mu}m$ was determined. The modulus was calculated from determining the plain-strain biaxial elastic modulus at the respective unloading slopes of the stress-strain curve and for the Poisson's ratio of 0.34.

• Transactions of Materials Processing
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• v.6 no.4
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• pp.338-345
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• 1997

The behaviour of alloys in the semi-solid state strongly depends on the imposed stress stage and on the morphology of the phase which can vary from dendritic to globular. To optimal net shape forging of semi-solid materials, it is important to investigate for material behaviour for variation of strain rate. Therefore, to investigate the effect of compression speed on deformation of aluminum alloy with globular microstructure, the compression test for semi-solid aluminum alloy with controlled solid fraction is perform by material test system which is attracted with furance. The behavior of semi-solid aluminum alloy were discussed for the various solid fraction and die speed. The material constants in stress-strain were are also proposed.

• Proceedings of the Korean Magnestics Society Conference
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• 2011.06a
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• pp.7-8
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• 2011

Basically, the lattice mismatch between film and substrate can make those BiFeO3(BFO) films distorted with strain structure. BFO phase can be stabilized on LaAlO3(LAO) represents the example of a multiferroic with giant axial ratio. Its crystal structure is not strictly tetragonal, but tetragonal with a slight monoclinic distortion and related to the rotation of the oxygen octahedra. In this study, we show that phases with a tetragonal-like epitaxial BFO films can indeed be ferroelectric and also can be stabilized via epitaxial growth onto LAO. Recent reports on epitaxial BFO films show that the crystal structure changes from nearly rhombohedral ("R-like") to nearly tetragonal("T-like") at strains exceeding approximately -4.5%, with the "T-like" structure being characterized by a highly enhanced c/a ratio. While both the "R-like" and the "T-like" phases are monoclinic, our detailed x-ray diffraction results reveal asymmetry change from MA and MC type, respectively. By applying additional strain or by modifying the unit cell volume of the film by substituting Ba for Bi, the monoclinic distortion in the "T-like" MC phase is reduced, i.e. the system approaches a true tetragonal symmetry. There are two different M-H loops for $Bi_{1-x}Ba_xFeO_{3-{\delta}}$(BBFO) and BFO films on SrTiO3(STO) & LAO substrates. Along with the ferroelectric characterization, these magnetic data indicate that the BFO phase stabilized on LAO represents the first example of a multiferroic with giant axial ratio. However, there is a significant difference between this phase and other predicted ferroelectrics with a giant axial ratio: its crystal structure is not strictly tetragonal, but tetragonal with a slight monoclinic distortion. Therefore, in going from bulk to highly-strained films, a phase sequence of rhombohedral(R)-to-monoclinic ["R-like" MA-to-monoclinic, "T-like" MC-to-tetragonal (T)] is observed. This sequence is otherwise seen only near morphotropic phase boundaries in lead-based solid-solution perovskites (i.e. near a compositionally induced phase instability), where it can be controlled by electric field, temperature, or composition. Our results show that this evolution can occur in a lead-free, stoichiometric material and can be induced by stress alone. Those major results are summarized as follows ; 1) Ba-doping increases the unit cell volume, 2) BBFO on LAO can be fully strained up to x=0.08 as a strain limit (Fig. 1), 3) P(E) & M(H) properties can be tuned by the variation of composition, strain, and film thickness.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1999.06a
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• pp.15-32
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• 1999

A relationship between stress and stain is very important to design a die to avoid defects of products during semi-solid forming process. Since the liquid will be of eutectic composition in alloys liquid segregation will result in significant or undesirable situation. The materials used in this experiment are A 357. A390, Al2024 alloys that is fabricated by the electro-magnetic stirring process from Pechiney in France. The compression test was performed by induction heating equipment and MTS. In order to prevent the liquid segregation these measured temperature would be useful to control of strain rate during compression test. The liquid segregation is controlled as change of the strain rate and solid fraction during the compression process, The characteristics of flow between solid and liquid phase considering liquid segregation is examined through the above experiments. In the case of medium and high volume fractions of solid the distribution of strain rate is calculated by using compression test data of semi-solid materials (SSM). The thixoforming experiments with the designed die are carried out successfully. The die filling patterns of SSM for variation of die temperature and pressing force have been investigated. The hardness of the thixoformed scroll products is evaluated in terms of the microstructure for each position.