• Title/Summary/Keyword: Step 경화

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The Study of Curing Day Reduction by Step Curing of HTPB/AP Propellant (HTPB/AP계열의 고체 추진제의 Step 경화 방법을 통한 경화일(기간) 단축)

  • Kim, Kahee;Park, Jung-Ho;Choi, Sunghan
    • Journal of the Korean Society of Propulsion Engineers
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    • v.24 no.6
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    • pp.101-107
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    • 2020
  • In this paper, step-curing, which includes the change of curing temperature on the curing process, was applied to reduce curing day of HTPB/AP based propellant. This study targets the improvement of productivity of HTPB/AP based solid rocket motor. Comparison of mechanical properties of propellant resulted in the change of normal curing condition (60℃, 5 days) to step-curing condition (60℃, 1 day / 65℃, 3 days). Post-cure test was conducted to determine the impact on the shelf life of the solid rocket motor. The aging characteristics of propellants were analyzed by measuring mechanical properties and thermal expansion factor. To step-cured propellant, accelerated aging test was performed for 12 weeks, followed by tensile test. Sm(bar) and Em(%) were higher than 8 bar and 40% each, showing excellent mechanical properties.

Low temperature plasma nitricarburizing and 2-step plasma processes of 304L austenitic stainless steels (304L 스테인리스강의 저온 플라즈마질탄화 및 2-step 플라즈마 프로세스)

  • Lee, In-Seop
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2007.11a
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    • pp.65-68
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    • 2007
  • 저온 플라즈마 기술을 이용하면 오스테나이트계 스테인리스강의 내식성과 표면경도를 동시에 증가 시킬 수 있다. 여러 가지 처리방법 중 질탄화와 2-step 공정으로 처리한 AISI304L강의 표면을 분석하였다. 처리한 모든 시편의 표면은 expanded austenite(${\gamma}_N$)이 형성되었고, 표면 경도도 모재보다 약 4배 이상 증가 하였다. 저온플라즈마 질탄화 공정의 경우 경화층의 두께가 최대 15 ${\mu}m$밖에 형성되지 않았지만 2-step공정의 경우 질탄화 공정보다 짧은 시간으로 약 2배의 경화층을 얻을 수 있었다. 두 가지 공정 모두 온도와 시간이 증가할수록 경화층의 두께가 두꺼워졌지만, 과도하게 높은 온도와 긴 공정시간은 석출물을 형성 시켰다. 석출물이 형성되지 않은 시편의 경우 내식성이 증가하였다.

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Effect of Die Attach Film Composition for 1 Step Cure Characteristics and Thermomechanical Properties (다이접착필름의 조성물이 1단계 경화특성과 열기계적 물성에 미치는 영향에 관한 연구)

  • Sung, Choonghyun
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.12
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    • pp.261-267
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    • 2020
  • The demand for faster, lighter, and thinner portable electronic devices has brought about a change in semiconductor packaging technology. In response, a stacked chip-scale package(SCSP) is used widely in the assembly industry. One of the key materials for SCSP is a die-attach film (DAF). Excellent flowability is needed for DAF for successful die attachment without voids. For DAF with high flowability, two-step curing is often required to reduce a cure crack, but one-step curing is needed to reduce the processing time. In this study, DAF composition was categorized into three groups: cure (epoxy resins), soft (rubbers), hard (phenoxy resin, silica) component. The effect of the composition on a cure crack was examined when one-step curing was applied. The die-attach void and flowability were also assessed. The cure crack decreased as the amount of hard components decreased. Die-attach voids also decreased as the amount of hard components decreased. Moreover, the decrease in cure component became important when the amount of hard component was small. The flowability was evaluated using high-temperature storage modulus and bleed-out. A decrease in the amount of hard components was critical for the low storage modulus at 100℃. An increase in cure component and a decrease in hard component were important for the high bleed-out at 120℃(BL-120).

Cure Cycle for Thick Glass/Polyester Composites (두꺼운 유리섬유/폴리에스터 복합재료를 위한 경화 사이클)

  • 김형근;오제훈;이대길
    • Composites Research
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    • v.14 no.2
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    • pp.33-42
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    • 2001
  • The cure kinetic equation fur 52-glass/polyester prepreg composites was established through DSC (differential scanning calorimetry). Using the established kinetic equation, the temperature distribution of the thick composite was calculated considering the change of heat transfer resistance due to resin impregnation of bleeder plies used. In order to reduce the overheat during cure of thick glass fiber composites, the cure cycle was modified by introducing the cooling and reheating steps. Then the thick glass composites were cured both by the conventional cycle without any cooling or reheating step and the modified cure cycle. The mechanical properties of the thick composites cured by the both cycles were tested by the short beam shear test and the Barcol hardness test, and then their results were compared.

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A multi Step Cure Process to Prevent Residual Bubbles in LED Encapsulation Silicone Resin (LED Encapsulation 실리콘의 기포잔류방지를 위한 Step 경화공정 연구)

  • Song, M.J.;Kim, H.K.;Yoon, G.S.;Kim, K.H.
    • Transactions of Materials Processing
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    • v.21 no.2
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    • pp.101-106
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    • 2012
  • Generally, rapid cure reaction of LED encapsulation silicone resin causes serious defects in cured resin products such as warpage, residual bubbles, and reduced wettablility. In order to prevent residual bubbles in silicone resin, the step cure process was examined in the present paper. Three kinds of step cure processes were applied, and bubble-free phenomenon was observed. Most of the bubbles were removed under $70^{\circ}C$, the minimum temperature for activating cure reaction. In addition, degree of cure(DOC) and temperature distribution were predicted by using FEM analysis of heat transfer. It was concluded that maintaining cure temperature which provide a DOC under 0.5~0.6 effectively reduces residual bubbles.

A Study on Wear Resistance and Surface Hardening of 3%Cr-Mo-V Steel by Two-step Gas Nitriding (3%Cr-Mo-V강의 2단 가스질화처리를 통한 표면경화 및 내마모성 연구)

  • Jung, G.B.
    • Journal of the Korean Society for Heat Treatment
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    • v.22 no.6
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    • pp.361-367
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    • 2009
  • The two-step gas nitriding was adopted to increase the depth of surface hardening in 3%Cr-Mo-V steel. The two-step gas nitriding consisted of Step I; $520^{\circ}C{\times}20\;hrs$ and Step II; $550^{\circ}{\times}70\;hrs$. The layer of two-step gas nitriding showed better uniformity and deeper nitriding layer than one-step gas-nitriding layer. The maximum surface hardness showed the value of 850 Hv. The maximum depth of nitrogen permeation showed $750\;{\mu}m$ (350 Hv). X-ray diffraction analysis showed that compound layer was mainly consisted of CrN and $\varepsilon-Fe_3N$ phases. These phases were presumed contributing to surface hardening and wear resistance. However, the corrosion resistance of gas-nitrided Cr-Mo-V steel were not improved in the solution of 1 N HCl and NaOH. Therefore, it is necessary that the continuous study for improvement of corrosion resistance hereafter.

A Study on the Development Direction of the Next-generation Smart Training Education Platform(STEP) for the Development of National Lifelong Vocational Skills (국민 평생직업능력개발을 위한 차세대 스마트직업훈련플랫폼 개발 방향에 관한 연구)

  • Kyung-Hwa Rim;Il-chan Jung;Doo-wan Lee
    • Journal of Practical Engineering Education
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    • v.15 no.1
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    • pp.143-154
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    • 2023
  • The purpose of this study is to present the role and function of Smart Training Education Platform(STEP) as a public online platform that should be aimed at for the development of customized lifelong vocational skills as the existing Occupational Skills Development Act was revised to the National Lifelong Vocational Skills Development Act. To this end, the role and function of STEP's public service was derived based on domestic public online platform service case studies and expert FGI, and an expert verification meeting was held. Based on this, implications for the role and function of STEP as a public online platform were presented.

A Study on Penetration Effect of Penetrating Hardener for Prevention of Scattering of Asbestos Building Materials (석면 건축자재의 비산 방지를 위한 침투성 경화제 침투 효과에 관한 연구)

  • Song, Tae-Hyeob;Park, Ji-Sun;Shin, Hyun-Gyoo
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.6 no.4
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    • pp.324-330
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    • 2018
  • In accordance with the amendment of the Industrial Safety and Health Act of 2007, Korea completely prohibited the import, distribution and manufacture of asbestos like Europe and Japan. Accordingly, the current problem of asbestos is the safe maintenance and disposal of asbestos construction material, the disposal of asbestos, and the final disposal of asbestos building materials. In the past, Korea used 100,000 tons of asbestos every year, and the building materials using it exceeded 1 million tons per year. These asbestos building materials continued to be used until 2006, and the Ministry predicted that these materials would continue to be maintained until 2044. When the permeable hardening agent is applied to the asbestos building material installed in the pre-pretreatment step for the harmless treatment of the asbestos waste and the dismantling is carried out, the scattering of the asbestos is suppressed in the disassembling step, detoxification treatment conditions can be improved. Therefore, permeable hardeners should be stably penetrated into asbestos building materials. In this study, it is suggested that pre - pretreatment methods for the harmlessization of waste asbestos building materials with medium density level can be presented. In order to efficiently perform pre - treatment for chemical harmlessness in the future, the mixing ratio of permeable hardener and middle water Optimization is the most important factor.

A New Algorithm for the Integration of Thermal-Elasto-Plastic Constitutive Equation (열탄소성 구성방정식 적분을 위한 새로운 알고리즘)

  • 이동욱;신효철
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.18 no.6
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    • pp.1455-1464
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    • 1994
  • A new and efficient algorithm for the integration of the thermal-elasto-plastic constitutive equation is proposed. While it falls into the category of the return mapping method, the algorithm adopts the three point approximation of plastic corrector within one time increment step. The results of its application to a von Mises-type thermal-elasto-plastic model with combined hardening and temperature-dependent material properties show that the accurate iso-error maps are obtained for both angular and radial errors. The accuracy achieved is because the predicted stress increment in a single step calculation follows the exact value closely not only at the end of the step but also through the whole path. Also, the comparison of the computational time for the new and other algorithms shows that the new one is very efficient.

Evaluation of Anisotropic Hardening Models using Two-Step Tension Tests (2단 인장 실험을 통한 이방성 경화 모델의 평가)

  • Ha, J.;Lee, M.G.;Barlat, Frederic
    • Transactions of Materials Processing
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    • v.21 no.6
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    • pp.372-377
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    • 2012
  • In this study, the plastic flow behaviors of extra deep drawing quality (EDDQ) steel subjected to non-proportional strain paths were investigated. Two-step uniaxial tension tests, in which the first step was performed in the rolling direction (RD) and the subsequent test in different directions in $15^{\circ}$ increments from the RD, were conducted. The experiments clearly showed that stress overshooting and strain hardening stagnation were the dominant features, which were captured reasonably well using a recently proposed distortional hardening model.