• 한국입자에어로졸학회지
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• 제13권3호
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• pp.133-139
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• 2017

In this paper, we proposed an emulsification method without using an emulsifier and investigated the effects of particle size distribution in fluids on dispersion stability. Surfactant-free oil in water emulsion was prepared with 1 % (w/w) of olive oil by using high speed agitation, high pressure and ultrasonic dispersion methods. The particle size, microscopic observation, and dispersion stability of each sample were evaluated and dispersion stability according to various dispersion methods was compared. As a result, the emulsion dispersed by the ultrasonic dispersion method showed the smallest particle size and uniform distribution of $0.07{\sim} 0.3{\mu}m$ and was the most stable in a 7 days stability evaluation. In the above experiment, four olive oil emulsions having different particle sizes were prepared using ultrasonic dispersion technology that was capable of producing stable emulsions. The dispersion stability of each samples with oil droplet sizes of (A) 0.1 to $0.5{\mu}m$, (B) 0.3 to $4{\mu}m$, (C) 1 to $10.5{\mu}m$ and (D) 2 to $120{\mu}m$, was observed for 7 days, and the relationship between the stability and performance was studied. Emulsion (A) with particle size less than $0.5{\mu}m$ displayed the dispersion stability showing below 5 % change in a 7 days stability evaluation. In the case of (B), (C), and (D) that had larger particle than $0.5{\mu}m$, the changes of dispersion stability were 10 %, 13 % and 35 % respectively. From these results, it was proved that dispersion stability of emulsion with uniform particle size of $0.5{\mu}m$ or less was confirmed to be very stable.

• 한국분말재료학회지
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• 제25권5호
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• pp.395-401
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• 2018

The improvement of dispersion stability for the primary polishing slurry in a CMP process is achieved to prevent defects produced by agglomeration of the slurry. The dispersion properties are analyzed according to the physical characteristics of each silica sol sample. Further, the difference in the dispersion stability is confirmed as the surfactant content. The dispersibility results measured by Zeta potential suggest that the dispersion properties depend on the content and size of the abrasive in the primary polishing slurry. Moreover, the optimum ratio for high dispersion stability is confirmed as the addition content of the surfactant. Based on the aforementioned results, the long-term stability of each slurry is analyzed. Turbiscan analysis demonstrates that the agglomeration occurs depending on the increasing amount of surfactant. As a result, we demonstrate that the increased particle size and the decreased content of silica improve the dispersion stability and long-term stability.

• Journal of the Korean Statistical Society
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• 제32권4호
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• pp.337-357
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• 2003

This paper introduces new measures for the stability of slope estimation on the second order response surface at a point and on a sphere. As a measure of point stability of slope estimation, we suggest a point dispersion measure of slope variances over all directions at a point. A spherical dispersion measure is also proposed as a measure of spherical stability of slope estimation on each sphere. Some designs are studied to explore the usefulness of the proposed measures. Using the point dispersion measure, another concept of slope rotatability called equally-stable slope rotatability is proposed as a useful property of response surface designs. We provide a set of conditions for a design to have equally-stable slope rotatability.

• 한국염색가공학회지
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• 제15권5호
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• pp.321-326
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• 2003

In order for disperse dye based ink to be fitted with the critical requirements of ink jet printing, this study was undertaken to investigate the effects of 6 different dispersants on the milling efficiency of insoluble dye particles and dispersion stability of the final ink. It was found that a polystyrene dispersant with high molecular weight exerted relatively better dispersion stability which may be associated with its steric stabilization effect in the ink solution.

• 한국전자파학회논문지
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• 제22권4호
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• pp.407-415
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• 2011

본 논문에서는 등방성(isotropic) 특성과 작은 분산 오차(low dispersion error)를 갖는 3차원 등방성 시간 영역 유한 차분법(ID-FDTD: Isotropic Dispersion Finite Difference Time Domain) 방법의 stability condition과 광대역 해석 특성에 대해 논의하였다. 3차원 ID-FDTD 방법은 기존의 Yee FDTD 방법의 비등방성 특성과 큰 분산 오차를 개선하기 위해 제안되었다. 기존 연구에서는 3차원 ID-FDTD 방법의 stability condition을 수치적으로 계산하였지만, 이에 대한 검증이 충분히 이뤄지지 않은 상태이다. 이에 본 논문에서는 단일 주파수와 광대역 주파수 신호를 입력원으로 한 모의 실험 환경에서 3차원 ID-FDTD 방법의 stability condition 검증을 수행하였다. 또한 광대역 특성에 대해 3차원 ID-FDTD 방법과 유사한 알고리즘들을 비교 분석해 해보았고, 마지막으로 3D ID-FDTD을 적용하여 대형 크기 구 모델에 대해 radar cross section(RCS) 해석을 수행함으로써, 실질적 해석을 통한 알고리즘 검증 및 분석을 마무리 하였다.

• 한국세라믹학회지
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• 제52권6호
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• pp.497-501
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• 2015

Inkjet printing is a widespread technology, offering advantages such as high-quality decoration, a continuous process, and the accurate direct reproduction of patterns or pictures. In inkjet printing technology, the dispersion stability of ceramic ink is one of the most important factors. In this study, the dispersion stability of blue $CoAl_2O_4$ ink for ceramic inkjet printing is systematically investigated. Blue $CoAl_2O_4$ pigment was synthesized by a solid-state reaction and then milled to less than 300nm in size. In order to investigate the influence of the viscosity on the dispersion stability, two types of $CoAl_2O_4$ ceramic inks (termed here Blue L and Blue H) were prepared using different volume ratios of ethylene glycol and ethanol. The Blue L and Blue H ink solutions contained cetyltrimethylammonium bromide(CTAB) as a dispersive agent. The viscosity, surface tension and jetting stability of the $CoAl_2O_4$ ceramic inks were analyzed using a rheometer, a surface tension meter and a dropwatcher. The dispersion stability of the $CoAl_2O_4$ ceramic ink was investigated by a multiple light-scattering method. Blue H, a ceramic ink with higher viscosity, showed much better dispersion stability than the Blue L ceramic ink.

• 한국분말재료학회지
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• 제20권6호
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• pp.479-486
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• 2013

In the present work, physicochemical treatments were introduced for de-aggregation and stable dispersion of detonation nanodiamonds (DND) in polar solvents. The DNDs in water exhibited a particle size of 138 nm and high dispersion stability without particular treatment. However, the DNDs in ethanol were severely aggregated to several micrometers in size and showed poor dispersion stability with time. To break down aggregates of DNDs and enhance the dispersion stability of them in ethanol, mechanical force and chemical surfactant were introduced as functions of zirconia ball size, kind of surfactant and amount of surfactant added. From the analyses of average particle size and Turbiscan results, it was suggested that the size of DNDs in ethanol can be reduced by only mechanical force; however, the DNDs were re-aggregated due to high surface activity. The long-term dispersion stability can be achieved by applying mechanical force to break down the aggregates of DNDs and by preventing re-aggregation of them using proper surfactant.

• 한국추진공학회:학술대회논문집
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• 한국추진공학회 2009년도 춘계학술대회 논문집
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• pp.163-166
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• 2009

알루미늄슬러리 연료 제조 시 알루미늄의 분산안정성에 미치는 공정변수의 영향을 조사하였다. 알루미늄슬러리연료의 분산안정성은 Laser의 산란 현상을 이용하여 물질의 분산 안정성을 파악하는 Turbiscan을 이용하여 확인하였다. 여러 종류의 첨가제 적용시 시간 경과에 따른 입자 크기 및 농도 변화를 측정한 결과, TPAB (Tetrapropyl ammonium bromide) 사용시 다른 첨가제보다 좋은 결과를 나타내었다.

• 한국추진공학회지
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• 제13권3호
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• pp.34-40
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• 2009

카본슬러리 연료 제조 시 카본의 분산안정성에 미치는 공정변수의 영향을 조사하였다. 카본슬러리연료의 분산안정성은 위치별 입도분석, 카본함량 분석, 그리고 원심분리 후 분산상태 관찰을 통해서 측정하였다. 여러 종류의 첨가제를 적용한 결과, NB463S84 사용시 분산성과 분산안정성이 가장 우수한 것을 알 수 있었다. NB463S84와 비슷한 작용기를 가지는 PIBSI를 합성하였으며, 이를 카본슬러리 연료에 적용하여 유사한 분산안정도를 얻었다. 끝으로 g 규모에서 얻은 제조 조건을 kg 규모 제조에 적용하여 카본슬러리 연료의 실용화 가능성을 확인하였다.

• 대한기계학회논문집B
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• 제23권2호
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• pp.218-225
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• 1999

Flow visualization study has been conducted to simulate the turbulent dispersion behavior of a crossflow jet physically under the conditions of various thermal stratification in a wind tunnel. A smoke jet with the constant ratio of the jet to freestream velocity is injected normally to the cross flow of the thermally stratified wind tunnel(TSWT) for flow visualization. The typical natures of the smoke dispersion under different thermal stratifications such as neutral, weakly stable, strongly stable, weakly unstable, strongly unstable and inversion layer are successfully reproduced in the TSWT. The Instantaneous velocity and temperature fluctuations are measured by using a cold and hot-wire combination probe. The time averaged dispersion behaviors, the centerline trajectories, the spreading angles and the virtual origins of the cross jet are deduced from the edge detected images with respect to the stability parameter. All the general characteristics of the turbulent dispersion behavior reveal that the definitely different dispersion mechanisms are inherent in both stable and unstable conditions. It is conjectured that the turbulent statistics obtained in the various stability conditions quantitatively demonstrate the vertical scalar flux plays a key role in the turbulent dispersion behavior.