• Title/Summary/Keyword: Solution reduction method

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Coating of Cobalt Over Tungsten Carbide Powder by Wet Chemical Reduction Method

  • Hong, Hyun-Seon;Yoon, Jin-Ho
    • Journal of Powder Materials
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    • v.21 no.2
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    • pp.93-96
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    • 2014
  • Cobalt coated tungsten carbide-cobalt composite powder has been prepared through wet chemical reduction method. The cobalt sulfate solution was converted to the cobalt chloride then the cobalt hydroxide. The tungsten carbide powders were added in to the cobalt hydroxide, the cobalt hydroxide was reduced and coated over tungsten carbide powder using hypo-phosphorous acid. Both the cobalt and the tungsten carbide phase peaks were evident in the tungsten carbide-cobalt composite powder by X-ray diffraction. The average particle size measured via scanning electron microscope, particle size analysis was around 380 nm and the thickness of coated cobalt was determined to be 30~40 nm by transmission electron microscopy.

Study on Robustness of Incomplete Cholesky Factorization using Preconditioning for Conjugate Gradient Method (불완전분해법을 전처리로 하는 공액구배법의 안정화에 대한 연구)

  • Ko, Jin-Hwan;Lee, Byung-Chai
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.27 no.2
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    • pp.276-284
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    • 2003
  • The preconditioned conjugate gradient method is an efficient iterative solution scheme for large size finite element problems. As preconditioning method, we choose an incomplete Cholesky factorization which has efficiency and easiness in implementation in this paper. The incomplete Cholesky factorization mettled sometimes leads to breakdown of the computational procedure that means pivots in the matrix become minus during factorization. So, it is inevitable that a reduction process fur stabilizing and this process will guarantee robustness of the algorithm at the cost of a little computation. Recently incomplete factorization that enhances robustness through increasing diagonal dominancy instead of reduction process has been developed. This method has better efficiency for the problem that has rotational degree of freedom but is sensitive to parameters and the breakdown can be occurred occasionally. Therefore, this paper presents new method that guarantees robustness for this method. Numerical experiment shows that the present method guarantees robustness without further efficiency loss.

Automated static condensation method for local analysis of large finite element models

  • Boo, Seung-Hwan;Oh, Min-Han
    • Structural Engineering and Mechanics
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    • v.61 no.6
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    • pp.807-816
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    • 2017
  • In this paper, we introduce an efficient new model reduction method, named the automated static condensation method, which is developed for the local analysis of large finite element models. The algebraic multilevel substructuring procedure is modified appropriately, and then applied to the original static condensation method. The retained substructure, which is the local finite element model to be analyzed, is defined, and then the remaining part of the global model is automatically partitioned into many omitted substructures in an algebraic perspective. For an efficient condensation procedure, a substructural tree diagram and substructural sets are established. Using these, the omitted substructures are sequentially condensed into the retained substructure to construct the reduced model. Using several large practical engineering problems, the performance of the proposed method is demonstrated in terms of its solution accuracy and computational efficiency, compared to the original static condensation method and the superelement technique.

A Hybrid ON/OFF Method for Fast Solution of Electromagnetic Inverse Problems Based on Topological Sensitivity

  • Kim, Dong-Hun;Byun, Jin-Kyu
    • Journal of Magnetics
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    • v.16 no.3
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    • pp.240-245
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    • 2011
  • A new hybrid ON/OFF method is presented for the fast solution of electromagnetic inverse problems in high frequency domains. The proposed method utilizes both topological sensitivity (TS) and material sensitivity (MS) to update material properties in unit design cells. MS provides smooth design space and stable convergence, while TS enables sudden changes of material distribution when MS slows down. This combination of two sensitivities enables a reduction in total computation time. The TS and MS analyses are based on a variational approach and an adjoint variable method (AVM), which permits direct calculation of both sensitivity values from field solutions of the primary and adjoint systems. Investigation of the formulations of TS and MS reveals that they have similar forms, and implementation of the hybrid ON/OFF method that uses both sensitivities can be achieved by one optimization module. The proposed method is applied to dielectric material reconstruction problems, and the results show the feasibility and effectiveness of the method.

Experimental Study of Friction Drag Reduction in Turbulent Flow with Polymer and Microbubble Injection (폴리머와 미소기포 주입에 의한 난류마찰저항 감소에 대한 연구)

  • Kim D.S.;Kim W.J.;Kim H.T
    • Proceedings of the KSME Conference
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    • 2002.08a
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    • pp.483-486
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    • 2002
  • Injection of microbubbles and/or polymer solution has been known to be a promising method for the reduction of frictional drag of water-borne vehicles. Naval Architects have been interested in friction drag reduction technology, since the friction drag of a commercial ship can be over $70{\%}$ of total resistance. The reduction of friction drag is also important for autonomous underwater vehicles and naval submarines to improve their durability and survivability In this study two sets of experiments were carried out for the friction drag reduction of 2-D channel wall and flat plate in the circulating water channels in Chungnam National University. Preliminary results from the experiments are presented and discussed.

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Electrocatalytic Reduction of Molecular Oxygen at Poly(1,8-diaminonaphthalene) and Poly(Co(II)-(1,8-diaminonaphthalene)) Coated Electrodes

  • Park, Hyun;Kwon, Tae-guen;Park, Deog-Su;Shim, Yoon-Bo
    • Bulletin of the Korean Chemical Society
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    • v.27 no.11
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    • pp.1763-1768
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    • 2006
  • The application of poly(Co(II)-(1,8-diaminonaphthalene))(poly(Co-DAN)) and poly(1,8-diaminonaphthalene) (Poly(1,8-DAN)) to the electrocatalytic reduction of molecular oxygen was investigated, which were electrochemically grown by the potential cycling method on the glassy carbon electrodes. The reduction of oxygen at the polymer and its metal complex polymer coated electrodes were irreversible and diffusion controlled. The Poly(1,8-DAN) and Poly(Co-DAN) films revealed the potential shifts for the oxygen reduction to 30 mV and 110 mV, respectively, in an aqueous solution, compared with that of the bare electrode. Hydrodynamic voltammetry with a rotating ring-disk electrode showed that Poly(1,8-DAN) and Poly(Co-DAN) coated electrodes converted respectively 84% and 22% of $O_2$ to $H_2O$ via a four electron reduction pathway.

A Study on Model Reduction for Effective Analysis of Structure (구조물의 효율적인 해석을 위한 모델 축소기법 연구)

  • 박영창;황재혁;오화석
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2001.11b
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    • pp.1370-1375
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    • 2001
  • Substructure coupling or component mode synthesis may be employed in the solution of dynamic problems for structure. The model is partitioned into several subdomains. and a generalized Craig-Bampton representation is derived. In this paper the mode sets(normal modes. constraint modes) have been employed for model reduction. A generalized model reduction procedure has been described. Those reduction methods which adapt constraint modes have been described in detail. As examples. a flexible structure and a 10 DOF damped system are analyzed. Comparison with a conventional reduction method based on a complete model has been made via eigenpairs and dynamic responses.

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Performance Enhancement of Speech Intelligibility in Communication System Using Combined Beamforming (directional microphone) and Speech Filtering Method (방향성 마이크로폰과 음성 필터링을 이용한 통신 시스템의 음성 인지도 향상)

  • Shin, Min-Cheol;Wang, Se-Myung
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2005.05a
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    • pp.334-337
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    • 2005
  • The speech intelligibility is one of the most important factors in communication system. The speech intelligibility is related with speech to noise ratio. To enhance the speech to noise ratio, background noise reduction techniques are being developed. As a part of solution to noise reduction, this paper introduces directional microphone using beamforming method and speech filtering method. The directional microphone narrows the spatial range of processing signal into the direction of the target speech signal. The noise signal located in the same direction with speech still remains in the processing signal. To sort this mixed signal into speech and noise, as a following step, a speech-filtering method is applied to pick up only the speech signal from the processed signal. The speech filtering method is based on the characteristics of speech signal itself. The combined directional microphone and speech filtering method gives enhanced performance to speech intelligibility in communication system.

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PROPER ORTHOGONAL DECOMPOSITION OF DISCONTINUOUS SOLUTIONS WITH THE GEGENBAUER POST-PROCESSING

  • SHIN, BYEONG-CHUN;JUNG, JAE-HUN
    • Journal of the Korean Society for Industrial and Applied Mathematics
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    • v.23 no.4
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    • pp.301-327
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    • 2019
  • The proper orthogonal decomposition (POD) method for time-dependent problems significantly reduces the computational time as it reduces the original problem to the lower dimensional space. Even a higher degree of reduction can be reached if the solution is smooth in space and time. However, if the solution is discontinuous and the discontinuity is parameterized e.g. with time, the POD approximations are not accurate in the reduced space due to the lack of ability to represent the discontinuous solution as a finite linear combination of smooth bases. In this paper, we propose to post-process the sample solutions and re-initialize the POD approximations to deal with discontinuous solutions and provide accurate approximations while the computational time is reduced. For the post-processing, we use the Gegenbauer reconstruction method. Then we regularize the Gegenbauer reconstruction for the construction of POD bases. With the constructed POD bases, we solve the given PDE in the reduced space. For the POD approximation, we re-initialize the POD solution so that the post-processed sample solution is used as the initial condition at each sampling time. As a proof-of-concept, we solve both one-dimensional linear and nonlinear hyperbolic problems. The numerical results show that the proposed method is efficient and accurate.

Sn02 Two-dimensional Nanostructures Prepared by Solution Reduction Method and Their Gas Sensing Characteristics (용액환원법에 의한 Sn02 2차원 나노구조의 합성과 가스 감응 특성)

  • Park, Hong-Chul;Kim, Hae-Ryong;Lee, Jong-Heun
    • Korean Journal of Materials Research
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    • v.18 no.8
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    • pp.438-443
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    • 2008
  • SnO nanosheets were prepared at room temperature through a reaction between an aqueous solution of $SnCl_2$, $N_2F_4$, and NaOH and were converted into $SnO_2$ nanosheets without a morphological change. The SnO nanosheets were formed through a dissolution-recrystallization mechanism. Uniform and well-dispersed SnO nanosheets with the round-shape morphology were attained when the solution was treated by ultrasonic sound immediately after the addition of NaOH. The $SnO_2$ nanosheets prepared by means of solution reduction under the ultrasonic treatment, and subsequent oxidation at $600^{\circ}C$ showed a high level of gas sensitivity to $C_2H_5OH$ and $CH_3COCH_3$.