• Title/Summary/Keyword: Solid-Liquid System

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Solid-Liquid Mass Transfer in Gas-Solid-Liquid 3-Phase System Agitated Vessel (기 - 액 - 고 3상계 교반조내의 고-액간 물질이동)

  • Lee, Young Sei;Kato, Yoshihito;Suzuki, Junichiro
    • Applied Chemistry for Engineering
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    • v.17 no.5
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    • pp.509-516
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    • 2006
  • The solid-liquid mass transfer coefficients $k_L$ in a gas-liquid-solid three phases agitated vessel were measured with conventional impellers (e.g. Rushton turbine, paddle, and propeller). For the conventional impellers the rotational speed for the complete suspension $N_{js}$ changes with the impeller height and gas flow rate. Mass transfer coefficient of the Rushton turbin impeller, for which the particle suspension was independent of the aeration, is correlated only with Pgv. Mass transfer coefficients $k_L$ for the Rushton turbine, paddle and propeller impellers were affected by the impeller position.

Multisample Extraction system for Solid Phase Extraction of Dissolved Organic Compounds from Sea Water (해수로부터 용존 윤기물의 Solid Phase Extraction을 위한 다수 시료 처리 장치)

  • Cho Ki Woong;Jung Kyungwha;Shin Jongheon;Kim Suk Hyun;Hong Gi-Hoon
    • Journal of the Korean Society for Marine Environment & Energy
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    • v.3 no.3
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    • pp.34-40
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    • 2000
  • A multisample extraction device was newly designed for efficient extraction of dissolved lipophillic organic compounds from sea water sample. This device allowed extraction of organic compounds from up to 96 sample at a time using 96 multifolder on the principle of solid phase extraction with commercially available octadecyl silane (ODS) cartridges. The recovery yield of the new divice was higher than 90 % while that of conventional liquid-liquid extraction process are only 60 - 70 %. The amount of solvent required for the new device could be reduced to less than 20㎖ per 1ℓ of sample while 1 - 2 ℓ of solvent were used in the conventional liquid-liquid extraction process. The usefulness of this novel method was demonstrated with sea water samples collected from Yellow sea, and the qualitative and quantitative analyses results of the dissolved hydrocarbon showed this method was superior to that of conventional liquid-liquid extraction process in efficiency and reliability.

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TRANSIENT SIMULATION OF SOLID PARTICLE DISTRIBUTION WITH BAFFLES DESIGN PARAMETERS IN A STIRRED TANK (배플 형상에 따른 교반기 내부 고체입자 분포의 비정상상태 해석)

  • Kim, Chi-Gyeom;Won, Chan-Shik;Hur, Nahm-Keon
    • 한국전산유체공학회:학술대회논문집
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    • 2008.03a
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    • pp.171-175
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    • 2008
  • In the present study, a numerical simulations are investigated in a stirred solid/liquid system by using Eulerian multi-phase model. The transient flow field of liquid phase and distribution of solid particles are predicted in stirred tanks consisting of 4-pitched paddles impeller and baffles. The effects of number and width of baffles on the mixing time and the quality of solid suspension in a stirred tank are presented numerically. The result shows that the mixing time decreases as the width and number of baffles increase.

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TRANSIENT SIMULATION OF SOLID PARTICLE DISTRIBUTION WITH VARIOUS DESIGN PARAMETERS OF THE BAFFLE IN A STIRRED TANK (배플 형상에 따른 교반기 내부 고체입자 분포의 비정상상태 해석)

  • Kim, Chi-Gyeom;Lee, Seung-Jae;Won, Chan-Shik;Hur, Nahm-Keon
    • Journal of computational fluids engineering
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    • v.14 no.4
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    • pp.1-6
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    • 2009
  • In the present study, numerical simulations were performed in a stirred solid/liquid system by using Eulerian multi-phase model. The transient flow field of liquid and distribution of solid particles were predicted in the stirred tank with pitched paddle impeller and baffles. The Frozen rotor method is adopted to consider the rotating motion of the impeller. The effects of number and width of baffles on the mixing time and the quality of solid suspension in the stirred tank are presented numerically. The result shows that the mixing time decreases as the width and number of baffles increase. The present numerical methodology can be applied to optimizing mixing condition of industrial mixer.

An Economic Analysis on Slush Hydrogen Containing Liquid and Solid Phase for Long-Term and Large-Scale Storage (장주기/대용량 수소저장을 위한 액체/고체기반 Slush 수소의 저장 비용 분석)

  • PARK, SUNGHO;LEE, CHANGHYEONG;RYU, JUYEOL;HWANG, SEONGHYEON
    • Transactions of the Korean hydrogen and new energy society
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    • v.33 no.3
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    • pp.247-254
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    • 2022
  • Slush hydrogen containing liquid and solid hydrogen is expected to achieve zero boil-off by suppressing boil-off gas because heat of fusion for solid absorbe the heat ingress from atmosphere. In this paper, quantitative analysis on storage cost considering specific energy consumption between 1,000 m3 class liquid hydrogen storage system with re-liquefaction and slush hydrogen storage system during equivalent zero boil off period. Even though approximately 50% of total storage capacity should be converted into solid phase during the initial cargo bunkering, total energy consumption to convert into slush hydrogen is relatively 25% less than re-liquefaction energy for boil off hydrogen during zero boil off period. That's because energy consumption of slush phase change take up only 1.8% of liquefaction energy. moreover, annual revenue requirement including CAPEX, OPEX and electric cost for slush hydrogen storage could be more reduced approximately 32.5% than those of liquid hydrogen storage and specific energy storage cost ($/kg-H2) could also be lowered by about 41.7% compared with liquid hydrogen storage.

Measurements of Transient Mixing Concentrations between Solid Powder and Liquid Fuel (고체분말/액체연료의 과도혼합 농도 분포 측정)

  • Doh, Deoghee;Yum, Jooho;Cho, Gyeongrae;Min, Seongki;Kim, Myungho;Ryu, Gyongwon;Yoo, Namhyun
    • Transactions of the Korean hydrogen and new energy society
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    • v.23 no.6
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    • pp.678-687
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    • 2012
  • Concentration fields of solid powder in a liquid fuel were quantitatively measured by a visualization technique. The measurement system consists of a camcoder and three LCD monitors. The solid powder (glass powder) were filled in a head tank which was installed over a main mixing tank ($D{\times}H$, $310{\times}370mm$). The main mixing tank was filled with JetA1 fuel oil. With a sudden opening of the upper tank by pressurized nitrogen gas with 1.9 bar, the solid powder were poured into the JetA1 oil. An impeller type agitator was being rotated in the mixing with 700 rpm for the enhancements of mixing. Uniform visualization for the mixing flow field was made by the light from the three LCD monitors, and the visualized images were captured by the camcoder. The color images captured by the camcoder The color information of the captured images was decoded into three principle colors R, G, and B to get quantitattive relations between the concentrations of the solid powder and the colors. To get better fitting for the strong non-linearity between the concentration and the color, a neural network which has strong fitting performances was used. Analyses on the transient mixing of the solid powders were quantitatively made.

Reflection and refraction of magneto-thermoelastic plane wave at the pre-stressed liquid-solid interface in generalized thermoelasticity under three theories

  • Kakar, Rajneesh;Kakar, Shikha
    • Earthquakes and Structures
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    • v.9 no.3
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    • pp.577-601
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    • 2015
  • The thermomagnetic effect on plane wave propagation at the liquid-solid interface with nonclassical thermoelasticity is investigated. It is assumed that liquid-solid half-space is under initial stress. Numerical computations are performed for the developed amplitude ratios of P, SV and thermal waves under Cattaneo-Lord-Shulman theory, Green-Lindsay theory and classical thermoelasticity. The system of developed equations is solved by the application of the MATLAB software at different angles of incidence for Green and Lindsay model. The effect of initial stress and magnetic field in the lower half-space are discussed and comparison is made in LS, GL and CT models of thermoelasticity. In the absence of magnetic field, the obtained results are in agreement with the same results obtained by the relevant authors. This study would be useful for magneto-thermoelastic acoustic device field.

Unsteady Analysis of the Conduction-Dominated Three-Dimensional Close-Contact Melting (열전도가 주도적인 삼차원 접촉융해에 대한 비정상 해석)

  • Yoo, Hoseon
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.23 no.8
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    • pp.945-956
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    • 1999
  • This work reports a set of approximate analytical solutions describing the initial transient process of close-contact melting between a rectangular parallelepiped solid and a flat plate on which either constant temperature or constant heat flux is imposed. Not only relative motion of the solid block tangential to the heating plate, but also the density difference between the solid and liquid phase is incorporated in the model. The thin film approximation reduces the force balance between the solid weight and liquid pressure, and the energy balance at the melting front into a simultaneous ordinary differential equation system. The normalized model equations admit compactly expressed analytical solutions which include the already approved two-dimensional solutions as a subset. In particular, the normalized liquid film thickness is independent of all pertinent parameters, thereby facilitating to define the transition period of close-contact melting. A unique behavior of the solid descending velocity due to the density difference is also resolved by the present solution. A new geometric function which alone represents the three-dimensional effect is introduced, and its properties are clarified. One of the representative results is that heat transfer is at least enhanced at the expense of the increase in friction as the cross-sectional shape deviates from the square under the same contact area.

Fabrication and Evaluation of Colloidal Silica Containing Powders for Solid Self-emulsifying Drug Delivery System of Poorly Water Soluble Rivaroxaban (난용성 리바록사반 약물의 자가 유화 시스템 분말 제조를 위한 콜로이드 실리카 함유 분말의 제조 및 평가)

  • Sung Giu Jin
    • Journal of Powder Materials
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    • v.30 no.4
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    • pp.305-309
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    • 2023
  • This study aims to prepare a colloidal silica-containing powder to enhance the solubility and dissolution rate of rivaroxaban using a self-nanoemulsifying drug delivery system (SNEDDS). We investigate the impact of colloidal silica on a nanoemulsion system for preparing powdered SNEDDS. The liquid SNEDDS comprises 30/20/50 (w/w/w) Peceol/Cremophor RH40/Tween 80, which results in the formation of the smallest droplets. Three powdered SNEDDS formulations are prepared by suspending the liquid SNEDDS formulation using colloidal silica and spray drying. The powdered SNEDDS prepared with liquid SNEDDS and colloidal silica at a ratio of 1/0.5 (w/w) exhibits the highest water solubility (0.94 ± 0.62 vs. 26.70 ± 1.81 ㎍/mL) and dissolution rate (38.4 ± 3.6 vs. 85.5 ± 3.4%, 45 min) when compared to the drug alone. Morphologically, the liquid SNEDDS is adsorbed onto colloidal silica and forms smaller particles. In conclusion, an SNEDDS containing rivaroxaban, prepared using colloidal silica, facilitates the creation of a nanoemulsion and enhances the water solubility of rivaroxaban. Accordingly, this technology holds significant potential for commercialization.

The Basic Insulation Characteristics of Solid-Nitrogen for Cryocooling of HTS Systems (고온초전도 시스템 냉각용 고화질소의 기초 절연 특성)

  • Choi, Jae-Hyeong;Choi, Jin-Wook;Lee, Hai-Gun;Song, Jung-Bin;Kim, Hae-Jong;Seong, Ki-Chul;Kim, Sang-Hyun
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.58 no.1
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    • pp.132-136
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    • 2009
  • Recently, for improvement of the magnetic field of high temperature superconductor (HTS) apparatus, many studies investigating on operating in the range of $20{\sim}65\;K$ with liquid helium or the conducting method using cryocooler are actively reviewed. Also, the cooling method using solid nitrogen as cryogen is being suggested. Since the nitrogen has very large specific heat in solid state, it is expected that it can be operated for a long time without a continuous supply of cooling energy. However, there are still insufficient data on the characteristics of solid nitrogen such as thermodynamic properties and liquid-solid phase change. Especially, there was almost no study done on the electrical insulation properties of solid nitrogen so far. In this study, solid nitrogen to find the electrical characteristics was made by using cryocooler and cryostat, and investigated the flashover discharge and breakdown. The results of this study will be useful as a basic data for electrical insulation design of the HTS system using solid nitrogen as cryogen.