• 한국진공학회:학술대회논문집
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• 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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• pp.149-149
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• 2016

Ceramic is widely known material due to its outstanding mechanical property. Besides, Zirconia(ZrO2) has a low thermal conductivity so it is advantage in a heat insulation. Because of these superior properties, ZrO2 is attracted to many fields using ultra high temperature for example vehicle engines, aerospace industry, turbine, nuclear system and so on. However brittle fracture is a disadvantage of the ZrO2. In order to overcome this problem, we can make the ceramic materials to the forms of ceramic nanoparticles, ceramic nanowhiskers and these forms can be used to an agent of composite materials. In this work, we selected Au catalyzed Vapor-Liquid-Solid mechanism to synthesize ZrO2 nanowhiskers. The ZrO2 whiskers are grown through Hot-wall Chemical Vapor Deposition(Hot wall CVD) using ZrCl4 as a powder source and Au film as a catalyst. This Hot wall CVD method is known to comparatively cost effective. The synthesis condition is a temperature of $1100^{\circ}C$, a pressure of 760torr(1atm) and carrier gas(Ar) flow of 500sccm. To observe the morphology of ZrO2 scanning electron microscopy is used and to identify the crystal structure x-ray diffraction is used.

• 한국결정성장학회지
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• 제23권6호
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• pp.265-271
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• 2013

Czochralski(CZ) 성장공정은 LED 기판용 고품질의 사파이어 단결정을 성장시키기 위한 중요한 기술 중 하나이다. 본 연구에서는 300 mm 길이의 사파이어 단결정 위한 유도 가열방식의 CZ 성장공정을 FEM으로 수치적 해석하였다. 또한 도가니의 형상 및 상부 단열재 보강 등 hot zone 구조를 변경하고, 결정의 온도 변화를 분석하였다. 본 연구의 결과, 고-액 계면의 높이는 성장 속도의 균형이 이루어져 초기에 80 mm 부터 중기 이후 40 mm 정도까지 감소하였다. 또한 CZ 성장로의 최적 입력 전력은 도가니 형상 변경 및 상부 단열재 보강에 의한 보상효과로 기존 300 mm 용 CZ 성장로 조건과 유사하다. 그리고 Hot zone 구조를 변경한 CZ 성장로를 이용해 성장시킨 결정의 온도는 기존 보다 약 10 K 정도 상승 되는 것으로 분석되었다. 본 연구에서 도출된 결과를 CZ 성장공정에 적용하여 300 mm 길이를 갖는 c-축 사파이어 단결정을 성공적으로 성장시킬 수 있었고, 단결정 성장공정에 대한 시뮬레이션 분석기법의 타당성 및 유용성을 확인하였다.

• KIEAE Journal
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• 제8권4호
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• pp.63-69
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• 2008

The thesis is a comparative analysis of Infill Technologies between Korea's long-life Mock-up House, a study driven by 'Durability and Flexibility of Long-life Housing Technology Development' of R&D, and Japan's KSI experimental house, the major example of Japan's long-llfe housing. In terms of the domestic Mock-up House, a system of building the floor first was applied. The floor material of each housing unit required a development of dry heating component that is partially substitutable in order to avoid conflict with the finishing. Also, a development of a floor system that can counteract against the construction inaccuracy was required. In the Case of an outer wall, need to make the wall with the chassis. In the case of ceiling, need to develop the double ceiling system which is good for sound insulation. Also, in comparison to KSI experimental house in Japan, it would require to develop a wiring system of the ceiling which can react to the movement of the wall. Especially, to assure the flexible nature of an internal wall, it would desperately require the research and development of the products related to components and flexible system of mechanical/electrical/communication parts as well as supporting institutionalized system for this development. Furthermore, for KSI experimental house in Japan, it would be necessary to formulate a construction manual as well as a systematic and practical planning guide to invent a new interface rule which will secure simplicity of assembling, dismantling, installation and replacement of architectural components for which research development is quite insignificant at the moment. This effort will have to continue to give a solid direction for better application of such reference manual during construction and development of long life span apartment by public sector as well as private corporations.

• International Journal of Precision Engineering and Manufacturing
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• 제9권1호
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• pp.39-46
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• 2008

The end plates of fuel cell assemblies are used to fasten the inner stacks, reduce the contact pressure, and provide a seal between Membrane-Electrode Assemblies (MEAs). They therefore require sufficient mechanical strength to withstand the tightening pressure, light weight to obtain high energy densities, and stable chemical/electrochemical properties, as well as provide electrical insulation. The design criteria for end plates can be divided into three parts: the material, connecting method, and shape. In the past, end plates were made from metals such as aluminum, titanium, and stainless steel alloys, but due to corrosion problems, thermal losses, and their excessive weight, alternative materials such as plastics have been considered. Composite materials consisting of combinations of two or more materials have also been proposed for end plates to enhance their mechanical strength. Tie-rods have been traditionally used to connect end plates, but since the number of connecting parts has increased, resulting in assembly difficulties, new types of connectors have been contemplated. Ideas such as adding reinforcement or flat plates, or using bands or boxes to replace tie-rods have been proposed. Typical end plates are rectangular or cylindrical solid plates. To minimize the weight and provide a uniform pressure distribution, new concepts such as ribbed-, bomb-, or bow-shaped plates have been considered. Even though end plates were not an issue in fuel cell system designs in the past, they now provide a great challenge for designers. Changes in the materials, connecting methods, and shapes of an end plate allow us to achieve lighter, stronger end plates, resulting in more efficient fuel cell systems.

• KEPCO Journal on Electric Power and Energy
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• 제6권4호
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• pp.447-454
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• 2020

Since SF₆ gas was discovered in the early 1900s, it has been widely used as an insulation material for electrical equipment. While various indicators have been developed to diagnose oil-immersed transformers, there are still insufficient indicators for the diagnosis of gas-insulated transformers. When necessary, chemical diagnostic methods can be used for gas-insulated transformers. However, the field suitability and accuracy of those methods for transformer diagnosis have not been verified. In addition, since various types of decomposition gases are generated therein, it is also necessary to establish appropriate analysis methods to cover the variety of gases. In this study, a gas-insulated transformer was diagnosed through the analysis of decomposition gases. Reliability assessments of both simple analysis methods suitable for on-site tests and precise analysis methods for laboratory level tests were performed. Using these methods, a gas analysis was performed for the internal decomposition gases of a 154 kV transformer in operation. In addition, simulated discharge and thermal fault experiments were demonstrated. Each major decomposition gas generation characteristics was identified. The results showed that an approximate diagnosis of the inside of a gas-insulated transformer is possible by analyzing SO₂, SOF₂, and CO using simple analysis methods on-site. In addition, since there are differences in the types of decomposition gas generation patterns with various solid materials of the internal transformer, a detailed examination should be performed by using precise analysis methods in the laboratory.

• 한국화재소방학회논문지
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• 제16권1호
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• pp.18-23
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• 2002

저독성 폴리올레핀 절연재료, Sheath재료의 저독성, 연기밀도특성, 연소가스부식성 분석을 하기 위하여 저독성 내화케이블의 성능평가 시험을 수행하였다. 화재 발생시 화염확산 및 유독성가스발생의 주원인으로 피난안전계획에 매우 중요하다. 90년대 후반기부터 연이어 발생한 씨랜드 화재사고와 인천 인현동 라이브클럽등의 동일한 유형을 가진 화재사건을 계기로 국내 내화케이블에 사용되는 재료가 화재시 인명참사에 미치는 영향이 크다는 점이 발견되었다. 본 연구에서는 고체물질에서 발생하는 연기의 특성광학밀도를 ASTM E662를 근거로 하여 실험을 하였다. 전기로의 시스템은 20분동안 밀폐된 챔버내에서 2.5$\pm$0.04w/$\textrm{cm}^2$을 지닌 조사열량을 일정한 상태 하에서 방사를 유지할 수 있도록 하였다. NFR-8과 FR-PVC 연기밀도의 분해 결과에 따라 완전연소에 의한 연기밀도 최대값 NFR-8은 25.2에서 39.6 FR-PVC에서 51.1의 값을 얻을 수 있었다. 비연소 열분해에 의한 연기밀도 최대값 NFR-8은 100.4에서 112.2 FR-PVC는 126.5에서 398.8의 값을 얻을 수 있었다. 또한 시료의 연기밀도 분석결과 PVC가 폴리올핀 시료보다 상당히 많은 양의 CO가 발생되는 반면 $CO_24의 양은 적게 발생하였다.