• Title/Summary/Keyword: Size-characterization

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Characterization of Alumina Gel Prepared by Hydrolysis of Al(OC3H7i)3 (Al(OC3H7i)3의 가수분해로부터 얻어진 Al2O3 겔의 특성에 관한 연구)

  • 이서우;문종수;조성백
    • Journal of the Korean Ceramic Society
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    • v.25 no.2
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    • pp.89-94
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    • 1988
  • Alumina gel was prepared by the hydrolysis of aluminum isopropoxide Al(OC3H7i)3 at low temperature. Sample were calcined at the various temperatures for 10 houres in the electric furnace, respectively. In order to investigate the various propertis-thermal properties, pore size and distribution, and the transition of crystals, infrared spectroscopy, thermal analysis, particle size analysis, scanning electron microscopy, and porosimetry were employed. Transparent alumina gel was opalized at 1200$^{\circ}C$. Porosity was about 87% with pores below 0.7$\mu\textrm{m}$ and 55% at 1200$^{\circ}C$. The gel was transformed along the rising of temperature as follows; Boehmite\longrightarrow$\delta$-Al2O3\longrightarrow$\theta$\longrightarrowAl2O3\longrightarrow${\alpha}$-Al2O3.

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Image and Display Quality Evaluation

  • Ha, Yeong-Ho
    • 한국정보디스플레이학회:학술대회논문집
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    • 2009.10a
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    • pp.1224-1227
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    • 2009
  • When evaluating the quality of images and displays, it is important to combine the characteristics as perceived by the human visual system and measured by equipment using subjective and objective methods, respectively. In the case of objective methods, the quality of a display is measured using colorimetric or radiometric devices according to existing standards covering the color temperature, gamut size, gamma characteristic, and device characterization. Meanwhile, subjective methods assess the quality of an image using the human visual system based on a comparison with a reference or counterpart using such metrics as the sharpness, noise, contrast, saturation, and color accuracy. Objective and subjective methods are usually used together in comparison, as ultimately it is observers watching images on a display. In addition to existing objective methods, a new image quality metric is also introduced as regards the JPEG compression ratio that is reflected in the relationship between the gamut size and the color fidelity in CIELAB color space.

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Preparation and Characterization of CdTe Quantum Dots (CdTe 양자점 합성과 물리적 특성 분석)

  • 김현석;송현우;조경아;김상식;김성현
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.8
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    • pp.663-668
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    • 2003
  • CdTe quantum dots(QDs) were synthesized in aqueous solution by colloidal method. The synthesized CdTe QDs were identified to be cubic-structured ones by x-ray diffraction(XRD). The photoluminescence(PL) was performed for CdTe QDs prepared as a function of Te precursor concentration, condensation time and aging time. The PL intensity is strongly dependent on Te precursor concentration, indicating that the ratio of Te to Cd ions affects the particle size and size distribution of the CdTe QDs. Our PL study reveals that the intensity of PL peaks strengthens as the condensation time elongates, implying that annealing by thermal energy transferred during condensation would eliminate defects which act as killing centers in CdTe particles. Our photocurrent study suggests that the CdTe QDs materials are one of the prospective materials for optoelectronics including photodetectors.

Characterization of Soot Particles Generated in Non-sooting and Sooting Normal Diffusion Flames (Sooting 및 Non-Sooting 정상 확산 화염에서 생성되는 매연 입자의 특성에 대한 연구)

  • Choi, In-Chul;Lee, Jae-Bok;Hwang, Jung-Ho
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.24 no.7
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    • pp.984-993
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    • 2000
  • Characteristics of carbon soot particles generated in diffusion flames were studied. Non-sooting and sooting normal diffusion flames using propane or ethylene as fuel were selected. In the flames, soot volume fraction was measured by a thermocouple, and primary particle diameter and cluster size were analyzed by TEM photographs. The characteristics of soot particles depended on flame(non-sooting or sooting) and fuel(propane or ethylene) type. Unlike the sooting diffusion flames, particle growth and oxidation processes were clearly observed in the non-sooting diffusion flames. In the sooting diffusion flames, soot particle size was slightly changed at the flame tip.

Construction of Chromosome-Specific BAC Libraries from the Filamentous Ascomycete Ashbya gossypii

  • Choi Sang-Dun
    • Genomics & Informatics
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    • v.4 no.2
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    • pp.80-86
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    • 2006
  • It is clear that the construction of large insert DNA libraries is important for map-based gene cloning, the assembly of physical maps, and simple screening for specific genomic sequences. The bacterial artificial chromosome (BAC) system is likely to be an important tool for map-based cloning of genes since BAC libraries can be constructed simply and analyzed more efficiently than yeast artificial chromosome (YAC) libraries. BACs have significantly expanded the size of fragments from eukaryotic genomes that can be cloned in Escherichia coli as plasmid molecules. To facilitate the isolation of molecular-biologically important genes in Ashbya gossypii, we constructed Ashbya chromosome-specific BAC libraries using pBeloBAC11 and pBACwich vectors with an average insert size of 100 kb, which is equivalent to 19.8X genomic coverage. pBACwich was developed to streamline map-based cloning by providing a tool to integrate large DNA fragments into specific sites in chromosomes. These chromosome-specific libraries have provided a useful tool for the further characterization of the Ashbya genome including positional cloning and genome sequencing.

Effect of Carbon Addition and Sintering Temperature on Densification and Microstructural Evolution of Sinter-Hardening Alloys Steels

  • Verma, N.;Anand, S.;Upadhyaya, A.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.557-558
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    • 2006
  • In all conventional sintered PM products, the pores present are of two types, primary and secondary. Primary pores forming during compaction and latter during sintering, due to penetration of formed liquid through the matrix grain boundary. Effect of carbon addition on diffusion of Cu in SH737-2Cu system was investigated. After compaction and transient liquid phase sintering at $1120^{\circ}C$ and $1180^{\circ}C$, samples were characterized for densification, showing rise in sintering density and reduction in swelling on carbon addition. Quantitative microstructural characterization (shape factor and pore size) revealed bimodal distribution for 0% carbon, more rounded pores for 0.9% carbon and higher sintering temperature, and pore coarsening at higher sintering temperature.

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A Study on the Surface Characterization of Fe-17wt.%Cr Steel for Cast-bonding of Al and Stainless Steel (Al과 스텐레스강의 주조접합을 위한 STS430(Fe-17wt.%Cr)강의 표면처리 특성연구)

  • Kim, Eok-Soo
    • Journal of Korea Foundry Society
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    • v.25 no.3
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    • pp.134-141
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    • 2005
  • To overcome the undesirable deformation, peeling off and geometrical restrictions which were mainly caused by differences in thermal expansion coefficients during the cladding of aluminum strip and stainless strip, new processing method based on vacuum die casting is designed and implemented in fabricating Al/Fe-17wt%Cr steel(stainless steel). To increase cast-bonding ability, the surface of Fe-17wt%Cr steel is electrochemically etched to have optimum pit size and density. The optimum conditions to generate best pit are as follows: Solution: 1 M $Fecl_{3}$+1 M Nacl, Addition: $CuCl_{2}+HCl$, Current density: 80 $mA/cm^{2}$, Total current: 400 $coulomb/cm^{2}$, AC frequency :60 Hz.

Preparation and Characterization of Spherical Silica-coated Ceria Nanoparticles by Sol-Gel Method

  • Ahn, Yang-Kyu;Jeoung, Hae-Chan
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.96-96
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    • 2010
  • Monodispersed spherical silica-coated ceria nanoparticles were prepared through a sol-gel process using tetraethylorthosilicate (TEOS) and ceria fine particles. In this process, ceria fine particles were also prepared from cerium nitrate. The mean size of ceria particles was 300nm. Silica nanoparticles with narrow particle size distribution were prepared by controlled hydrolysis of TEOS solution. The silica sols were obtained by peptization, the process of redispersing a coagulated colloid, and were coated on ceria particles by the control of the weight ratio of silica/ceria and the pH of the mixture in aqueous solution. The morphologies of particles were characterized with scaning electron microscopy(SEM), transmission electron microscopy(TEM) and atomic force microscopy(AFM). The coating thickness of silica particles obtained by using this method was controlled in the range of 30 - 70nm.

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Optical Characterization of Smart Dust Based on Photonic Crystals and Its Sensing Applications

  • Kim, Sung Gi
    • Journal of Integrative Natural Science
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    • v.4 no.1
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    • pp.7-10
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    • 2011
  • Various types of smart dust based on photonic crystal exhibiting unique reflectivity were successfully obtained by an electrochemical etching of silicon wafer using square wave currents. Smart dust containing Bragg structure obtained from the sonication of DBR porous silicon film in solution retained its optical reflectivity. Field emission scanning electron micrograph (FE-SEM) was used to measure the size of optically encoded smart dust and its size can be tuned from few hundred nanometers to few microns depending on the duration of sonication. Optical characteristics of smart dust were used to investigate a possible applications such as chemical sensors.

Local Structure and Magnetic Properties of Fe-Mn Nanocrystalline Alloys Fabricated by Mechanical Alloying Technique as a Function of Milling Time

  • Tarigan, Kontan;Yang, Dong Seok;Yu, Seong Cho
    • Journal of Magnetics
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    • v.18 no.1
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    • pp.1-4
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    • 2013
  • Structural and magnetic properties of $Fe_{50}Mn_{50}$ nanocrystalline alloys prepared by the mechanical alloying technique (using commercial Fe and Mn powders as the precursors) are studied as a function of milling time, 1 hr to 48 hrs. The nano-crystallite size and shape are examined by using scanning electron microscopy (SEM). The effect of milling time on structural characterization was investigated using X-ray diffractometer (XRD) and extended X-ray absorption fine structure spectroscopy (EXAFS). Both XRD and EXAFS studies showed that the alloying process should be completed after 36 hrs milling. Concerning the magnetic behavior, the data obtained from superconducting quantum interference devices (SQUID) exhibited both magnetic saturation ($M_s$) and coercivity ($H_c$) depend strongly on the milling time, which are related to the changes in the crystallite size and magnetic dilution.