• Title/Summary/Keyword: Sintering process condition

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Machining characteristics on ultrasonic vibration assisted micro-electrical discharge machining of carbon-nanotube reinforced conductive Al2O3 composite (전도성을 가지는 탄소나노튜브강화 알루미나복합소재의 마이크로방전가공에서 초음파진동 부가에 의한 가공특성)

  • Kang, Myung-Chang;Tak, Hyun-Seok;Lee, Chang-Hoon;Kim, Nam-Kyung
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.13 no.6
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    • pp.119-126
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    • 2014
  • Micro-holes of conductive ceramic are required in micro structures. Micro-electrical discharge machining (Micro-EDM) is an effective machining method since EDM is as process for shaping hard metals and complex-shaped holes by spark erosion in all kinds of electro-conductive materials. However, as the depth of micro hole increases, the machining condition becomes more unstable due to inefficient removal of debris between the electrode and the workpiece. In this paper, micro-EDM was performed to evaluate machining characteristic such as electrode wear, machining time, taper angle, radial clearance with varying voltage and ultrasonic vibration on 10 vol.% Carbon-nanotube reinforced conductive $Al_2O_3$ composite fabricated by spark plasma sintering in previous research.

Performance Evaluation of Chip Breaker Utilizing Neural Network (신경망기법에 의한 칩브레이커의 성능평가)

  • Kim, Hong-Gyoo;Sim, Jae-Hyung
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.16 no.3
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    • pp.64-74
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    • 2007
  • The continuous chip in turning operation deteriorates precision of workpiece and causes a hazardous condition to operator. Thus the chip form control becomes a very important task for reliable machining process. So, grooved chip breaker is widely used to obtain reliable discontinuous chip. However, developing new cutting insert having chip breaker takes long time and needs lots of research expense due to a couple of processes such as forming, sintering, grinding and coating of product and many different evaluation tests. In this paper, performance of commercial chip breaker is evaluated with neural network which is learned with a back propagation algorithm. For the evaluation, several important elements(depth of cut, land, breadth, radius) which directly influence the chip formation were chosen among commercial chip breakers and were used as input values of neural network. With the results of these input values, the performance evaluation method was developed and applied that method to the commercial tools.

Phase Transition and Thermal Expansion Behavior of Zirconia Setter Fabricated from Fused CaO Stabilized Zirconia

  • Park, Ji-Hoon;Bang, Il-Hwan;Lee, Sang-Jin
    • Journal of the Korean Ceramic Society
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    • v.56 no.2
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    • pp.184-190
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    • 2019
  • To improve resistance in thermal shock of zirconia setter which is frequently and repeatedly exposed to high temperature, high degree of porosity and control of thermal expansion are needed for which the fused CSZ (CaO stabilized zirconia) is used to produce the zirconia setter. In the present study, the effects of sintering temperature, cool down condition, addition of CaO stabilizer, and addition of other additives on phase transition and thermal expansion behavior of the fabrication process of zirconia setter, were examined. The zirconia setter, fabricated with fused CSZ at 1550℃, exhibited 20.4 MPa of flexural strength, 6.8% of absorbance, and 27.9% of apparent porosity. The rapid change in thermal expansion of zirconia setter is observed at temperature around 800℃, and it was reduced by low firing temperature, slowed cooled down, and addition of CaO.

Fabrication and Physical Properties of Honeycomb Type Cordierite Ceramic Filter Using Fly-Ash (플라이 애쉬를 이용한 코디어라이트 세라믹 하니컴 필터 제조 및 물성)

  • Kim, Sung-Jin;Bang, Hee-Gon;Park, Sang-Yeup
    • Journal of the Korean Ceramic Society
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    • v.43 no.6 s.289
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    • pp.351-357
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    • 2006
  • The fabrication process of the honeycomb filter was investigated using synthesized cordierite with the addition of pore former and extrusion additives (either organic matter or graphite). Also, the effect of additives on the resultant properties of honeycomb filter such as porosity, thermal expansion coefficient and mechanical strength were investigated. With increasing the organic matter up to 10 wt%, porosity was increased but compressive strength was decreased. With increasing the graphite content, however, both porosity and compressive strength were increased. The specimen with an optimum processing condition (C-17A30G, sintering at $1150^{\circ}C$) was demonstrated 59% in porosity, 69 MPa in compressive strength, and $2.4{\times}10^{-6}/^{\circ}C\;(25{\sim}1000^{\circ}C$) in thermal expansion coefficient, which physical properties are appropriate for the honeycomb filter applications.

Oxygenation of Zone-melting NbBaCuO superconductor (구역용융법으로 제작된 NdBaCuO 초전도체의 산소흡착 특성)

  • Soh, Dea-Wha;Fan, Zhanguo;Kim, Hee-Nam;Li, Xinyu;Gao, Weiying;Kim, Tae-Wan
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11b
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    • pp.292-295
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    • 2001
  • The NdBaCuO superconducting samples were prepared by the Zone melting under low oxygen partial pressure. After the zone-melting the oxygenation process of the NdBaCuO samples in a oxygen flow furnace was studied. In order to compare the oxygenation condition the sintering NdBaCuO samples were studied also. In the study it is found that the optimum temperature for the oxygenation is $350^{\circ}C$, and the oxygen flow speed, the sample volume and the surface area of the sample would influence the oxygenation and the oxygen content.

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Fabrication of BSCCO high-Tc superconducting current lead (BSCCO 고온초전도 전류도입선의 제조)

  • 하동우;오상수;류강식;장현만
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1996.05a
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    • pp.252-255
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    • 1996
  • Superconducting current lead is one of the promising applications of the oxide high-Tc superconductors, because they have the advantage of decreasing heat conduction to low temperature region, comparing with a conventional cooper alloy lead. High critical current density is a key factor for the applications such as current lead. (Bi,Pb)$_2$Sr$_2$Ca$_2$Cu$_3$O$\_$x/ high Tc superconductor haute been investigated in terms of critical current density. Bi-2223 superconducting current lead made by CIP and solid state sintering process. Bi-2223 current lead that heat treated at 836$^{\circ}C$ for 240 h in 1/13 P$\_$O$_2$/ had over 150 A/$\textrm{cm}^2$ of critical current density at 77K. We knew that the superconducting properties of tube type current leads were better than rods type of them. And we investigated the relation of Bi-2223 formation and heat treatment condition by XRD and SEM analysis.

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Densification and Thermo-Mechanical Properties of Al2O3-ZrO2(Y2O3) Composites

  • Kim, Hee-Seung;Seo, Mi-Young;Kim, Ik-Jin
    • Journal of the Korean Ceramic Society
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    • v.43 no.9 s.292
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    • pp.515-518
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    • 2006
  • The microstructure of $ZrO_2$ toughened $Al_2O_3$ ceramics was carefully controlled so as to obtain dense and fine-grained ceramics, thereby improving the properties and reliability of the ceramics for capillary applications in semiconductor bonding technology. $Al_2O_3-ZrO_2(Y_2O_3)$ composite was produced via Ceramic Injection Molding (CIM) technology, followed by Sinter-HIP process. Room temperature strength, hardness, Young's modulus, thermal expansion coefficient and toughness were determined, as well as surface strengthening induced by the fine grained homogenous microstructure and the thermal treatment. The changes in alumina/zirconia grain size, sintering condition and HIP treatment were found to be correlated.

Synthesis and Properties of Ni-Zn Ferrite by Wet-Direct Process (습식 직접 합성법에 의한 Ni-Zn Ferrite의 합성 및 물성 연구)

  • 이경희;이병하;이융걸;황우연
    • Journal of the Korean Ceramic Society
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    • v.28 no.3
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    • pp.225-233
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    • 1991
  • In this study, we tried to find out the appropriate synthetic condition and magnetic properties of Ni-Zn ferrite {(NixZn1-x)Fe2O4} powders (where X=0, 0.1, 0.2, 0.3, ……0.9, 1). Ferrite powders were prepared by wet-direct method at 86℃ for 6hrs from FeCl36H2O, NiCl26H2O, and ZnCl2. The powders of (NixZn1-x)Fe2O4 (where X=0.4, 0.5, 0.6) have a good crystallinity, but the other ferrite powders consist of crystal and precursor ferrite. The ferrite powder's lattice constant is increased when ratio of ZnO contant is increased in the ferrite composition. And initial permeability was measured after sintering, result indicated regular pattern except (Ni0.4Zn0.6)Fe2O4 when the frequency were changed 10KHz to 10MHz.

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Oxygenation of Zone-melting NdBaCuG Superconductor (구역용융법으로 제작된 NdBaCuG 초전도체의 산소흡착 특성)

  • Soh, Dea-Wha;Fan, Zhanguo;Kim, Hee-Nam;Li, Xinyu;Gao, Weiying;Kim, Tae-Wan
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11a
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    • pp.292-295
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    • 2001
  • The NdBaCuO superconducting samples were prepared by the Zone melting under low oxygen partial pressure. After the zone-melting the oxygenation process of the NdBaCuO samples in a oxygen flow furnace was studied. In order to compare the oxygenation condition the sintering NdBaCuO samples were studied also. In the study it is found that the optimum temperature for the oxygenation is $350{\circ}C$, and the oxygen flow speed, the sample volume and the surface area of the sample would if1uence the oxygenation and the oxygen content.

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Sinter-hardening Process of P/M Steels and its Recent Developments

  • Yi, Jianhong;Ye, Tuming;Peng, Yuandong;Xia, Qinglin;Wang, Hongzhong
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.303-304
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    • 2006
  • The mechanical properties of ferrous powder metallurgy (P/M) materials are directly related to their microstructure. Ferrous P/M materials with sufficient hardenability will develop microstructures containing significant percentages of martensite in the as-sintered condition. Recently, sinter-hardening has developed into a highly cost effective production method through hardened P/M parts without the need for additional heat-treatments. This paper reviews the advances of sinter-hardening as well as some key processing parameters such as sintering temperature, cooling rate, tempering required to produce high quality sinter-hardened components. Specific topics including effect of alloying elements, alloying methods, and the Characterization and observation of microstructure are discussed.

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