• Title/Summary/Keyword: Single component

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Headspace Hanging Drop Liquid Phase Microextraction and GC-MS for the Determination of Linalool from Evening Primrose Flowers

  • Kim, Nam-Sun;Jung, Mi-Jin;Yoo, Zoo-Won;Lee, Sun-Neo;Lee, Dong-Sun
    • Bulletin of the Korean Chemical Society
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    • v.26 no.12
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    • pp.1996-2000
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    • 2005
  • Headspace hanging drop liquid phase micro-extraction (HS-HD-LPME) is studied as a novel solvent-based sample pretreatment method for floral volatile aroma compounds. This paper reports on application of the HSHD- LPME combined with GC-MS for the analysis of linalool component emitted from evening primrose flowers. The effect of several variables on the method performance was investigated. Additionally, the separation of enantiomers on a cyclodextrin capillary column was performed to identify chirality of (−)-linalool component. Since the unsurpassed volume of a few micro-liters of solvent is used, there is minimal waste or exposure to toxic organic solvents. This method enables to combine extraction, enrichment, clean-up, and sample introduction into a single step prior to the chromatographic process.

A basic study on ignitor for lean burn (희박연소용 점화장치에 대한 기초연구)

  • Lee, Sang-Jun;Na, Seong-O;Lee, Jong-Tae
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.21 no.1
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    • pp.36-48
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    • 1997
  • In order to establish the ignition system for lean burn, the influence of the number of spark plug, spark times and spark intervals on discharge pattern of spark energy on ignitability and combustion characteristics were evaluated. It showed that, ignitability remarkably increased with the case of multiple spark ignition system than with the case of single spark and the lean limit extended fuel/air equivalence ratio by 0.1, the increase of magnitude and lasting time of capacity component and inductance component was multi spark discharge in a row.

Motion of a System with Varying Damping Subject to Harmonic Force - Analytical Analysis (변화하는 감쇠를 갖는 계가 조화력을 받을 때의 운동 - 이론적 해석)

  • Park, O-Cheol;Lee, Gun-Myung
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2006.11a
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    • pp.898-902
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    • 2006
  • The motion of a system composed of a plate, constant springs and varying dampers is considered when the system is subject to harmonic force. Letting the frequencies of harmonic force and damper variation ${\Large f}_1\;and\;{\Large f}_2$ respectively, the displacement at the center of the plate has the strongest component at frequency ${\Large f}_1$. The angular displacement of the plate has strong components at ${\Large f}_1-{\Large f}_2$ and the natural frequency of the rotational mode of the system. If these two frequencies coincide, the plate oscillates with almost single frequency and a large amplitude. Part of these simulation results are proved analytically.

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Matrix Method in Multiple Projection through Plagioclase (사장석(斜長石)을 포함(包含)한 복수투영(複數投影)에 있어서의 행렬식(行列式) 이용(利用)에 관(關)한 연구(硏究))

  • Lee, Sang Hun
    • Economic and Environmental Geology
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    • v.17 no.4
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    • pp.283-288
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    • 1984
  • Projection method has been used in the phase equilibria study. The projection is made through the saturated phase on the smaller chemical system from larger system. This decreases the number of phases which are included in the larger chemical system. In multiple projection containing plagioclase as a projection phase, there is a difference in matrix calculation when plagioclase is treated as a single composite component and separately as an albite and anorthite. The matrix calculation is considered to be more usable and easier in multiple projection. The value of the A component in the AFM system, which is the smaller system projected from the larger one, is effected and varies according to the change in the An content in plagioclase that is examined as an example.

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Analysis and Design of DC-DC Converter with Independent Dual Outputs (독립적인 이중 출력을 갖는 DC-DC 컨버터의 해석 및 설계)

  • Heo, Tae-Won;Park, Ji-Ho;Kim, Dong-Wan;Woo, Jung-In
    • The Transactions of the Korean Institute of Electrical Engineers P
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    • v.54 no.4
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    • pp.171-178
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    • 2005
  • The proposed dual-output DC-DC converter that bases on flyback converter can obtain two output voltage with non-isolated main-output and isolated sub-output at the same time using single-winding high frequency transformer. It can solve problems in multi-winding converter that use one main-switch, and also control quality of isolated sub-output voltage can be improved by additional sub-switch to the second. For analysis and design of the proposed converter system, converters are classified as operation mode from switching state and are become modeling by applying state space averaging method. Steady-state characteristics and dynamic characteristics are analyzed by DC component and perturbation component from state space averaging model. From experiment converter, validity of analysis and design for the propose converter system is confirm.

Fabrication and Straining Model of a CNT/EAP Composite Film (카본나노튜브/도전성폴리머(CNT/EAP) 복합재 필름의 제조 및 특성분석)

  • Zhang, Shuai;Kim, Cheol
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2005.11a
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    • pp.117-120
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    • 2005
  • The relationship between strain and applied potential was derived for composite actuators consisting single-wall carbon nanotubes (SWNTs) and conductive polymers (CPs). During deriving the relationship, an electrochemical ionic approach is utilized to formulate the electromechanical actuation of the composite film actuator. The results show that the well-aligned SWNTs composite actuator can give good actuation responses and high actuating forces available. The actuation is found to be affected by both SWNTs and CPs components and the actuation of SWNTs component has two kinds of influences on that of the CPs component: reinforcement at the positive voltage and abatement at the negative voltage. CNT/EAP was fabricated successfully using the chemical polymerization method.

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Identification of Fish Species using Affine Transformation and Principal Component Analysis of Time-Frequency Images of Broadband Acoustic Echoes from Individual Live Fish (활어 개체어의 광대역 음향산란신호에 대한 시간-주파수 이미지의 어파인 변환과 주성분 분석을 이용한 어종식별)

  • Lee, Dae-Jae
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.50 no.2
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    • pp.195-206
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    • 2017
  • Joint time-frequency images of the broadband echo signals of six fish species were obtained using the smoothed pseudo-Wigner-Ville distribution in controlled environments. Affine transformation and principal component analysis were used to obtain eigenimages that provided species-specific acoustic features for each of the six fish species. The echo images of an unknown fish species, acquired in real time and in a fully automated fashion, were identified by finding the smallest Euclidean or Mahalanobis distance between each combination of weight matrices of the test image of the fish species to be identified and of the eigenimage classes of each of six fish species in the training set. The experimental results showed that the Mahalanobis classifier performed better than the Euclidean classifier in identifying both single- and mixed-species groups of all species assessed.

Test of KSR-III Rocket Propellant Feeding System Using PTA-II Test Facility (PTA-II 시험설비를 활용한 KSR-III Rocket 추진기관시스템 종합시험)

  • Kang Sun-il;Cho Sang-yoen;Kwon Oh-sung;Lee Jeong-ho;Oh Seung-hyup;Ha Sung-up;Kim Young-han
    • Proceedings of the KSME Conference
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    • 2002.08a
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    • pp.263-266
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    • 2002
  • The KSR-III developed by KARI is the first rocket vehicle which is adopting the liquid propellant rocket engine system in Korea. Not only the engine itself, but also the propellant feeding system is one of the most important component in liquid rocket vehicle. In this paper, the authors are intended to introduce the multi-purpose test facility(PTA-II Test Facility) which is constructed for the variety of tests on KSR-III feeding system(single component tests, verification tests, cold flow tests and combustion tests). With the results of these tests, we can identify the characteristics of rocket feeding system and decide the optimum setting values of feeding system for the successful flight.

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RELSYS: A computer program for structural system reliability

  • Estes, Allen C.;Frangopol, Dan M.
    • Structural Engineering and Mechanics
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    • v.6 no.8
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    • pp.901-919
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    • 1998
  • Most reliability-based analyses focus on the reliability of the individual components of a structure. There are many advantages to examining the components in combination as an entire structural system. This paper illustrates an algorithm used in the computer program RELSYS (RELiability of SYStems) which computes the system reliability of any structure which can be modeled as a series-parallel combination of its components. A first-order method is used to initially compute the reliability of each individual component. The system reliability is computed by successively reducing the series and parallel systems until the system has been simplified to a single equivalent component. Equivalent alpha vectors are used to account for the correlation between failure modes during the system reduction process.

The Crystal Structure of Licarin-B $(C_{20}H_{20}O_4)$, A Component of the Seeds of Myristica fragrans

  • Kim, Yang-Bae;Park, Il-Yeong;Shin, Kuk-Hyun
    • Archives of Pharmacal Research
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    • v.14 no.1
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    • pp.1-6
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    • 1991
  • The crystal structure of licarin-B, a component of Myristicae Semen was determined by single crystal X-ray diffraction analysis. Crystal of the compound, which was recrystallized from the mixture of hexane and ether, is monoclinic with a=12.740(1), b=7.219(1), c=9.284(1) ${\AA}$, ${\beta}=94.75(1)^{\circ}$, $D_x=1.26$, $D_m=1.27\;g/cm^3$, space group P21, and Z=2. The structure was solved by direct method and refined by least-squares procedure to the final R value of 0.040 for 1532 independent reflections ${F{\ge}3{\sigma}(F)}$. The compound is a dimeric phenylpropanoid, and belongs to the neolignan analogues. The molecules are arranged along with the screw axis. The intermolecular contacts appear to be the normal van der Waals' forces.

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