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http://dx.doi.org/10.5012/bkcs.2005.26.12.1996

Headspace Hanging Drop Liquid Phase Microextraction and GC-MS for the Determination of Linalool from Evening Primrose Flowers  

Kim, Nam-Sun (Department of Chemistry, Seoul Women's University)
Jung, Mi-Jin (Department of Chemistry, Seoul Women's University)
Yoo, Zoo-Won (Department of Chemistry, Seoul Women's University)
Lee, Sun-Neo (Department of Chemistry, Seoul Women's University)
Lee, Dong-Sun (Department of Chemistry, Seoul Women's University)
Publication Information
Bulletin of the Korean Chemical Society / v.26, no.12, 2005 , pp. 1996-2000 More about this Journal
Abstract
Headspace hanging drop liquid phase micro-extraction (HS-HD-LPME) is studied as a novel solvent-based sample pretreatment method for floral volatile aroma compounds. This paper reports on application of the HSHD- LPME combined with GC-MS for the analysis of linalool component emitted from evening primrose flowers. The effect of several variables on the method performance was investigated. Additionally, the separation of enantiomers on a cyclodextrin capillary column was performed to identify chirality of (−)-linalool component. Since the unsurpassed volume of a few micro-liters of solvent is used, there is minimal waste or exposure to toxic organic solvents. This method enables to combine extraction, enrichment, clean-up, and sample introduction into a single step prior to the chromatographic process.
Keywords
Headspace hanging drop liquid phase microextraction (HS-HD-LPME); Evening primrose; Linalool; GC-MS;
Citations & Related Records
Times Cited By KSCI : 1  (Citation Analysis)
Times Cited By Web Of Science : 3  (Related Records In Web of Science)
Times Cited By SCOPUS : 4
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1 Liu, H.; Dasgupta, P. K. Tr. Anal. Chem. 1996, 15, 468
2 Liu, S.; Dasgupta, P. K. Anal. Chem. 1995, 67, 2042   DOI
3 Kim, N. S.; Lee, D. S. J. Sep. Sci. 2004, 27, 96   DOI   ScienceOn
4 Brenna, E.; Fuganti, C.; Serra, S. Tetrahedron: Asymmetry 2003, 14, 1   DOI   ScienceOn
5 Marriott, P. J.; Shellie, R.; Cornwell, C. J. Chromatogr. A 2001, 936, 1   DOI   ScienceOn
6 Steffen, A.; Pawliszyn, J. J. Agric. Food Chem. 1996, 44, 2187   DOI   ScienceOn
7 Bicchi, C.; Drigo, S.; Rubiolo, P. J. Chromatogr. A 2000, 892, 469   DOI   ScienceOn
8 Miller, M. E.; Stuart, J. D. Anal. Chem. 1999, 71, 23   DOI   ScienceOn
9 Lee, S. N.; Kim, N. S.; Lee, D. S. Anal. Bioanal. Chem. 2003, 377, 749   DOI   ScienceOn
10 Kim, N. S.; Lee, D. S. J. Chromatogr. A 2002, 982, 31   DOI   ScienceOn
11 Yoo, Z. W.; Kim, N. S.; Lee, D. S. Bull. Korean Chem. Soc. 2004, 25, 271   DOI   ScienceOn
12 Liu, H.; Dasgupta, P. K. Anal. Chem. 1996, 68, 1817   DOI   ScienceOn
13 Theis, A. L.; Waldack, A. J.; Hansen, S. M.; Jeannot, M. A. Anal. Chem. 2001, 73, 5651   DOI   ScienceOn
14 Przyjazny, A.; Kokosa, J. M. J. Chromatogr. A 2002, 977, 143   DOI   ScienceOn
15 Yamini, Y.; Hojjati, M.; Haji-Hosseini, M.; Shamsipur, M. Talanta 2004, 62, 265   DOI   ScienceOn
16 Zhao, R. S.; Lao, X. J.; Xu, X. B. Talanta 2004, 62, 751   DOI   ScienceOn
17 Zhang, Z.; Pawliszyn, J. Anal. Chem. 1993, 65, 1843   DOI   ScienceOn
18 Psillakis, E.; Kalogerakis, N. J. Chromatogr. A 2001, 938, 113   DOI   ScienceOn
19 Hou, L.; Lee, H. K. J. Chromatogr. A 2002, 976, 377   DOI   ScienceOn
20 Zabaras, D.; Wyllie, S. G. Flavour Fragr. J. 2001, 16, 411   DOI   ScienceOn
21 Bicchi, C.; D'Amato, A.; Rubiolo, P. J. Chromator. A 1999, 843, 99   DOI   ScienceOn
22 Psillakis, E.; Kalogerakis, N. Trends Anal. Chem. 2002, 21, 53
23 Jeannot, M. A.; Cantwell, F. F. Anal. Chem. 1996, 68, 2236   DOI   ScienceOn
24 He, Y.; Lee, H. K. Anal. Chem. 1997, 69, 4634   DOI   ScienceOn
25 Psillakis, E.; Kalogerakis, N. J. Chromatogr. A 2001, 907, 211   DOI   ScienceOn
26 de Jager, L. S.; Andrews, A. R. J. Chromatographia 1999, 50, 733   DOI   ScienceOn