• Title/Summary/Keyword: Sieve

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A Study on the Separation of n-Hexane by Molecular Sieve 5A and the Purification for HPLC use (분자체 5A를 이용한 n-헥산의 분리와 HPLC급으로의 정제에 관한 연구)

  • Choi, Beom Suk;Kim, Young Man;Kim, Sun Tae
    • Analytical Science and Technology
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    • v.6 no.1
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    • pp.21-27
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    • 1993
  • Technical grade n-hexane whose purity is 54% has been purified for HPLC use. Methylcyclopentane, 2-methylpentane, and 3-methylpentane which are hardly isolated by fractional distillation were separated by the liquid-solid chromatography using molecular sieve 5A. UV and fluorescence impurities whose contents are critically regulated for HPLC solvent were removed by the adsorptive separation with alumina and silica gel. The present method also reduced the impurities of color(APHA), acidity, water, residue after evaporation, sulfur, and thiophene content, and the impurity contents were well within the specifications of HPLC solvent.

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Preparation, Characterization, and Gas Permeation Properties of Carbon Molecular Sieve Membranes Derived from Dense P84-Polyimide Film

  • Park, Ho-Bum;Nam, Sang-Yong;Jang, Jeong-Gyu;Lee, Young-Moo
    • Korean Membrane Journal
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    • v.4 no.1
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    • pp.25-35
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    • 2002
  • The gas permeation properties have been studied on carbon molecular sieve (CMS) membranes prepared by pyrolysis of P84 polyimide under various conditions. P84 polyimide shows high permselectivities (O$_2$/N$_2$= 9.17 and CO$_2$/N$_2$= 35) for various gas pairs and has a good processibility because it is easily soluble in high polar solvents such as N-methylpyrrolidinone (NMP), dimethylformamide (DMF), and N,N-dimethylacetamide (DMAc). After pyrolysis under Ar flow, the change in the heating rate was found to affect the gas permeation properties to some extent. The permeabilities of the selected gases were shown to be in the order He > CO$_2$> O$_2$> N$_2$for all the CMS membranes, whose order was in accordance with the order of kinetic gas diameters. It also revealed that the pyrolysis temperature considerably influenced the gas permeation properties of the CMS membranes derived from P84 polyimide. The CMS membranes pyrolized at 700$\^{C}$ temperature exhibited the highest permeability with relatively targe loss in permselectivity. This means that the pyrolysis temperature should be varied in accordance with target gases to be separated.

A Study on a Heat Transfer Characteristics of Direct Contact Heat Exchanger for Steam Condensation According to Various Cooling Water Flow and Internal Pressure(The Purpose of Combination with LNG Evaporator) (증기응축용 직접접촉식 열교환기의 냉각수 유량과 내부압 변화에 따른 열전달 특성연구(LNG 기화기와의 조합목적))

  • Lee, B.C.;Han, S.T.;Kim, C.B.
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.3 no.3
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    • pp.153-160
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    • 1991
  • Heat transfer characteristics of a direct contact heat exchanger utilizing sieve trays and spray nozzles for steam condensation for the purpose of combining with a LNG evaporator have been investigated with various cooling water flow rates and different vacuum pressures within the heat exchanger for the purpose of steam condensation. Temperature profiles and the volumetric overall heat transfer coefficients in a direct contact heat exchanger have been obtained for comparisons. The results show that the temperature differences between cooling water and steam along the direct contact heat exchanger height are rapidly decreasing and the volumetric overall heat transfer coefficients of the exchanger improves greatly as the inside vacuum pressure increases. The values of the overall heat transfer coefficients at P=-680mmHg have been increased significantly compared with at atmospheric pressure. At given pressure conditions, it is found that the values of average volumetric overall heat transfer coefficients for the sieve tray are found to be approximately 10% higher than those of the spray nozzle.

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A Study on Shear Strength of Granular Due to The Various Particle Size (조립질 입자크기가 전단강도에 미치는 영향)

  • Lee, Seungho;Seo, Hyungil
    • Journal of the Korean GEO-environmental Society
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    • v.13 no.4
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    • pp.71-76
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    • 2012
  • Shear strength of soil is power that resists failure and sliding according to any face in soils and one of the most important factors during engineering properties of soil. Shear strength is used for engineering science problems as bearing capacity methods of foundation or piles, slope stability after dam or Cutting Embankment and stability problem analysis of soils as lateral earth pressure of soil structures, ets. This study has analyzed shear strength change of samples classified 2.00mm(10sieve)와 0.85mm(20sieve), 0.475mm(40sieve) using direct shear tester after removing and drying cohesive soil ingredient of Weathered granite soil Therefore, this study would help studies about shear strength properties by particle size.

Development of hiting sesamer thresher (타격식 참깨탈곡기 개발)

  • 박회만;정성근;홍성기;최희석;홍현유
    • Proceedings of the Korean Society for Agricultural Machinery Conference
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    • 2003.07a
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    • pp.309-316
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    • 2003
  • Generally, sesame are dried on the field after being harvested in Korea. Since harvesting season is rainy autumn and sesame drying is mainly affected sun and natural wind, it is difficult to dry sesame in time. Moreover, sesame threshing by hand is very laborious work. Therefore, tractor mounted sesame thresher which threshes sesame bundles fed in upside down and conveyed along threshing bar was developed to mechanize sesame threshing and to reduce labor cost in this research. the thresher was equipped with a threshing bar which beats sesame bundles and a three layer sieve which screens sesame. The results are summarized as follows ; 1 The sesame thresher was consisted of a hitting-stick, a feeding chain conveyor, a threshing bar, conveyor belt, and the three-layer shaking sieve. 2. In threshing test, prototype thresher showed maximum threshing ratio 98.5%, 98.7% at 14, 17 cpm beating rate respectively. 3. In screening test, prototype sieve showed maximum threshing ratio 97.2% at 12$^{\circ}$ of inclined angle and 220 cpm of sieve vibrating rate. 4. Prototype showed 98.7% of threshing ratio, 1.3% of threshing loss, 97.0% of screening ratio, 0.7% of screening loss on the rest condition of 15 sesame bundles/min of feeding rate, 14 cpm of beating rate, 220 cpm of sieve vibrating rate. 5. The working performance of prototype was 0.5hr/10a. It was 9.6 times more efficient than manual work. And, operation cost of prototype was saved by 45.9% compared to manual work.

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The Reapperarance of Relative Density by the Multiple Sieving Pluviation Method (다중체 낙하법에 의한 상대밀도 재현에 관한 연구)

  • 주재우;곽정민
    • Proceedings of the Korean Geotechical Society Conference
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    • 1994.09a
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    • pp.265-272
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    • 1994
  • The relative density seems to be important as a factor of controlling the physical properties in the case of cohesionless soil ground as sand. Therefore, the study is more important about the method for reappearing the same relative density when the specimen of shearing test is to be produced or the model test of ground is to be made. In this study, the apparatus making use of the multiple sieving pluviation method - one of the reappearance of relative density - could be made. Using this apparatus, tests were practiced varying the factors such as the size of sieve mesh and the number of sieve, the amount of falling discharge, the falling height etc. about the standard sand in Jumunjin and Hadong sand. When laboratory test is performed by the cohensionless soil , it presents the method for reappearing of the relative density in field.

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