• 한국전기전자재료학회논문지
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• 제27권11호
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• pp.712-717
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• 2014

Glass ceramic has a high mechanical strength and low sintering temperature. So, it can be used as a thick film substrate or a high strength insulator. A series of glass ceramic samples based on MgO-$Al_2O_3-SiO_2-ZrO_2$ (MASZ) were prepared by melting at $1,600^{\circ}C$, roll-quenching and heat treatment at various temperatures from $900^{\circ}C$ to $1,400^{\circ}C$. Dependent on the heat treatment temperature used, glass ceramics with different crystal phases were obtained. Their nucleation behavior, microstructure and mechanical properties were investigated with differential thermal analysis (DTA), X-ray diffraction (XRD), scanning electron microscopy (SEM), and Vicker's hardness testing machine. With increasing the heat treatment temperature of MASZ samples, their hardness and toughness initially increase and then reach the maximum points at $1,300^{\circ}C$, and begin to decrease at above this temperature, which is likely to be due to the softening of glass ceramics. As the content of $ZrO_2$ in MAS glass ceramics increases from 7.0 wt.% to 13 wt.%, Vicker's hardness and fracture toughness increase from $853Kg/mm^2$ to $878Kg/mm^2$ and $1.6MPa{\cdot}m^{1/2}$ to $2.4MPa{\cdot}m^{1/2}$ respectively, which seems to be related with the nucleation of elongated phases like fiber.

• 한국세라믹학회지
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• 제47권5호
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• pp.381-386
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• 2010

Some basic properties of inorganic coatings hardened by the room temperature reaction with alkalies were examined. The coating paste was prepared from the powders in the system $Al_2O_3-SiO_2$-CaO using blast furnace slag, fly ash and amorphous ceramic fiber after mixing with a solution of sodium hydroxide and water glass. The mineralogical and morphological examinations were performed for the coatings prepared at room temperature and after heating to $1200^{\circ}C$ respectively. The binding force of the coating hardened at room temperature was caused by the formation of fairly dense matrix mainly composed of oyelite-containing amorphous phase formed by the reaction between blast furnace slag and alkali solution. At the temperature, fly ash and ceramic fiber was not reacted but imbedded in the binding phase, giving the fluidity to the paste and reinforcing the coating respectively. During heating up to $1200^{\circ}C$, instead of a break in the coating, anorthite and gehlenite was crystallized out by the reaction among the binding phase and unreacted components in ternary system. The crystallization of these minerals revealed to be a reason that the coating maintains dense morphology after heating. The maintenance of binding force after heat treatment is seemed to be also caused by the formation of welldispersed fiber-like mineral phase which is originated from the shape of the amorphous ceramic fiber used as a raw materials.

• 한국광물학회지
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• 제21권3호
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• pp.283-287
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• 2008

$SiO_2$를 함유한 테트라에시실란(Tetracthoxysilanc: TEOS)과 알루미늄-섹-버트옥사이드(alumimum-sec-butoxide: ASB)를 출발물질로 이용하여 $100^{\circ}C$ 이하에서 결정성이 양호한 이모골라이트를 합성하였다. 합성실험은 환류장치가 부착된 둥근 플라스크에서 연속교반하면서 수열법으로 수행하였다. 이때, 화학조성은 $Al_{2}O_{3}/SiO_2$ = 1의 조건이었다. TEOS와 ABS의 농도 0.5 M의 조건에서 합성된 이모골라이트의 분말 X-선 회절 분석결과. d = 22.4. 9.5 등에서 회절선들을 관찰할 수 있었고, DTA/TG 분석견과에서는 $68^{\circ}C$에서 탈수반응에 의한, 그리고 $249^{\circ}C$에서 탁수산화 반응에 의한 흡열반응이 관찰되었으며 중량손실은 약 41%이었다. 또한, 합성된 이모골라이트는 Si-O-Al 신축진동(953과 $993cm^{-1}$)과 O-Si-O 굽힘 진동$(562cm^{-1})$에 의해서 미약하고 비대핑형의 피크 분리가 관찰되었고, TEM 분석결과, 이모골라이트 결정은 섬유상이었으며 거리줄 모양의 네트워크 구조를 보였다.

• 대한전기학회:학술대회논문집
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• 대한전기학회 1996년도 추계학술대회 논문집 학회본부
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• pp.439-441
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• 1996

A simple coupling method between APD(avalanche photodiode) arrays and SMF(single mode fiber) arrays on a Silicon carrier composed of V-grooves is proposed and carried out. Jacketed fibers embedded in V-grooves are used as alignment marks instead of patterned pedestals or solder bumps and a optical receiver module are packaged.

• Corrosion Science and Technology
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• 제9권1호
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• pp.48-55
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• 2010

The many vessels are built with FRP(Fiber-Reinforced Plastic) material for small boats and medium vessels. However, FRP is impossible to be used for recyclable material owing to environmental problems and causes large proportion of collision accidents because radar reflection wave is so weak that large vessels could not detect FRP ships during the sailing. Hence, Al alloy comes into the spotlight to solve these kinds of problems as a new-material for next generation instead of FRP. Al alloy ships are getting widely introduced for fish and leisure boats to save fuel consumption due to lightweight. In this study, it was selected 6061-T6 Al alloy which are mainly used for Al-ships and carried out various electrochemical experiment such as potential, anodic/cathodic polarization, Tafel analysis, potentiostatic experiment and surface morphologies observation after potentiostatic experiment for 1200 sec by using the SEM equipment to evaluate optimum corrosion protection potential in sea water. It is concluded that the optimum corrosion protection potential range is -1.4 V ~ -0.7 V(Ag/AgCl) for 6061-T6 Al alloy, in the case of application of ICCP(Impressed current cathodic protection), which was shown the lowest current density at the electrochemical experiment and good specimen surface morphologies after potentiostatic experiment for Al-Mg-Si(6061-T6) Al alloy in seawater environment.

• 폴리머
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• 제25권6호
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• pp.866-875
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• 2001

본 연구에서는 고온 산화분위기 하에서 탄소/탄소 복합재료의 열적 향상을 위해 사용된 tetraethylorthosilicate(TEOS)의 첨가량에 따른 복합재료의 kinetic parameter에 기초한 열분해 메카니즘 및 열안정성을 열중량분석기(TGA)를 사용하여 고찰하였다 TEOS를 함유한 탄소/탄소 복합재료의 kinetic parameter, 즉 열분해 활성화 에너지 ($E_d$), 반응차수(n), 지수앞 인자 (A)는 각각 136 kJ/mol, 0차, 및 2.3$\times$$10^9s^{-1}$을 나타내었으며, 특히 IPDT 및 $E_d$로부터 살펴본 복합재료의 열안정성은 탄소/탄소 복합재료에 TEOS가 첨가되면 크게 향상되었는데, 이는 산소에 대한 산화방지막, 즉 $SiO_2$의 형성으로 인한 복합재료 표면에서의 카본 활성종에 산소의 침투를 방해하여 TEOS를 함유한 복합재료가 이를 함유하지 않은 것에 비하여 표면 산화 속도가 감소되어 열안정성이 증가하였다고 사료된다.

• 한국산학기술학회논문지
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• 제9권2호
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• pp.291-297
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• 2008

일방향 탄소섬유 강화 복합재료(CFRP)의 고체입자 마식 거동을 다양한 충돌각도 (${\alpha}$), 속도 (V) 및 섬유 방향 (${\beta}$)에 대하여 연구하였다. 실험결과 30o 충돌각도에서 최대 마식률을 나타내었고, 마식률은 멱함수 법칙 $E{\propto}\;V^n$에 따라 충돌속도에 크게 의존하였다. 본 연구에서는 이상의 결과로부터 일방향 탄소섬유 강화 복합재료의 마식률을 충돌속도, 충돌각도 및 섬유방향 각도로부터 예측하는 방법을 제안하였다.

• Smart Structures and Systems
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• 제13권4호
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• pp.501-515
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• 2014

This paper presents a linear computational homogenization framework to evaluate the effective (or generalized) electromechanical coupling coefficient (EMCC) of adaptive structures with piezoelectric structural fiber (PSF) composite elements. The PSF consists of a silicon carbide (SiC) or carbon core fiber as reinforcement to a fragile piezo-ceramic shell. For the micro-scale analysis, a micromechanics model based on the variational asymptotic method for unit cell homogenization (VAMUCH) is used to evaluate the overall electromechanical properties of the PSF composites. At the macro-scale, a finite element (FE) analysis with the commercial FE code ABAQUS is performed to evaluate the effective EMCC for structures with the PSF composite patches. The EMCC is postprocessed from free-vibrations analysis under short-circuit (SC) and open-circuit (OC) electrodes of the patches. This linear two-scale computational framework may be useful for the optimal design of active structure multi-functional composites which can be used for multi-functional applications such as structural health monitoring, power harvest, vibration sensing and control, damping, and shape control through anisotropic actuation.

• 한국잠사학회:학술대회논문집
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• 한국잠사학회 2003년도 International Symposium of Silkworm/Insect Biotechnology and Annual Meeting of Korea Society of Sericultural Science
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• pp.78-79
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• 2003

To further understanding of the role of calreticulin in insects, we have isolated a cDNA of calreticulin from silkworm, Bombyx mori. The cDNA encodes a 398 amino acid residues of B. mori calreticulin with endoplasmic reticulum retentional HDEL motif at its C-terminus, and a predicted molecular mass of 45801 Da. The B. mori calreticulin shows high protein homology with those of G mellonella (88%), A. aegypti (71%) and H. sapiens (63%). (omitted)

• 한국광학회지
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• 제10권6호
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• pp.500-506
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• 1999

레이저 다이오드와 수신광검출기가 집적된 소자를 V-홈을 가진 실리콘 광학벤치에 flip-chip 본딩하고, 경사면을 가진 하나의 단일모드 광섬유와 수동정렬하는 방법을 사용하여 가입자망을 위한 저가의 양방향 송수신 모듈을 설계, 제작하였다. 광섬유의 단면 경사각에 따른 송신광결합 효율과 수신광결합 효율사이의 병목점을 찾기 위해 Gaussian빔 모델을 사용하여 수평정렬거리, 광섬유 단면 경사각, 수직정렬오차등의 변수에 따른 광결합계수를 계산함으로써, 최적의 광정렬조건을 예측하였다. 또한 실리콘 광학벤치에서 광결합효율을 측정하여 광섬유의 수직정렬오차에 따른 광결합계수의 감소가 광섬유의 경사각에 의해 보상될 수 있다는 계산결과의 타당함을 확인하였다. 실제의 sub-module 제작 및 광결합 실험에서 송신빔이 광섬유 단면에 반사되어 PD로 입사되는 것을 최소화하기 위하여 광섬유 단면을 경사절두원추형으로 제작함으로써 PD의 수신 잡음을 $30mu$m 이상의 정렬거리에서 -35dB이하로 유지할 수 있었다. 같은 조건에서 단면 경사각이 $12^{\circ}$인 광섬유에 의해 -12.1dB의 송신출력과 0.2A/W의 responsivity를 얻을 수 있었다.