• 열처리공학회지
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• 제22권5호
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• pp.267-274
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• 2009

Titanium Chromium Nitrided (TiCrN) coatings were deposited on stainless steel 316 L and Si (100) wafer by inductively coupled plasma assisted D.C. magnetron sputtering at the various sputtering power on Cr target and $N_2/Ar$ gas ratio. Increasing the sputtering power of Cr target, XRD patterns were changed from TiCrN to nitride $Cr_2Ti$. The maximum hardness was $Hk_{3g}$ 3900 at $0.3\;N_2/Ar$ gas ratio. The thickness of the TiCrN films increased as the Cr target power increased, and it showed over $Hk_{5g}3100$ hardness at 100 W, 150 W. TiCrN films were deposited by the ICP assisted DC magnetron sputtering shown good wear resistance as the $N_2/Ar$ gas ratio was 0.1, 0.3.

• 한국재료학회지
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• 제22권9호
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• pp.482-488
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• 2012

To fabricate a precise micro metal mold, the electrochemical etching process has been researched. We investigated the electrochemical etching process numerically and experimentally to determine the etching tendency of the process, focusing on the current density, which is a major parameter of the process. The finite element method, a kind of numerical analysis, was used to determine the current density distribution on the workpiece. Stainless steel(SS304) substrate with various sized square and circular array patterns as an anode and copper(Cu) plate as a cathode were used for the electrochemical experiments. A mixture of $H_2SO_4$, $H_3PO_4$, and DIW was used as an electrolyte. In this paper, comparison of the results from the experiment and the numerical simulation is presented, including the current density distribution and line profile from the simulation, and the etching profile and surface morphology from the experiment. Etching profile and surface morphology were characterized using a 3D-profiler and FE-SEM measurement. From a comparison of the data, it was confirmed that the current density distribution and the line profile of the simulation were similar to the surface morphology and the etching profile of the experiment, respectively. The current density is more concentrated at the vertex of the square pattern and circumference of the circular pattern. And, the depth of the etched area is proportional to the current density.

• 한국해양공학회지
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• 제24권5호
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• pp.67-74
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• 2010

Chromate conversion coating is a coating technique used to passivate aluminum, zinc, cadmium, copper, silver, magnesium, tin, and their alloys to slow corrosion. The process uses various toxic chromium compounds, which may include hexavalent chromium. The industry is developing less toxic alternatives in order to comply with substance restriction legislation, such as RoHS. One alternative is to develop a Cr-free coating solution. In this study, eco-friendly, Cr-free solutions (urethane solution S-700, organic/inorganic solution with Si LRO-317) were used. Test specimens were dried in a drying oven at $190^{\circ}C$ for 3, 5, 7, and 9 minutes. Corrosion resistance was evaluated using a salt spray test for 72 hours. The results show that the optimum corrosion resistance was achieved at $190^{\circ}C$ for five minutes for EGI and three or five minutes for HDGI, respectively. The adhesive properties of the two types of coating solutions were superior regardless of drying time.

• 지질공학
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• 제18권1호
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• pp.93-102
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• 2008

최근 국내 터널현장에서는 기존 H형 강지보의 단점을 보완한 격자지보의 사용이 증가하고 있다. 격자지보는 숏크리트와 일체구조를 형성하며 지반을 지지한다. 따라서 지반하중을 산정하기 위해서는 격자지보 계측이 필요하다. 그러나 국내 터널 현장에서 격자지보 계측은 거의 수행되지 않고 있으며 적절한 계측 방법에 대한 이론도 확립되지 못한 상태이다. 숏크리트 계측에서는 무응력 상태에서 지반하중과 관계없이 숏크리트에서 발생하는 변형률에 대한 고려가 필요하지만 이에 대한 보정은 거의 이루어지지 알고 있다. 본 연구에서는 터널 현장에서의 격자지보와 무응력 숏크리트 계측 결과를 분석하여 주지보 계측의 신뢰성을 향상시킬 수 있는 방안을 제시하였다.

• 한국분말재료학회지
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• 제22권3호
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• pp.197-202
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• 2015

In this study, porous stainless steel (STS316L) sintered body was fabricated by powder metallurgy method and its properties such as porosity, compressive yield strength, hardness, and permeability were evaluated. 67.5Fe-17Cr- 13Ni-2.5Mo (wt%) powder was produced by a water atomization. The atomized powder was classified into size with under $45{\mu}m$ and over $180{\mu}m$, and then they were compacted with various pressures and sintered at $1210^{\circ}C$ for 1 h in a vacuum atmosphere. The porosities of sintered bodies could be obtained in range of 20~53% by controlling the compaction pressure. Compressive yield strength and hardness were achieved up to 268 MPa and 94 Shore D, respectively. Air permeability was obtained up to $79l/min{\cdot}cm^2$. As a result, mechanical properties and air permeability of the optimized porous body having a porosity of 25~40% were very superior to that of Al alloy.

• 한국재료학회지
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• 제17권6호
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• pp.293-297
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• 2007

Microstructure and tensile strength of the vacuum brazed stainless steel(STS303) and Cu were investigated. For brazing, the BNi-2, 3, 4, 6 and 7 (A.W.S standard) were used as filler metals. The Oxides such as $Cr_2O_3$ and $SiO_2$ were observed at brazed layers between STS303 and Cu matrix. Also, the intermetallic compounds of Cr-B and Ni-P were observed at brazed layers. Brazed STS303-Cu specimens with BNi-2, 3, 4 filler metals showed almost elastic deformation followed by plastic yielding and strain hardening up to a peak stress. On the other hand, it is likely that the fracture of the brazed specimens with BNi-6 and 7 was occurred in elastic range without plastic yielding up to a peak stress. Among these filler metals, the BNi-2 brazed at $1050^{\circ}C$ showed excellent wettability and the highest tensile strength (101.6MPa).

• Journal of Welding and Joining
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• 제16권5호
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• pp.119-133
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• 1998

To implement full automation in pipe welding, it si most important to develop special sensors and their related systems which act like human operator when detecting irregular groove conditions. In this study, an automatic pipe Gas Metal Arc Welding (GMAW) system was proposed to full control pipe welding procedure with intelligent sensor systems. A five-axes manipulator was proposed for welding torch to automatically access to exact welding position when pipe size and welding angle were given. Pool status and torch position were measured by using a weld-pool image monitoring and processing technique in root-pass welding for weld seam tracking and weld pool control. To overcome the intensive arc light, pool image was captured at the instance of short circuit of welding power loop. Captured image was processed to determine weld pool shape. For weld seam tracking, the relative distance of a torch position from the pool center was calculated in the extracted pool shape to move torch just onto the groove center. To control penetration of root pas, gap was calculated in the extracted pool image, and then weld conditions were controlled for obtaining appropriate penetration. welding speed was determined with a fuzzy logic, and welding current and voltage were determined from a data base to correspond to the gap. For automatic fill-pass welding, the function of human operator of real time weld seam control can be substituted by a sensor system. In this study, an arc sensor system was proposed based on a fuzzy control logic. Using the proposed automatic system, root-pass welding of pipe which had gap variation was assured to be appropriately controlled in welding conditions and in torch position by showing sound welding result and good seam tracking capability. Fill-pass welding by the proposed system also showed very successful result by tracking along the offset welding line without any control of human operator.

• Tribology and Lubricants
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• 제30권1호
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• pp.59-63
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• 2014

Laser Surface Texturing(LST) is a surface engineering process used to improve tribological characteristics of materials by creating patterned microstructures on the mechanical contact surface. In LST technology, a pulsated laser beam is used to create arranged dimples on a surface by a material ablation process, which can improve such as load capacity, wear resistances, lubrication lifetime, and reduce friction coefficients. In the present study, the effect of multi-scale LST on lubricant regime was investigated. A pulsed Nd:YAG laser was applied on the bearing steel(AISI 52100) to create arranged dimples. To optimize the surface texturing effect on friction, multi-scale texture dimples with some specific formula arrays were fabricated by combining circles, ellipses and the laser ablation process. The tribological testing of multi-scale textured surface was performed by a flat-on-flat unidirectional tribometer under lubrication and the results compared with that of the non-textured surface. Through an increase in sliding speed, the beneficial effect of multi-scale LST performance was achieved. The multi-scale textured surface had lower friction coefficient performances than the non-textured surface due to the hydrodynamic lubrication effect.

• 한국자기학회지
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• 제4권2호
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• pp.142-149
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• 1994

두께가 0.30 mm, 0.27 mm인 3% 방향성 규소강판에서 표면 선긋기의 간격(39~1.22 mm)과 집합조직(texture) 방향에 대한 선긋기 각도의 변화($90^{\circ}~50^{\circ}$)에 따라 Barkhausen Noise를 측정하였다. 두께 0.27 mm의 시편에서 선긋기를 하지 않았을 때와 선긋기의 간격이 39 mm인 경우 에 대체로 Barkhausen noise envelope은 두개의 peak 현상을 보였으며, 그 현상은 $180^{\circ}$ 자구벽(domain wall)이 생성과 소멸과정을 거듭할 때 많은 activation energy가 필요함에 따른 것으로 설명할 수 있었다. 선긋기 횟수를 늘려감에 따라 즉 선긋기의 간격이 줄어듦에 따라 Barkhausen noise envelope의 크기값이 감소하였지만, 선간격 9.75 mm부터는 감소현상이 둔화되는 것으로 나타났다. 이는 선긋기 획수가 늘어남에 따라 선긋기 근처에서 $180^{\circ}$ 자구의 생성과 소멸이 쉽게 일어나기 때문에 Barkhausen Noise의 크기가 감소하는 것으로 설명할 수 있다. 이러한 현상은 0.30 mm의 시편에서도 유사하게 설명될 수 있었다. Barkhausen noise power는 선긋기 간격이 줄어듦에 따라 감소하였으며, 각도변화에 따른 결과는 $50^{\circ}$ 근처에서 가장 적은 값을 보였다.

• Korean Chemical Engineering Research
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• 제53권1호
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• pp.103-110
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• 2015

본 연구에서는 가스 하이드레이트 기술을 이용하여 철강 공정 배기가스로부터 $CO_2$를 분리하는데 사용하는 여러 촉진제의 성능을 조사하였다. 이 실험에서는 $CO_2/N_2$ 혼합가스 ($CO_2/N_2$=20/80, 40/60)와 $CO_2/N_2$ 이외에 CO, $H_2$가 첨가된 Blast furnace gas (BFG) 모델 가스를 대상 가스로 사용하였다. 촉진제로는 구조 II 하이드레이트를 형성한다고 알려진 tetrahydrofuran (THF), propylene oxide, 1,4-dioxane 를 사용하였으며, 각 가스에 대하여 촉진제를 농도별로 첨가했을 때 상평형점의 변화를 측정하였다. 상평형점은 "연속" Quartz crystal microbalance (QCM) 방식을 이용하였다. 또한, Powder X-ray diffraction (PXRD) 분석을 통하여 촉진제의 첨가가 가스 하이드레이트 구조에 미치는 영향을 알아보았다.