• 제목/요약/키워드: Sampling Tube

검색결과 140건 처리시간 0.019초

작업현장의 환경조건에 따른 방독마스크 정화통의 수명예측 -모사에 의한 정화통과 샘플관의 파과시간- (Prediction of Service Life of a Respirator Cartridge by the Occupational Environment -Simulation of Breakthrough Curve for Respirator Cartridge and Sampling Tube-)

  • 김덕기;신창섭
    • 한국안전학회지
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    • 제11권2호
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    • pp.89-95
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    • 1996
  • To predict the service life of an organic vapor respirator cartridge, the breakthrough curve of respirator was simulated using a fixed-bed adsorption model and compared with that of sampling tube. And the effects of bed porosity, length to diameter ratio and flow rate of the sampling tube were studied. The life time of respirator cartridge was increased with the decrease of particle size and bed porosity. And the breakthrough time of sampling tube was affected by the flow rate, however not by the length to diameter ratio. The 10% breakthrough time of the sampling tube was corresponded with that of cartridge.

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Yoon과 Nelson의 흡착모델을 이용한 방독마스크 정화통의 수명예측(I) (Prediction of Service Life of a Respirator Cartridge for Organic Solvent by Using Yoon and Nelson's Adsorption Model)

  • 김기환;원정일
    • 한국산업보건학회지
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    • 제18권1호
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    • pp.20-31
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    • 2008
  • A respirator is useful to protect a worker from the harmful gases and vapors in the workplace, and the evaluation of respirator cartridge service life is important for the worker's health and safety. The performance of cartridge is effected by several factors such as concentration of gas and vapor, humidity, temperature, adsorbents and cartridge packing density. Adsorption model was applied to both sampling tube and respirator cartridge to predict the service life for organic vapors. The variables of the adsorption model were measured from the experiment with the sampling tube, and it was used to predict the service life of respirator cartridge. In the experiment, we used carbon tetrachloride as a organic vapor and activated carbon take out respirator cartridge as activated carbon. As a result, it was possible to predict the service life of respirator cartridge and predicted service life was quite correct. Breakthrough time decreased with increase of CCl4 concentration. In case of sampling tube, adsorbed amount of CCl4 was larger than respirator cartridge due to linear velocity. Also, rate constant of sampling tube was larger than respirator cartridge, because of, effect of flow rate, packing density. In the prediction of service life of respirator cartridge by using sampling tube, the time required for 50% contaminant breakthrough(${\tau}$) is more effective than the rate constant(k').

점성토 시료추출관이 시료교란에 미치는 영향 (Effect of Thin Wall Tube on Clay Soil Disturbance during Sampling)

  • 임성훈
    • 한국농공학회논문집
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    • 제51권5호
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    • pp.51-58
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    • 2009
  • The total recovery ratio test on undisturbed clay soil sampling in the field and the finite element method analysis on modified static state of penetration process were conducted for the purpose of deciding the most important factor among the shape factors of thin wall tube. The adhesion between tube wall and soil did not decrease although internal clearance ratio of tube increased within the little change of tube area ratio. The most part of disturbance occurred in the tip of sampling tube during the penetration. The longitudinal displacement was larger than the lateral displacement because soil was confined laterally after being entered into tube, and also the longitudinal displacement was larger in the upper part of the sample tube than in the lower part.

전단파를 이용한 쉘비 튜브의 샘플 교란 효과 평가 (Assessing sample disturbance of shelby tube using shear waves)

  • 윤형구;이종섭;김준한;조용순
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2008년도 춘계 학술발표회 초청강연 및 논문집
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    • pp.134-141
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    • 2008
  • To evaluate the engineering properties of soil, the laboratory test always is carried out using samples obtained from the field. There are many studies to estimate the effect of sampling disturbance. The objective of this study appraises the disturbance using the shear wave velocity. The new shelby tube which three transducers are installed every 20cm interval is used. To laboratory tests, the large-scale consolidometer (calibration chamber) is used. During 1cm penetration, the shear wave velocity is measured by every transducer. The initial sampling disturbance is assessed through the velocity difference from bottom to right upside transducer. After finishing the sampling, the velocity is still measured every time to assess the soil disturbance in shelby tube itself. Through the measured velocity, the effect of disturbance is appraised. This study suggests that the sampling disturbance of shelby tube is effectively evaluated using shear wave velocity.

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작업현장의 환경조건에 따른 방독마스크 정화통의 수명예측(II) (Prediction of Service Life of a Respirator Cartridge by the Occupational Environment(II))

  • 김기환;김덕기;신창섭
    • 한국안전학회지
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    • 제11권4호
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    • pp.72-78
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    • 1996
  • The breakthrough curves of a sampling tube were studied to predict the service life of a respirator cartridge for organic vapors. The fixed bed adsorption model was applied to respirator cartridge and it's variables were calculated from tile experiment of sampling tube. By the experiment and simulation, it was possible to predict the service life of a respirator cartridge, however, not adequate at low $CCl_4$ concentration less than 700ppm and at high air humidify. The breakthrough curves of sampling tube were irregular compare to that of respirator cartridge due to .packing density.

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CFCs 조사를 위한 지하수 시료채취방법 비교 및 평가

  • 고동찬;이대하;성현정;강철희;고경석
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2002년도 추계학술발표회
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    • pp.21-23
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    • 2002
  • Two sampling methods for chlorofluorocarbons(CFCs) in groundwater were compared and assessed with groundwater samples in Jeju Island. CFCs concentrations from copper tube method were widely variable among triplicates and higher than those from flame-sealed glass ampule method. For the copper tube method, this is aggravated by rubber packings in the faucet of discharge line of wells, which was removed for the glass ampule method. The poor reproducibility and apparent contamination of results by copper tube method is due to the improper sealing of copper tubes and materials in water discharge line. This suggests that it is more difficult to achieve complete isolation from the atmosphere in the copper tube method and that materials that could release CFCs should be avoided along the sampling flow lines. It seems that the flame-sealed glass ampule method is more relevant for groundwater sampling for CFCs though it requires more complicated equipments and procedures.

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지하수의 CFCs(Chlorofluorocarbons) 조사를 위한 시료 채취 방법의 평가 (Evaluation of Ground-Water Sampling Techniques for Analysis of Chlorofluorocarbons)

  • 고동찬;이대하
    • 한국지하수토양환경학회지:지하수토양환경
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    • 제8권2호
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    • pp.1-8
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    • 2003
  • Chlorofluorocarbons(CFCs) 조사를 위한 지하수 시료 채취 방법 중 cold-welded copper tube method(구리관법)과 flame-sealed borosilicate glass ampule method(유리앰퓰법)의 두 방법을 비교하고 검토하였다. 구리관법에 의해 채취된 시료의 CFCs 농도는 중복시료간에 재현성이 불량한 반면, 유리앰퓰법은 상대표준오차가 5% 이내로 좋은 재현성을 보여주었다. 이것은 구리관법을 적용할 때, 관정의 출수구와 구리관의 연결의 밀봉성이 좋지 않았기 때문인 것으로 추정된다. 또한 구리관법에 의한 CFCs 농도는 전체적으로 유리앰퓰에 의한 값보다 높았으며 이러한 특징은 CFC-11이 CFC-12보다 더 두드러졌다. 구리관법의 경우에 플라스틱 관이나 관정에 설치된 출수구에 포함된 고무 패킹 등이 시료를 CFCs로 오염시켰을 것으로 평가된다. 유리앰퓰법을 적용했을 때에는 이러한 가능성을 제거하기 위해 stainless steel과 nylon 재질만을 이용하고, 시료채취장비를 관정의 주배수관에 직접 연결하였다. 인위적인 공급원에 의한 CFCs가 없을 것으로 예상되는 시료에서 유리앰퓰법에 의해 매우 낮은 수준의 CFCs농도가 측정됨으로써 이 시료채취과정의 유효성이 검증되었다.

공기중 염화비닐단량체의 포집시 공기 포집량이 파과에 미치는 영향 (Effect of sampling volume on the breakthrough of charcoal tube during vinyl chloride monomer sampling)

  • 윤존중;임남구;김치년;노재훈
    • 한국산업보건학회지
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    • 제11권3호
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    • pp.241-248
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    • 2001
  • The main factors of breakthrough are known to sampling time, flow rate, concentration of the sample, temperature, humidity, and the physical characteristics of the solid sorbent tube. However, no study has been reported the effect of temperature and sampling volume on the breakthrough of acharcoal tube during vinyl chloride monomer (VCM) sampling. The objective of this study is to suggest the optimal sampling condition during VCM sampling based on National Institute for Occupational Safety and Health (NIOSH) method. To evaluate adequate sampling volume for VCM without breakthrough, volume of 1, 2, 3, 4, and 5 L each from VCM of 1, 5, 10, 15, and 20ppm at flow rate of 0.05 L/min were sampled in $22^{\circ}C$ and $40^{\circ}C$. At $22^{\circ}C$, in the case of 1, 5, 10, and 15ppm, VCM was adsorbed completely in first section of charcoal tube regardless of sampling volume. But in 20ppm, detection rates are 99.56% in first section and 0.44% in second section. At $40^{\circ}C$ of 1ppm, VCM was adsorbed completely in first section. In 10, 15, and 20ppm, detection rates of second, third, and forth sections were decreased significantly by reduction of sampling volume. In determination of breakthrough based on NIOSH method, no breakthrough was occurred in 20ppm at $22^{\circ}C$. At $40^{\circ}C$, breakthrough was occurred in 10, 15, and 20ppm when sampling volume was 5L. Although no breakthrough was occurred when sampling volume was 3L. Finally, in environment of temperature around $22^{\circ}C$, breakthrough may not occurred up to 20ppm during sampling for VCM. During sampling for VCM in environment of temperature around $40^{\circ}C$, no breakthrough occurred in 1-5ppm and 10-20ppm when sampling volume is 5L and 3L respectively. This result suggests that the sampling volume should be considered when VCM sampling under hot conditions (> $22^{\circ}C$) by the NIOSH method No. 1007.

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대기중 휘발성 유기화합물의 채취 및 분석 방법 비교 (Comparison of Sampling and Analysis Methods for Volatile Organic Compounds in Ambient Air)

  • 나광삼;김용표
    • 한국대기환경학회지
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    • 제14권5호
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    • pp.507-518
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    • 1998
  • A field comparison study was carried out to quantify differences among various sampling and analytical methods for volatile organic compounds (VOCs) at a site in Vlsan in June 1997. Air sampling containers (SUMMA canisters) were used by the Korea Institute of Science and Technology (KIST) and adsorption tubes (carbotrap) were used by Yeungnam University (YN Univ.) for sampling ambient air. Duplicate samples obtained by KIST were analyzed by KIST with a GC-MS system for aromatics and halogenated hydrocarbons and by Atm AA with a GC -FID system for C2∼C9 hydrocarbons, respectively. The adsorption tube samples were analyzed by YN Univ. with a GC-FID system for aromatics. VOC levels for the duplicate canister sampls analyzed by KIST and Atm AA were in good agreement. Concentrations of aromatics by the adsroption tube method were generally higher than those by the canister sampling method by factor of 1.5 to 2.0. Differences between the two sampling methods were discussed.

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공기중 유기용제 혼합물 측정방법의 비교연구 (Comparison of Sampling Methods for Determining Airborne Mixture of Organic Solvents)

  • 천미혜;백남원
    • 한국산업보건학회지
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    • 제1권1호
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    • pp.16-28
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    • 1991
  • A study on comparison of standard charcoal tube method, infrared gas analyzer, and detector tube method were conducted. Measurements were performed simultaneously at same sampling points in an air chamber containing benzene, toluene and xylene vapors. Charcoal tube samles were collected at sampling flowrates of 0.05, 0.2, 0.5, and 1.0 1pm. Results are as follows : 1. Coefficients of variation of results with charcoal tube method for bezene, toluene and xylene mixture vapor were 14.34 % in benzene(0.28-11.12 ppm), 9.20 % in toluene (2.68-135.09 ppm) and 10.21 % in xylene (2.56-82.64 ppm), respectively. 2. Results of infrared gas analyzer in mixture air were non-specific on benzene and toluene. Ratio of results of infrared gas analyzer to those of charcoal tube on benzene, toluene and xylene were 696.4 %, 30.3 % and 36.6 %, respectively. 3. Ratio of responses of detector tubes to those of charcoal tube were 49.4 % in benzene, 22.1 % in toluene and 223.9 % in xylene. Xylene detector tube were interfered by toluene greately. 4. Collection efficiencies of charcoal tubes at low concentraton(benzene : 1 ppm, toluene : 10 ppm, xylene : 10 ppm) were stable on various flowrate from 0.05 to 1.0 1pm, but at high concentrations the efficiency decreased at high flowrate above 0.5 1pm. 5. Within the saturation capacity of charcoal, collection effiency decreased at 0.5-1.0 1pm. Smpling feowrates of 0.05-0.20 1pm were appropriate for sampling organic vapors.

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