• Title/Summary/Keyword: Sample Holder

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X-Ray Diffraction Analysis of Various Calcium Silicate-Based Materials

  • An, So-Youn;Lee, Myung-Jin;Shim, Youn-Soo
    • Journal of dental hygiene science
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    • v.22 no.3
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    • pp.191-198
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    • 2022
  • Background: The purpose of this study was to evaluate the composition of the crystal phases of various calcium silicate-based materials (CSMs): ProRoot white MTA (mineral trioxide aggregate) (WMTA), Ortho MTA (OM), Endocem MTA (EM), Retro MTA (RM), Endocem Zr (EN-Z), BiodentineTM (BD), EZ-sealTM (EZ), and OrthoMTA III (OM3). Methods: In a sample holder, 5 g of the powder sample was placed and the top surface of the material was packed flat using a sterilized glass slide. The prepared slides were mounted on an X-ray diffraction (XRD) instrument (D8 Advance; Bruker AXS GmbH, Germany). The X-ray beam 2θ angle range was set at 10~90° and scanned at 1.2° per minute. The Cu X-ray source set to operate at 40 kV and 40 mA in the continuous mode. The peaks in the diffraction pattern of each sample were analyzed using the software Diffrac (version 2.1). Then, the peaks were compared and matched with those of standard materials in the corresponding Powder Diffraction File (PDF-2, JCPDS International Center for Diffraction Data). A powder samples of the materials were analyzed using XRD and the peaks in diffraction pattern were compared to the Powder Diffraction File data. Results: Eight CSMs showed a similar diffraction pattern because their main component was calcium silicate. Eight CSMs showed similar diffraction peaks because calcium silicate was their main component. Two components were observed to have been added as radiopacifiers: bismuth oxide was detected in WMTA, OM, and EM while zirconium oxide was detected in RM, EN-Z, BD, EZ, and OM3. Unusual patterns were detected for the new material, OM3, which had strong peaks at low angles. Conclusion: It was caused by the presence of Brushite, which is believed to have resulted in crystal growth in a particular direction for a specific purpose.

Electromagnetic Interference Shielding Effectiveness of Hybrid Conductive Fabrics (하이브리드 전도성 직조섬유의 전자파 차폐효과)

  • Han, Gil-Young;Kim, Ki-Yeol;Yun, Tae-Soon
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.14 no.2
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    • pp.81-86
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    • 2015
  • This study investigated electromagnetic interference (EMI) shielding effectiveness (SE) of hybrid conductive fabrics. The coaxial transmission line method was used to measure the EMI Shielding effectiveness of the conductive fabrics. We designed and constructed a measuring system, consisting of a network analyzer and a device that serves as a sample holder and at the same time as a transmission medium of incident electromagnetic waves. The measurements of SE were carried out in a frequency range from 100 MHz to 2 GHz. The results of the EMI shielding experiments showed that the maximum electromagnetic shielding effectiveness (EMSE) values of sandwich type C/A/C (carbon fiber sheet/aluminum foil tape/carbon fiber sheet) and C/Ni/C (carbon fiber sheet/magnetic shielding foil/carbon fiber sheet) samples were 55 dB and 113 dB, respectively, at a frequency of 1.9 GHz.

Construction of Ultrasound Pulsed Doppler Velocimeter (펄스 초음파 도플러 속도계의 제작에 관한 연구)

  • 현석봉;김수용;이재수
    • Progress in Medical Physics
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    • v.5 no.1
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    • pp.25-39
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    • 1994
  • To measure the velocity of heart wall and local flow transctaneously in blood vessels, we have developed a single channel 3.1 MHz pulsed ultrasonic Doppler velocity meter. Ultrasound pluse width and repetition frequency (PRF) used in the velocity meter is 1 ${\mu}$sec 6kHz reapectively, and the Doppler shift of the backscattered echo signal is sensed in a phase detector by coherent demodulation method. From the output of the phase detector, the Doppler signal corresponding to the mean velocity of acoustic wave scatterers over a small region is obtained by using a range gate, sample holder and band-pass filter. Mean frequency of Doppler signal is estimated by zero-crossing counter and the instantaneous velocity of scatters is displayed as a function of time. It is possible to estimate velocity profile, volume flow and flow acceleration of vessels in man if the number of channels and range resolution in increased.

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Measurement of Dielectric Properties of Cereal Grains by Nondestructive Microwave Measurement Technique (마이크로파 비파괴 계측기술을 이용한 곡류의 유전율 측정)

  • Kim, Ki-Bok
    • Journal of the Korean Society for Nondestructive Testing
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    • v.22 no.4
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    • pp.369-376
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    • 2002
  • The dielectric properties of cereal grains such as short-grain rough rice, brown rice and barley with various moisture contents were determined by measuring the attenuation and phase shift of the microwave signal trough the grain samples at 9.5GHz. The microwave free-space transmission measurement system consisted of sample holder, horn antenna and network analyzer. Dielectric constant and loss factor of grain samples increased with moisture content and bulk density and agreed well with previous research results. Moisture density, which is defined as the product of moisture content and bulk density, was proposed as a bulk density and variety compensation factor. The technique for measurement of dielectric properties based on free-space transmission may be useful for other particulate materials.

Technological Experience and Crop Production in Dryland Farming Systems in Africa : The Case of Draught Animal Power in Ghana

  • Panin, Anthony
    • Proceedings of the Korean Society for Agricultural Machinery Conference
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    • 1993.10a
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    • pp.591-600
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    • 1993
  • Considerable controversy exists about the trend of animal traction effects on crop production in dryland farming systems in sub-Saharan Africa (SSA). This problem arises on account of the failure of the few available empirical studies to recognise the important of technological experience of the individual adopting farmers. This study hence addresses this issue by examining the effects of experience in animal traction technology (ATT) on farm size, cropping emphasis, total crop output and farm productivity. It is based on farm management survey data on 42 small holder farm households fro Ghana. Thirty of these households used animal traction technology (ATT) fro crop cultivation and the rest, mainly hand-hoe. The animal traction sub-sample is classified into three groups according to farmers' years of experience with the technology , thus , those with 1-2, 3-10, and more than 10. Evidence from the study shows that the progression of years of experience with ATT leads to inten ification of labour and land use systems, enhancement of degree of motivation to enter into the market economy, increases in total crop output and farm productivity resulting for decreases in cultivated acreages. The implication of the findings is that institutioal and technical support that do accompany the introduction of such technologies should be structured to last for a relatively longer period to accomodate the learning process.

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The Analog-circuited Low-loss Bypass Current Sensing Method for Average Current Mode Control (아날로그 회로로 구현가능한 평균전류제어 저손실 bypass 전류센싱방법)

  • Kim, Seok-Hee;Choi, Byung-Min;Park, Joung-Hu;Jeon, Hee-Jong
    • The Transactions of the Korean Institute of Power Electronics
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    • v.19 no.2
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    • pp.133-138
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    • 2014
  • This paper proposes a low power-loss averaging current mode control using a resistor and bypass switch. Generally, current sensing method using a resistor has a disadvantage of power loss which degrades the efficiency of the entire systems. On the other hand, proposed measurement technique operating with bypass-switch connected in parallel with sensing resistor can reduce power loss significantly the current sensor. An analog-circuited bypass driver is implemented and used along with an average-circuit mode controller. The bypass switch bypasses the sensing current with a small amount of power loss. In this paper, a 50[W] prototype average current mode boost converter has been implemented for the experimental verification.

Fundamental Electro-Mechanical Characteristics of Ballooning-Resistant Bi-2223 HTS Tapes (벌루닝 손상에 강한 Bi-2223 테이프의 기본적인 전기-기계적 특성)

  • Dizon, John Ryan C;Shin, Hyung-Seop;Ha, Dong-Woo;Cho, Jeon-Wook;Oh, Sang-Soo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.11a
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    • pp.26-27
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    • 2006
  • The fundamental mechanical characteristics under tensile and bending deformations of hermetically-sealed reinforced Bi-2223 tape and CTOP processed Bi-2223 tape were examined at 77K. Also, the Tensile strain dependence of the critical current, $I_c$, was obtained at 77K and self-field. The reinforced hermetic tape showed higher tensile strength and a better Tensile strain tolerance than the CTOP processed tape. For bending tests, a rho-shaped sample holder was used giving multiple bending strains. in increasing order. In the same case under bending deformation, the hermetic tape showed a higher bending strain tolerance than the CTOP processed tape. This higher strength of the hermetic tape can be attributed to the thick hardened copper reinforcement layer.

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Development of Disposable Enzyme-linked Immunosensor Strip Platform (일회용 스트립형 효소면역센서용 플랫폼의 개발)

  • Choi, Ji-Hye;Yi, Seung-Jae;Chang, Seung-Cheol;Kim, Kyung-Chun
    • Journal of Sensor Science and Technology
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    • v.20 no.6
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    • pp.400-405
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    • 2011
  • This study introduced the development of a strip type disposable enzyme-linked immunosensor platform for the detection of IgG. Strips of the strip sensor were fabricated by using commercial nitrocellulose filter membranes and a housing holder for the strips was manufactured by using a standard injection molding process for a plastic material. An IgG-urease conjugate was prepared and used for the competitive immune-binding with sample IgG. From the enzymatic reaction between the conjugated urease and urea added, ammonia was generated and caused a localized alkaline pH change on the immobilized antibody band which was coated onto the sensor strips. This pH increase subsequently caused a color change of the antibody band in the presence of a pH indicator, phenol red. Used in conjunction with a competitive immunoassay format, the intensity of the color produced is directly linked with the concentration of target analyte, IgG, and specific measurement of IgG in a lateral flow immunoassay format was achieved over the range 100 ppb to 2000 ppb IgG.

Characterization of Electrostrictive Polyurethane Films for Micro-Actuators (전기왜곡성 폴리우레탄 엑츄에이터의 특성 평가)

  • Jeong, Eun-Soo;Park, Han-Soo;Jeong, Hae-Do;Jo, Nam-Ju;Jae, Woo-Seong
    • Journal of the Korean Society for Precision Engineering
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    • v.19 no.4
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    • pp.161-167
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    • 2002
  • For the purpose of applying to micro-actuator, thermal properties and displacement of electrostrictive polyurethane(PU) elastomers have been measured. In order to understand an effect of PU component, crosslinking agent are controlled by 0.5 wt% and 1 wt%. DMPA and anther chain extenders were used. PU sample that chain extenders are DMPA is added NaOH for comprehension of effect of ionic groups. The deposited electrode sire on PU films is equal to acrylic holder size when the displacement was measured. Dynamic response according to frequency, displacement and recovery time according to PU thickness were measured. 1 wt% crosslinking agent contents PU samples have higher displacement and lower recovery time than 0.5 wt% crosslinking agent contents PU. If the PU thickness is increased, the actuating voltage for generating of same displacement is increased, too.

MOISTURE CONTENT MEASUREMENT OF POWDERED FOOD USING RF IMPEDANCE SPECTROSCOPIC METHOD

  • Kim, K. B.;Lee, J. W.;S. H. Noh;Lee, S. S.
    • Proceedings of the Korean Society for Agricultural Machinery Conference
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    • 2000.11b
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    • pp.188-195
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    • 2000
  • This study was conducted to measure the moisture content of powdered food using RF impedance spectroscopic method. In frequency range of 1.0 to 30㎒, the impedance such as reactance and resistance of parallel plate type sample holder filled with wheat flour and red-pepper powder of which moisture content range were 5.93∼-17.07%w.b. and 10.87 ∼ 27.36%w.b., respectively, was characterized using by Q-meter (HP4342). The reactance was a better parameter than the resistance in estimating the moisture density defined as product of moisture content and bulk density which was used to eliminate the effect of bulk density on RF spectral data in this study. Multivariate data analyses such as principal component regression, partial least square regression and multiple linear regression were performed to develop one calibration model having moisture density and reactance spectral data as parameters for determination of moisture content of both wheat flour and red-pepper powder. The best regression model was one by the multiple linear regression model. Its performance for unknown data of powdered food was showed that the bias, standard error of prediction and determination coefficient are 0.179% moisture content, 1.679% moisture content and 0.8849, respectively.

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