• 한국전자현미경학회:학술대회논문집
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• 한국현미경학회 2001년도 제32차 추계학술대회
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• pp.18-22
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• 2001

A technique to characterize specific site of materials using a combination of a dedicated focused ion beam system(FIB), and Intermediate-voltage scanning transmission electron microscope(STEM) or transmission electron microscope(TEM) equipped with a scanning electron microscope(SEM) unit has been developed. The FIB system is used for preparation of electron transparent thin samples, while STEM or TEM is used for localization of a specific site to be milled in the FIB system. An FIB-STEM(TEM) compatible sample holder has been developed to facilitate thin sample preparation with high positional accuracy Positional accuracy of $0.1{\mu}m$ or better can be achieved by the technique. In addition, an FIB micro-sampling technique has been developed to extract a small sample directly from a bulk sample in a FIB system These newly developed techniques were applied for the analysis of specific failure in Si devices and also for characterization of a specific precipitate In a metal sample.

• 한국CDE학회논문집
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• 제10권5호
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• pp.365-374
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• 2005

Most of people who are engaged in research and development find it difficult to solve the engineering problems creatively due to the lack of ideas. TRIZ is one of the emerging problem solving techniques that leads us to a very useful and clear solution. TRIZ consists of several tools such as ideal final result (IFR), physical and technical contradictions, 40 invention principles, resource, effect, etc. However, many designers think that TRIZ is hard to be applied to a design problem since there are several tools in TRIZ. Machine designers may want to see which tool is more effective than others. Thus, this paper provides sample solutions of a design problem: holder design for the bottle etching machine by applying several TRIZ tools. Difficulties in applying TRIZ to a design problem are discussed.

• 한국산업보건학회지
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• 제23권4호
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• pp.348-355
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• 2013

Objectives: In working environment measurement, sampling is an important stage for obtaining reliable result as analysis. A personal air sampling pump is one of the most fundamental and important element in the work environment measurement, but it remains at the level of calibrating the flow rate of the pump before and after sampling. There is no checking whether the flow rate set at the initial stage would be hold during sampling. The purpose of this study was to develop a method to evaluate the flow rate performance of particulate sampling pump with three-pieces cassette holder containing filters commonly used to sample particulate. Materials and methods: We tested back pressure of particulate sampling pumps commonly used in Korea with three-pieces cassette holder containing various filters, and tried to find out the combination conditions of filters in accordance with back pressure required by ISO standard 13137. Results: We found out the matrix of sampling media such as three-pieces cassette holder containing filters applicable to the pressure drop required by the ISO standard for evaluating the flow rate stability under increasing pressure drop and long term(8 hour) performance. Conclusions: This evaluation method using sampling media matrix for checking flow rate stability proposed by this study could be very useful tool to find out good performance pumps before sampling.

• 한국산업보건학회지
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• 제19권2호
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• pp.81-87
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• 2009

Final purpose of this study was designed to develop the quality control(QC) sample for proficiency analytical testing of asbestos. This study consisted of two parts; first, development of manufacturing apparatus and sample preparing procedure for asbestos quality control(QC) sample: second, validation of the QC samples made by our developed method as asbestos proficiency analytical testing sample. The main results of the first part research are as followed We developed the apparatus for manufacturing the asbestos QC sample, consisted of filter hold, filter holder manifolder, vacuum system, and vacuum pump. The most proper filter of making the QC samples was a cellulose ester membrane filter with 25 mm diameter, pore size 0.8 um. And we presented the optimal procedure for preparing the asbestos QC sample by using the developed apparatus. We will verify the manufactured asbestos QC samples by this method, and present the validation results to confirm the reliability as a asbestos QC sample in next paper.

• 산업기술연구
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• 제23권A호
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• pp.21-27
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• 2003

The bio-micro pin is usually used for biochemistry analysis. The capability of manufacturing the micro-pin and array with effective and low-cost way is very important to developers. The micro-pin is composed of "sample channel" putting liquid into already fixed volume, "flat tip" having connection with printing quantity, and "head part" for preventing it from rotation of pin in the holder. We analyzed out printing variation in accordance with shape and tip size of the micro-pin point channel, In this study, we suggested the manufacturing progress and shape demand condition of the micro-pin which could put $0.2{\mu}{\ell}$-biochemistry material into the sample volume, and will be able to produce the micro-pin which can put $10n{\ell}$-biochemistry material into the sample volume in the future.

• 대한전자공학회:학술대회논문집
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• 대한전자공학회 2003년도 하계종합학술대회 논문집 I
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• pp.310-313
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• 2003

Complex permittivities of human head simulating liquids were measured by a sample holder of terminated slotted coaxial line with a movable probe at mobile communication frequencies. The validity of the liquid measurement system was checked by experiments with the reference liquids. Liquids of ingredients for human brain suggested in IEEE draft and those made by the authors were measured by this slotted line system.

• 분석과학
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• 제19권5호
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• pp.407-414
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• 2006

An X-ray diffractometer for spatially resolved X-ray diffraction measurements was developed to identify phase in the narrow (micron-scaled) region of high burn-up fuels and some nuclear materials. The micro-XRD was composed of an X-ray microbeam alignment system and a sample micro translation system instead of a normal slit and a fixed sample stage in a commercial XRD. The X-ray microbeam alignment system was fabricated with a microbeam concentrator having two Ni deposited mirrors, a vertical positioner, and a tilt table for the generation of a concentrated microbeam. The sample micro translation system was made with a sample holder and a horizontal translator, allowing movement of a specimen at $5{\mu}m$ steps. The angular intensity profile of the microbeam generated through a concentrator was symmetric and not distorted. The size of the microbeam was $4,000{\times}20{\mu}m$ and the spatial resolution of the beam was $47{\mu}m$ at the sample position. When the diffraction peaks were measured for a $UO_2$ pellet specimen by this system, the reproducibility ($2{\Theta}={\pm}0.01^{\circ}$) of the peaks was as good as a conventional X-ray diffractometer. For the cross section of oxidized titanium metal, not only $TiO_2$ in an outer layer but also TiO near an oxide-metal interface was observed.

• 대한기계학회논문집A
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• 제26권3호
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• pp.537-543
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• 2002

This paper examines a new in-process measurement system for the measurement of micro-defects on the surfaces of brittle materials by using the AFM (Atomic Force Microscopy). A new AFM scanning stage that can also perform nano-scale bending of the sample was developed by adding a bending unit to a commercially available AFM scanner. The bending unit consists of a PZT actuator and sample holder, and can perform static and cyclic three-point bending. The true bending displacement of the bending unit is approximately 1.8mm when 80 volts are applied to the PZT actuator. The frequency response of the bending unit and the stress on the sample were also analyzed, both theoretically and experimentally. Potential surface defects of the sample were successfully detected by this measurement system. It was confirmed that the number of micro-defects on a scratched surface increases when the surface is subjected to a cyclic bending load.

• 한국항해학회지
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• 제15권1호
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• pp.1-9
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• 1991

The coaxial sample holder with 20mm in diameter and the adaptor from type N connector-to-20mm${\phi}$ coaxial tube are designed and manufactured which have been used for designing and measuring the fabricated microwave absorber. In addition, the measure in method of material constants of the microwave absorbers is described, which is focused on minimizing the error due to the sample's shapes, the fitting conditions, etc. After describing the design method of a single-layed microwave absorber, the microwave absorbers for X-band, C-band and S-band RADARs are designed and fabricated, respectively, which are composed of ferrite, carborn, and binder and have good performance. Futhermore, we develop the high performance microwave absorber in extremely wide-band type for RADAR, which is composed of different material and its mixing ratio and which could cover nearly from 4 to 10 GHz.

• 반도체디스플레이기술학회지
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• 제2권4호
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• pp.23-26
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• 2003

The general users find difficulties in using ellipsometers. Thus, the object of this study is to construct an ellipsometer with simple operation principle. We developed an ellipsometer which does not require alignment and calibration before measuring sample. A basis structure model after rotating a compensator spectroscopic ellipsometry, the fixed incidence angle at $70^{\circ}$. This ellipsometer does not demand calibration, because the plane of incidence is not changed due to the novel sample holder structure. The results for various standard samples were compared with those from conventional RCSE to test the performance of this instrument. Also repeated measurements were performed to test the precision of the calibration coefficient in a plane of incidence fixed.