• 동력기계공학회지
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• 제15권3호
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• pp.58-64
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• 2011

As well known, the friction stir welding is a novel welding process which is a solid state welding process for sheet or plate using the friction stir phenomenon. This paper describes the effect of welding condition such as the rotation speed and the travelling speed during the friction stir welding process on the micro Virkers hardness and the microstructure of friction stir welded joints in AI-7075-T651 plate. From those investigations, the highest hardness of stir zone was observed at the welding condition of SO-3. The microstructures of the friction stir welded joints was not dependent on the welding conditions, but in the SO-4 specimen, the friction stir welding defect like tunnel shape was found in stir zone.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2002년도 Proceedings of the International Welding/Joining Conference-Korea
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• pp.499-504
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• 2002

The microstructural change associated with the hardness profile in friction stir welded, age-hardenable 6005 Al alloy had been evaluated. Frictional heat and plastic flow during friction stir welding created the fine recrystallized grain (Stir Zone, SZ), the elongated and recovered grain (Thermo-Mechanical Affected Zone, TMAZ) in the weld zone. Heat affected zone (HAZ), which could be only identified by hardness test because there is no difference in the grain structure compared with that of the base metal, was formed beside the weld zone. A softened region had been formed near the weld zone during friction stir welding process. The softened region was characterized by the dissolution and coarsening of the strengthening precipitate during the friction stir welding. The sound joints of 6005 Al alloys were successfully formed under a wide range of the friction stir welding conditions.

• 한국유기농업학회지
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• 제23권4호
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• pp.987-997
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• 2015

오미자의 포제방법에 따른 생리활성 변화를 비교하기 위해 항산화 활성을 평가하였다. 항산화 활성 평가를 위해 총 폴리페놀 및 플라보노이드 함량 측정, DPPH radical 소거활성, ABTS radical 소거활성 그리고 환원력을 측정하였다. 총 폴리페놀 함량은 포제처리를 하지 않은 오미자에 비해 청초 전처리, 주정 전처리를 한 오미자 모두 함량이 증가하였고 $220^{\circ}C$에서 12분 동안 청초 전처리를 하였을 때 가장 높게 증가하였으며 플라보노이드 함량에서도 폴리페놀 함량과 유사한 결과를 나타냈다. DPPH radical 소거활성에서는 $220^{\circ}C$에서 처리하였을 때 생오미자 보다 활성이 증가하였으며 12분 동안 처리된 청초오미자에서 효과적이었다. ABTS radical 소거활성에서는 $140^{\circ}C$에서 3분 동안 처리한 청초오미자의 활성이 효과적으로 나타났고 환원력을 측정한 결과 생오미자, 청초 전처리, 주정 전처리에서의 활성 차이는 미비하였으나 비교적 $220^{\circ}C$에서 12분간 처리를 하였을 때 가장 효과적이었다. 이 결과는 포제처리 과정 중 열에 의한 오미자의 약리성분이 변화됨으로써 생리활성 변화에 기인한 것으로 판단되어진다. 따라서, 오미자의 항산화 활성은 비교적 청초 전처리에서 효과적이었으며 $220^{\circ}C$에서 12분간 처리하였을 때 가장 효과적으로 활성이 증가함을 확인하였다.

• Journal of Welding and Joining
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• 제30권5호
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• pp.34-39
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• 2012

This study was conducted to investigate the microstructure and mechanical properties of friction stir lap joints. Invar 42 and SS 400 were selected as the experimental materials, and friction stir welding was carried out at a tool rotation speed of 200 rpm and welding speed of 100 mm/min. The application of friction stir welding to Invar 42 effectively reduced the grain size in the stir zone; the average grain size of Invar 42 was reduced from $11.5{\mu}m$ in the base material to $6.4{\mu}m$ in the stir zone, which resulted in an improvement in the mechanical properties of the stir zone. The joint interface between Invar 42 and SS 400 showed a relatively sound weld without voids and cracks, and the intermetallic compounds with $L1_2$ type in lap jointed interface were partially formed with size of 100 nm. Moreover, the hook in the advancing side of Invar 42 was formed from SS 400, which contributed to maintenance of the tensile strength. The evolution of microstructures and mechanical properties of friction stir lap jointed Invar 42 and SS 400 are also discussed herein.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2009년도 춘계학술대회 논문집
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• pp.242-243
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• 2009

Friction stir welding and friction stir processing is a new solid state processing technique for ioining and micro..structural modification in metallic materials. It has been applied not only joining for light metals but also modification of the microstructure to enhance mechanical properties. In thin study, we investigated the mechanical properties for applied friction stir welding and processing under various parameters such as probe diameter, probe type, traveling speed and rotating speed for 5456-H116 AI allov. As a result of experiments, optimum condition of friction stir welding is traveling speed of 15mm/min, rotating speed of 500RPM at 6mm diameter probe. Moreover, in the case of friction stir processing, the optimum condition is traveling speed of 15mm/min, rotating speed of 250RPM at full screw probe. As above mentioned, the mechanical characteristics enhanced with the decreasing of traveling speed and the increasing of friction areas because of plastic flow due to high friction heat. These result can be used as reference data for ship repairment.

• 소성∙가공
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• 제24권4호
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• pp.256-263
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• 2015

Electric resistance spot welding has been used to join overlapped steel sheets in automotive bodies. Recently to reduce weight in automotive vehicles, non-ferrous metals are being used or considered in car bodies for hoods, trunk lids, doors parts, etc. Various welding processes such as laser welding, self-piercing rivet, friction stir welding are being used. In the current study, a new electric resistance heated friction stir spot welding is suggested for the spot welding of non-ferrous metals. The welding method can be characterized by three uses of heat -- electric resistance heating, friction stir heating and conduction heating of steel electrodes -- for the fusion joining at the interfacial zone between the two sheets. The welding process has variables such as welding current, diameter of the steel electrodes, revolutions per minute (rpm) of the friction stir pin, and the insert depth of the stir pin. In order to obtain the optimal welding variables, which provide the best welding strength, many experiments were conducted. From the experiments, it was found that the welding strength could be reached to the required production value by using an electrode diameter of 10mm, a current of 7.6kA, a stirring speed of 400rpm, and an insert depth of 0.8mm for the electric resistance heated friction stir spot welding of 5052 aluminum 1.5mm sheets.

• 한국재료학회지
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• 제22권3호
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• pp.123-129
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• 2012

The microstructures and mechanical properties of friction stir welded lap joints of Inconel 600 and SS 400 were evaluated; friction stir welding was carried out at a tool rotation speed of 200 rpm and welding speed of 100 mm/min. Electron back-scattering diffraction and transmission electron microscopy were introduced to analyze the grain boundary characteristics and the precipitates, respectively. Application of friction stir welding was notably effective at reducing the grain size of the stir zone. As a result, the reduced average grain size of Inconel 600 ranged from $20{\mu}m$ in the base material to $8.5{\mu}m$ in the stir zone. The joint interface between Inconel 600 and SS 400 showed a sound weld without voids and cracks, and MC carbides with a size of around 50 nm were partially formed at the Inconel 600 area of lap joint interface. However, the intermetallic compounds that lead to mechanical property degradation of the welds were not formed at the joint interface. Also, a hook, along the Inconel 600 alloy from SS 400, was formed at the advancing side, which directly brought about an increase in the peel strength. In this study, we systematically discussed the evolution of microstructures and mechanical properties of the friction stir lap joint between Inconel 600 and SS 400.

• Journal of Welding and Joining
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• 제20권3호
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• pp.67-73
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• 2002

In an attempt to evaluate the feasibility of friction stir welding(FSW) for joining carbon steels, microstructures and mechanical properties of friction stir welded carbon steels with different grain structures were investigated. In comparison of O-type stir zone(SZ) appeared in various aluminium alloys, configuration of SZ in friction stir welded carbon steels displayed U-type. Plastically deformed pearlite band structure was identified to surround the SZ, indicating the existence of so-called thermo-mechanically affected zone(TMAZ). However, the TMAZ of carbon steels was much narrower than that of Al alloys. The microstructures of both stir zone and TMAZ revealed bainite matrix in a conventional carbon steel for shipbuilding, while, in the same region, ferrite matrix microstructures were formed in a low carbon fine grained steel. The conventional carbon steel showed superior stirring workability to that of the fine grained carbon steel. The yield and tensile strength of the friction stir welded joints were comparable to those of the base metals, and the elongation in welded joints demonstrated excellent ductility. Absorbed energy in SZ of the fine grained carbon steel was ten times higher than that obtained from conventional submerged arc weld metal of the same steel. Based on these results, the application FSW to carbon steels was found to be feasible.

• 한국재료학회지
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• 제21권7호
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• pp.410-414
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• 2011

This study was carried out to evaluate the microstructures and mechanical properties of a friction stir welded Ni based alloy. Inconel 600 (single phase type) alloy was selected as an experimental material. For this material, friction stir welding (FSW) was performed at a constant tool rotation speed of 400 rpm and a welding speed of 150~200 mm/min by a FSW machine, and argon shielding gas was utilized to prevent surface oxidation of the weld material. At all conditions, sound friction stir welds without any weld defects were obtained. The electron back-scattered diffraction (EBSD) method was used to analyze the grain boundary character distributions (GBCDs) of the welds. As a result, dynamic recrystallization was observed at all conditions. In addition, grain refinement was achieved in the stir zone, gradually accelerating from 19 ${\mu}m$ in average grain size of the base material to 5.5 ${\mu}m$ (150 mm/min) and 4.1 ${\mu}m$ (200 mm/min) in the stir zone with increasing welding speed. Grain refinement also led to enhancement of the mechanical properties: the 200 mm/min friction stir welded zone showed 25% higher microhardness and 15% higher tensile strength relative to the base material.

• 대한방사선기술학회지:방사선기술과학
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• 제33권1호
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• pp.45-50
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• 2010

본 연구는 T2고속스핀에코 3.0T 자기공명영상에서 지방조직 소거기법인 SPAIR와 STIR기법의 임상적 유용성에 관한 비교연구를 시행하였다. SPAIR와 STIR 프로토콜을 사용하여 뇌의 축방향 영상(20개), 요추의 시상단면영상(20개), 고관절의 관상단면영상(17개), 무릎관절의 축방향 영상(25개)을 획득하였다. 검사부위별로 지방억제기법의 지방소거능력과 화질을 파악하기위해 지방조직의 신호강도와 불균일성을 측정하였다. 지방조직에서 불균일치는 측정된 지방 신호의 평균치(mean)에 대한 표준편차(SD)로서 그 산출은 SD/mean으로 계산하였다. 수집된 자료는 SPSS(Statistical Package for the Social Science) WIN 13.0 프로그램을 이용하여 분석한 결과 다음과 같은 결론을 얻었다. 첫째, 뇌 검사는 SPAIR가 STIR보다 지방억제능력과 화질면에서 우수한 결과를 나타냈으며, 둘째, 요추, 고관절, 무릎관절 검사는 지방의 신호억제능력은 STIR가 우수하고, 화질면에서는 SPAIR가 우수한 결과를 나타냈다.