• Title/Summary/Keyword: SEM images

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Positron Annihilation Study of Vacancy Type Defects in Ti, Si, and BaSrFBr:Eu

  • Lee, Chong Yong
    • Applied Science and Convergence Technology
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    • v.25 no.5
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    • pp.85-87
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    • 2016
  • Coincidence Doppler broadening and positron lifetime methods in positron annihilation spectroscopy has been used to analyze defect structures in metal, semiconductor and polycrystal, respectively. The S parameter and the lifetime (${\tau}$) value show that the defects were strongly related with vacancies. A positive relationship existed between the scanning electron microscope (SEM) images and the positron annihilation spectroscopy (PAS). According to the SEM images and PAS results, measurements of the defects with PAS indicate that it was more affected by the defect than the purity.

Analysis of the Electrical Defect Detection Mechanism using a Low Energy Electron Beam on the TFT Substrate for TFT-LCDs (TFT-LCD용 TFT기판에서 저에너지 전자빔을 이용한 전기적 결함 검출 메카니즘 분석)

  • Oh, Tae-Sik;Kim, Ho-Seob;Kim, Dae-Wook;Ahn, Seung-Joon;Lee, Gun-Hee
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.12 no.4
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    • pp.1803-1811
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    • 2011
  • We have analyzed the electrical defect detection mechanism using low energy microcolumn on the TFT substrate for TFT-LCD. In this study, we have acquired the SEM images of the various pixel defects for 7-inch TFT substrate by scanning of low energy electron beam in the high vacuum chamber. Futhermore, we have interpreted the defect detection mechanism through the correlations between the SEM images and electrical behaviors of the defective pixels. As a result, we obtained consistent results as the follows. We can confirm that the SEM images using low energy electron beam are significantly affected by the space charge effect.

Images of deposited layers of organic light-emitting diodes observed by scanning-electron microscope (주사 전자 현미경으로 관찰한 유기 발광 소자의 누적층 모양)

  • Lee, Eun-Hye;Yoon, Hee-Myoung;Han, Wone-Keun;Kim, Tae-Wan;Lee, Won-Jae;Jang, Kyung-Uk;Ahn, Joon-Ho
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.298-299
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    • 2008
  • Images of deposited layers of organic light-emitting diodes were observed by scanning-electron microscope (SEM). We were able to see a clear cross-sectional view of deposited layers. The SEM is a type of electron microscope that images the sample surface by scanning it with a high-energy beam of electrons in a raster scan pattern. A thickness of deposited layer measured by thickness monitor is close to a real value measured by a-step surface profiler within 5%. We were able to see a formation of domains of size about 50-100nm from a surface morphology of Al, and pin holes of size about 50nm.

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Log-based petrophysical analysis of Khatatba Formation in Shoushan Basin, North Western Desert, Egypt

  • Osli, Liyana Nadiah;Yakub, Nur Yusrina;Shalaby, Mohamed Ragab;Islam, Md. Aminul
    • Geosciences Journal
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    • v.22 no.6
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    • pp.1015-1026
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    • 2018
  • This paper aims to investigate the good reservoir quality and hydrocarbon potentiality of the Khatatba Formation, Qasr Field in the Shoushan Basin of the North Western Desert, Egypt by combining results from log-based petrophysical analysis, petrographic description and images from scanning electron microscope (SEM). Promising reservoir units are initially identified and evaluated through well log analysis of three wells in the field of study. Petrophysical results are then compared with petrographic and SEM images from rock samples to identify features that characterize the reservoir quality. Well log results show that Khatatba Formation in the study area has good sandstone reservoir intervals from depths ranging from 12848 ft to 13900 ft, with good effective porosity records of 13-15% and hydrocarbon saturations of greater than 83%. Petrographic analysis of these sandstone reservoir units indicate high concentrations of vacant pore spaces with good permeability that can be easily occupied by hydrocarbon. The availability of these pore spaces are attributed to pore-enhancing diagenetic features, mainly in the form of good primary porosity and dissolution. SEM images and EDX analysis confirmed the presence of hydrocarbon, therefore indicating a good hydrocarbon-storing potential for the Khatatba Formation sandstones.

Development of membrane blend using casting technique for water desalination

  • El-Gendi, A.;Ali, S.S.;Ahmed, S.A.;Talaat, H.A.
    • Membrane and Water Treatment
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    • v.3 no.3
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    • pp.201-209
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    • 2012
  • Membrane separation technologies have some of advantages are considered a better alternative to traditional methods. Research of novel membranes is very vital for covering the higher required of membrane in several purposes like water desalting technology. In this work polyamide-6/cellulose acetate (PA-6/CA) blend membrane was developed according to the wet phase inversion system. The structures of the prepared membranes were examined by scanning electron microscopy (SEM). SEM images showed uniform particles distribution in the prepared membranes. Moreover, SEM images revealed that the membranes have relatively uniform surface (PA-6/CA). PA-6/CA blend membranes systems are evaluated by using synthetic NaCl solution. The separation performance showed that salt rejection increased with increasing of heat treatment of the casted films and it was improved with increasing of operating pressure.

Accelerating Effect of Organic Acid Treatment on Weight Reduction Characteristics of Sea-Island Type PET Supermicrofiber (1) (유기산 처리가 해도형 초극세 폴리에스터 섬유의 용출 특성에 미치는 영향 (1))

  • Kim, Hea-In;Jeong, Cheon-Hee;Min, Mun-Hong
    • Textile Coloration and Finishing
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    • v.24 no.1
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    • pp.45-53
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    • 2012
  • In order to make a supermicrofiber fabric with PET/co-PET sea-island type filament fiber, the optimum conditions of dissolution of co-PET composite filament fiber was examined. The data set was made at various organic acid concentration and steam temperature with treated time as a main variable. At the same time, the microstructure changes by organic acid treatment of sea-island type PET supermicrofibers were monitored by thermal analysis morphology, DSC thermgrams and SEM images. Weight reduction behavior of supermicrofibers by caustic treatment was investigated in a comparative method. The termination of dissolution was also confirmed using DSC thermgrams and SEM images.

Stem cell behaviors on periodic arrays of nanopillars analyzed by high-resolution scanning electron microscope images

  • Jihun Kang;Eun-Hye Kang;Young-Shik Yun;Seungmuk Ji;In-Sik Yun;Jong-Souk Yeo
    • Applied Microscopy
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    • v.50
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    • pp.26.1-26.3
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    • 2020
  • The biocompatible polyurethane acrylate (PUA) nanopillars were fabricated by soft lithography using three different sizes of nanobeads (350, 500, and 1000 nm), and the human adipose-derived stem cells (hASCs) were cultured on the nanopillars. The hASCs and their various behaviors, such as cytoplasmic projections, migration, and morphology, were observed by high resolution images using a scanning electron microscope (SEM). With the accurate analysis by SEM for the controlled sizes of nanopillars, the deflections are observed at pillars fabricated with 350- and 500- nm nanobeads. These high-resolution images could offer crucial information to elucidate the complicated correlations between nanopillars and the cells, such as morphology and cytoplasmic projections.

Biomedical Applications of Stereoscopy for Three-Dimensional Surface Reconstruction in Scanning Electron Microscopes

  • Kim, Ki Woo
    • Applied Microscopy
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    • v.46 no.2
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    • pp.71-75
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    • 2016
  • The scanning electron microscope (SEM) offers two-dimensional (2D) micrographs of three-dimensional (3D) objects due to its inherent operating mechanisms. To overcome this limitation, other devices have been used for quantitative morphological analysis. Many efforts have been made on the applications of software-based approaches to 3D reconstruction and measurements by SEM. Based on the acquisition of two stereo images, a multi-view technique consists of two parts: (i) geometric calibration and (ii) image matching. Quantitative morphological parameters such as height and depth could be nondestructively measured by SEM combined with special software programs. It is also possible to obtain conventional surface parameters such as roughness and volume of biomedical specimens through 3D SEM surface reconstruction. There is growing evidence that conventional 2D SEM without special electron detectors can be transformed to 3D SEM for quantitative measurements in biomedical research.

Preparation and Characteristics of Polyethersulfone Microfiltration Membranes (폴리에테르술폰 정밀여과막의 제조 및 특성 연구)

  • Kim, No-Won
    • Membrane Journal
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    • v.17 no.4
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    • pp.329-337
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    • 2007
  • This is the research about a new method to make the internal separation layer with smallest pore size in polyethersulfone (PES) membrane by adding p-toluenesulfonic acid (TSA) and polyvinylpyrolidone (PVP) to polymeric PES solution. The preparation and morphological characterization of PES sheet membranes containing PVP as a hydrophilic swelling material and TSA as a demixing material were performed. As a result by microflow porometery, the PVP and TSA added PES membranes showed good permeabilities and narrow pore size distributions, comparable to those of the commercial membranes. The concentration of PVP affected the PES characteristics on air permeability and surface structure. The concentration of TSA influenced on pore size distribution but do not affect air permeability. The surface images of FE-SEM shows similar pore size when TSA added or not. However, the cross-section images of FE-SEM show that the TSA added PES membranes have a increase of internal layer thickness with smallest pore size.

The Effect of Electron Beam Irradiation on Chemical and Morphological Properties of Hansan Ramie Fibers

  • Lee, Jung Soon
    • Fashion & Textile Research Journal
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    • v.15 no.3
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    • pp.430-436
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    • 2013
  • The purpose of this study investigates the effects of electron beam(EB) irradiation on the chemical and morphological properties of Hansan ramie fiber. Hansan ramie fibers were irradiated with electron beam doses of 0, 1, 3, 5 and 10kGy. The effect of electron beam irradiation on the chemical components of fibers as well as the surface chemical and morphological properties were investigated using chemical component analysis methods based on TAPPI standards, XPS, and SEM. The results indicate that the surface layers can be removed under suitable EB irradiation doses. Alcohol-benzene extraction and lignin content increases gradually with an increase in EB irradiation and reaching a maximum at an EB dose of 3kGy, and decreases at 10kGy. The surface chemical changes measured by XPS corresponded to the chemical composition analysis results. The C1 peak and the O/C ratio decreased with the removal of the multi-layer and primary layer by EB irradiation. The SEM images show the inter-fibrillar structure etched by EB irradiation up to 5kGy. At 10kGy, the surface structure of the ramie fiber shows highly aligned and distinctive striations in a longitudinal direction. The removal of these exterior layers of the fiber was confirmed by changes in surface morphology as observed in SEM images.