• Title/Summary/Keyword: SEM Image

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A Study on the Preparation of Tungsten Oxide powders Using Emulsion Evaporation Methods (에멀젼 증발법에 의한 산화텅스텐 분말의 제조에 관한 연구)

  • 신창훈;안종관;이응조
    • Journal of the Korean Ceramic Society
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    • v.35 no.6
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    • pp.543-550
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    • 1998
  • A process for the preparation of spherical tungsten oxide powders by the emulsion evaporation method was developed. The characteristics of the powders thus prepared were examined by means of TGA X-ray diffraction SEM and image analysis. The emulsion was prepared by fast mixing of tungsten containing aque-ous phase and the organic phase which contained kerosene surfactant and paraffin oil. The precursor was made by evaporating the emulsion in the kerosene bath at $160^{\circ}C$ and then calcined at $650^{\circ}C$ in order to pro-duce tungsten oxide powders. The average particle size of the tungsten oxide powders was $0.5\;\mu\textrm{m}$ and their shapes were spherical. Water-in-oil type emulsion wasmore advantageous to make less agglmerated. $W_{3}$ powders than the oil-in-water type emulsion for the emulsion evaporation experiments. As the HLB value of the surfactant increased and the concentration of tungsten ions in the aqueous phase decreased the mean particle size of tungsten oxide powders decreased whereas agglomeration increased. The optimum con-centration of Span 80 was 8 percent by volume and the optimum stirring speed in the emulsion formation was 5000 rpm in order to obtain find less agglomerated $W_{3}$ powders.

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A Study on the Characteristics of Linear Smoothing Algorithm for Image-Based Object Detection of Water Friendly Facilities in River (영상 기반의 하천 친수시설 추출을 위한 선형 평활화 알고리즘 특성 연구)

  • Im, Yun Seong;Kim, Seo Jun;Kim, Chang Sung;Kim, Seong Jun
    • Ecology and Resilient Infrastructure
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    • v.8 no.4
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    • pp.266-272
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    • 2021
  • Water friendly space refers to a place designated to plan and manage spaces for residents Water friendly activities. Efficient management of river Water friendly parks requires automated GIS data and DB construction of the water friendly facilities. Object-based classification using drone images or aerial images is attracting attention as an efficient means to acquire 3D spatial information in the country. To remove the miscellaneous image included in the extracted outline, a linear simplification of the outline is required, and it is difficult to apply manually, so various automation methods have been developed to overcome this, and among them, the most widely studied and utilized is the linear simplification method. In this study, the suitability of linear simplification algorithms such as Douglas-Peucker, Visvalingam-Whyatt, and Bend-simplify algorithms for the geometric shape of hydrophilic facilities was determined.

The Effects of the Favorability of Korean Food on the Favorability of Korean Wave, Country Image, and Visit Intention to Korea : Focused on Young Vietnamese (한식콘텐츠 이용 경험자에게 형성된 한식호감도가 한류호감도, 국가이미지, 한국 방문의도에 미치는 영향 : 베트남 2030세대를 중심으로)

  • Lee, Jisun;Chung, Lana
    • The Journal of the Korea Contents Association
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    • v.17 no.7
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    • pp.320-331
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    • 2017
  • The purpose of this study was to explore the effects of Korean food contents influence to the Korean wave favorability, country image, and visit intention to Korea. Korean food contents are defined as that information or contents related with Korea food. In this survey, total 4 type of Korean food contents, Korean food recipe contents, Korean food culture story contents, Korean food restaurant guide contents and Korean food media contents were explained. The respondents were 147 young Vietnamese in residing in Ho Chi Minh city. The data were analyzed by PLS-SEM to explore influence of Korean food favorability with Korean food contents usage. After using Korean food contents, Korean food favorability influence country image and visit intention to Korea, mediating with Korean wave favorability. While Korean food favorability was not shown to influence visit intention directly. This study would contribute to make strategic Korean food contents and distribution, further accord with Hansik Globalization.

Importance of Impregnation and Polishing for Backscattered Electron Image Analysis for Cementitious Self-Healing Specimen (시멘트계 자기치유 시편에 대한 반사전자현미경 이미지 분석을 위한 함침과 연마의 중요성)

  • Kim, Dong-Hyun;Kang, Kook-Hee;Bae, Seung-Muk;Lim, Young-Jin;Lee, Seung-Heun
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.5 no.4
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    • pp.435-441
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    • 2017
  • Studies on self-healing have currently been diversified and the methods to evaluate the studies have become more diversified as well. Among them, the back-scattered electron (BSE) image acquired through the scanning electron microscope (SEM) is attempted as the means to evaluate the self-healing effect on cracks. In order evaluate by the BSE image, sophisticated pre-processing of specimen is critical and this injected inside the particle, pore and artificial crack of the hardener to stabilize the structure of the newly generated self-healing product and it enables to endure the stress on polishing without deformation. The impregnated specimen smoothen the surface to obtain the BSE image of high resolution that polishing is made for diamond suspension for wet polishing after dry polishing. As a result of evaluating the self-healing product on the impregnated and polished self-healing specimen, the generated product is formed from the surface of the artificial crack and the self-healing substances are confirmed as $Ca(OH)_2$ and C-S-H.

Impact of Salespersons and Other Customers in a Fashion Store -Focus on Physical Attractiveness and Self-image Congruence- (패션 점포 내 판매원과 다른 고객에 대한 신체적 매력과 자기이미지 일치 효과)

  • Kim, Yunjeong;Lee, Yuri;Kim, Boram
    • Journal of the Korean Society of Clothing and Textiles
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    • v.38 no.6
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    • pp.783-795
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    • 2014
  • This study investigates how the physical attractiveness of salespeople and other customers and self-image congruence influence customer perception and brand attitude. As a result of a pretest, four types of pictorial stimuli were developed: physical attractiveness of salespeople (high/low) ${\times}$ that of other customers (high/low). Stimuli were developed using Photoshop CS. A total of 550 samples in two experiments were used and all respondents were women in their 20s and 30s. Data were analyzed using ANOVA and SEM. The result of analysis shows that the physical attractiveness of salesperson had a significant impact on perceived quality, but that of other customers did not. However, self-image congruence with other customers shows a significant effect on perceived quality; however, salespeople did not. The impact of the perceived product quality on brand attitude is higher than perceived service quality. This study adds to fashion retailing literature by demonstrating that physical attractiveness and self-image congruence can influence a customers' perception of product or service quality and brand attitude. It provides interesting insight into how retailers can use social factors as a strategic tool in a retail setting.

Feasibility as radiation detectors of Flexible ITO film fabricated by roll-to-roll sputtering (롤-투-롤 스퍼터링으로 제작된 Flexible ITO Film의 방사선검출기 적용가능성 연구)

  • Kim, Sung-Hun;Lee, S.H.;Jeon, S.P.;Park, G.U.;Heo, E.S.;Sung, Han-Kyu;Park, J.G.;Nam, Sang-Hee
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.374-374
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    • 2010
  • 본 연구는 Roll-to-Roll Sputtering 장비를 사용하여 제작된 Flexible ITO electrode 필름의 방사선 검출기로의 적용가능성을 알아보기 위해 기존의 Glass ITO electrode의 전기적 특성을 비교 평가하였다. 본 연구는 Flexible ITO electrode와 Glass ITO electrode을 하부전극으로 형성하고, 최근에 X-ray 변환체로 활발히 연구되고 있는 Powder 형태의 반도체물질인 HgI2 와 PbI2를 Binder와 일정한 비율로 혼합하여 3-Rolls-Miller를 사용하여 Powder를 일정한 미세크기로 만들고, 대면적 제작이 용이한 Screen-Printing method을 이용하여 시편을 제작하였다. 제작된 필름은 하부전극의 종류에 따른 X-ray 입사 후의 전기적신호의 차이를 측정하고, HgI2와 PbI2 중 Flexible ITO electrode와 더욱 효율적으로 반응하여 기존의 Glass ITO electrode를 대체할 수 있는 전극을 발견하여 진단용 의료영상의 왜곡 현상을 제거할 수 있는 Flexible 방사선 검출기의 제작의 초석을 제공하는 연구를 목적으로 한다. SEM(Scanning Electron Microscope) 통하여 반도체 물질의 결정구조와 크기를 알아보았고, 하부 전극의 종류에 따른 전기적 신호검출을 위해 제작된 필름의 암전류(Dark current) 와 민감도(Sensitivity)를 측정한 후, SNR (Signal -to- Noise)을 계산하여 평가하였다.

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The Preparation of Phosphor Screen for Video Phone Tube by Screen Printing Method (Screen Printing법에 의한 Video Phone Tube용 형광막 제조)

  • Lee Mi-Young;Lee Jong-Wook;Kim Young-Bae;Nam Su-Yong;Lee Sang-Nam;Moon Myung-Jun
    • Journal of Environmental Science International
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    • v.14 no.8
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    • pp.801-810
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    • 2005
  • The phosphor and ITO(Indium Tin Oxide) films for video phone tube (VPT) were simply prepared by the screen printing and thermal transfer methods. The increasing order of thermal firing of acrylic binder for phosphor and ITO was M6003 < M6664 < A/A 1919 < M500l < M670 1 and all mass of binders were perfectly decomposed at lower temperature than $400^{\circ}C.$ After thermal firing of phosphor paste, the residual of binder on the surface of phosphor could not be found by SEM. Aerosil as thickner provides the thixotropy property for phosphor paste but decrease the brightness of phosphor screen as residual after thermal firing. Since the thixotropy of M5001 binder without aerosil was shown and the storage modulus of phosphor paste by increasing the angular frequency was not nearly changed and the decrease of the storage modulus of phosphor paste by increasing the strain was remarkably shown. It was possible to prepare the phosphor paste which was predominant in the plate separation and the reproduction of pattern after the screen printing. Since the addition of dispersing agent to improve the printing process decreases the electrical conductivity and light transmission of ITa film, it could be found to be necessary the development of binder for phosphor paste that decreases the amount of dispersing agent possibly and does not use the aerosil as additive.

Development of Distortion Correction Technique in Tilted Image for River Surface Velocity Measurement (하천 표면영상유속 측정을 위한 경사영상 왜곡 보정 기술 개발)

  • Kim, Hee Joung;Lee, Jun Hyeong;Yoon, Byung Man;Kim, Seo Jun
    • Ecology and Resilient Infrastructure
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    • v.8 no.2
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    • pp.88-96
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    • 2021
  • In surface image velocimetry, a wide area of a river is photographed at an angle to measure its velocity, inevitably causing image distortion. Although a distorted image can be corrected into an orthogonal image by using 2D projective coordinate transformation and considering reference points on the same plane as the water surface, this method is limited by the uncertainty of changes in the water level in the event of a flood. Therefore, in this study, we developed a tilt image correction technique that corrects distortions in oblique images without resetting the reference points while coping with changes in the water level using the geometric relationship between the coordinates of the reference points set at a high position the camera, and the vertical distance between the water surface and the camera. Furthermore, we developed a distortion correction method to verify the corrected image, wherein we conducted a full-scale river experiment to verify the reference point transformation equation and measure the surface velocity. Based on the verification results, the proposed tilt image correction method was found to be over 97% accurate, whereas the experiment result of the surface velocity differed by approximately 4% as compared to the results calculated using the proposed method, thereby indicating high accuracy. Application of the proposed method to an image-based fixed automatic discharge measurement system can improve the accuracy of discharge measurement in the event of a flood when the water level changes rapidly.

Flowable Oxide를 이용한 저온 Flexible OLED 박막봉지 제작

  • Yong, Sang-Hyeon;Kim, Dae-Gyeong;Kim, Hun-Bae;Jo, Seong-Min;Chae, Hui-Yeop
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.249-249
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    • 2012
  • 최근 주목받고 있는 Flexible Organic Light Emitting Diode (OLED) display에서는 Flexible 특성이 요구된다. 이는 현재 쓰이는 유리기판 대신 플라스틱기판으로 만들어야 가능하다. 하지만 플라스틱기판은 구성물질로 유기물을 사용하므로 수분과 산소의 투과에 매우 취약하다. 이는 장시간 사용 시 기판 위에 제작된 소자성능저하를 야기하는 등의 소자 신뢰도에 치명적 결함을 갖게 하는 원인이 된다. 따라서 기판 위의 소자를 보호할 수 있는 봉지기술 개발이 필요한데 가장 잘 알려진 플라스틱 기판에 적합한 Barrier기술로 유기물과 무기물을 교대로 적층하는 기술[1] 등이 있다. 본 연구에서는 PE-CVD 공정기술을 이용한 Flowable Oxide 박막과 ALD 공정기술을 이용한 Al2O3 무기물 박막을 적층하여 봉지박막을 구성하려 한다. Flowable Oxide는 저온공정이 가능하며 높은 증착속도와 뛰어난 Gap fill 특성을 가지고 있는데 이는 플라스틱기판의 엉성한 분자구조를 치밀하게 만들 것으로 예상되며 표면의 Pin-hole 또한 쉽게 채우는 특성이 있다. 실험은 Polyethylene Naphthalate (PEN) film 위에 PE-CVD 공정을 이용하여 Flowable Oxide를 증착하고, 그 후에 ALD 공정을 이용하여 Al2O3을 적층한 것을 하나의 샘플로 하였다. 샘플의 분석은 Ca test를 이용한 Water Vapor Transmission rate(WVTR)과 FT-IR, FE-SEM을 이용하여 분석하였다. FT-IR로 박막의 구성요소를 확인 하고 FE-SEM으로 박막의 Cross section image를 얻을 수 있었으며 또한 $4.85{\times}10^{-5}g/m^2$ day의 초기 WVTR 값을 얻을 수 있었다.

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A study of CuxS thin film deposition using a low-temperature solution process (저온 용액공정을 이용한 CuxS 박막 증착에서 조성에 따른 특성 연구)

  • Hwang, Sooyeun;Lee, Jinyoung;Ryu, Siok
    • 한국신재생에너지학회:학술대회논문집
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    • 2010.11a
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    • pp.51.1-51.1
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    • 2010
  • 이번 연구에서는 저온 용액공정을 이용하여p-type 반도체로 많이 사용되고 있는 $Cu_xS$를 기판 위에 증착하여 그 특성을 분석하였다. $Cu_xS$는 x의 값에 따라 다섯가지의 결정구조를 가지는데 CuS, $Cu_{1.75}S$, $Cu_{1.8}S$, $Cu_{1.95}S$, $Cu_2S$ 들이 그것이다. 태양전지에서 p형 반도체로 중요한 역할을 담당하고 있는 $Cu_xS$는 cell에서 사용되었을 때 energy bandgap이 1.2-2.5eV일 때 가장 좋은 특성을 나타낸다. 이번 연구에서는 특히 조성에 따라서 물리적, 광학적으로 어떤 특성을 나타내는지에 대하여 XRD, SEM, Uv-vis 등의 분석을 해보았다. XRD의 경우 농도가 높아질수록 peak의 intensity는 커지지만 어느 농도 이상부터는 Cu가 Oxide화 되는 것을 관찰할 수 있었다. SEM image의 경우에는 조성에 따른 포면의 상태를 분석해보았다. 조성에 따른energy bandgap을 알아보기 위해서는 Uv-vis을 측정하였으며 이를 이용하여 증착된 박막의 투과도 역시 함께 분석해보았다.

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