• Title/Summary/Keyword: SEM (scanning electron microscope)

Search Result 1,887, Processing Time 0.026 seconds

Investigation of shinning Spot Defect on Hot-Dip Galvanized Steel Sheets

  • Liu, Yonggang;Cui, Lei
    • Corrosion Science and Technology
    • /
    • v.13 no.4
    • /
    • pp.125-129
    • /
    • 2014
  • Shinning spot defects on galvanized steel sheets were studied by optical microscope, scanning electron microscope(SEM), Energy Dispersive Spectrometer (EDS) and Laser-Induced Breakdown Spectroscopy Original Position Statistic Distribution Analysis (LIBSOPA) in this study. The research shows that the coating thickness of shinning spot defects which caused by the substrate defect is much lower than normal area, and when skin passed, the shinning spot defect area can not touch with skin pass roll which result in the surface of shinning spot is flat while normal area is rough. The different coating morphologies have different effects on the reflection of light, which cause the shinning spot defects more brighter than normal area.

The Study on Microstructures and Mechanical Properties of Mild Steel Joined with Various Spot Welding Conditions (점용접 조건에 의한 연강의 미세조직 및 기계적특성에 관한 연구)

  • 강연철;김대영;김완기;김석원
    • Journal of Welding and Joining
    • /
    • v.18 no.1
    • /
    • pp.52-58
    • /
    • 2000
  • Spot welding, namely a kind of electric resisting welding has been used widely in field of automobile and aircraft industries because of easiness to apply. Specimens used in this study was a mild steel of 1.2mm thickness and the electrode was a Cu-Cr alloy of 6mm diameter. The surface sheared of specimens after testing of tensile shear was observed by SEM(scanning electron microscope) after ultrasonic cleaning for 10min., and microstructures and grain size of all specimens were measured with using of O.M.(Optical microscope). By the means of measurement and observations of tensile shear load, fatigue strength and share surface, the weldability of spot welding was evaluated. When tensile shearing testing, fracture starting point in all specimens was took place at the bond between HAZ(Heat affected zone) and nugget. With increasing in number of layers, fatigue strength was decreased. With increasing in electric current, grain size in the HAZ became more fine.

  • PDF

A Contribution to the Pollen Morphology of Salix viminalis L. (Salix viminalis의 화분형태(花粉形態)에 관(關)한 연구(硏究))

  • Kim, Kae Hwan
    • Journal of Korean Society of Forest Science
    • /
    • v.66 no.1
    • /
    • pp.64-67
    • /
    • 1984
  • The genus Salix is nowadays becoming increasingly important for both biomass energy production and the expanding paper industry. The enlarging plantations will however create some potential as well as problem. The great potential of genetical improvement as well as the prevention of pollen allergies requires knowledge about e.g, the pollen morphology of the most used Salix species. This study investigated the pollen morphology of Salix viminalis L. both on light microscope (LM) and scanning electron microscope (SEM).

  • PDF

Study on Finding Optimum Condition of Plasma Treatment on SiO2 Substrates to Reduce Contact Resistance at Graphene-Metal Interface (그래핀-금속 접촉 저항을 줄이기 위한 SiO2 기판 플라즈마 처리의 최적화 연구)

  • Gang, Sa-Rang;Ra, Chang-Ho;Lee, Dae-Yeong;Yu, Won-Jong
    • Proceedings of the Korean Institute of Surface Engineering Conference
    • /
    • 2013.05a
    • /
    • pp.96-96
    • /
    • 2013
  • 그래핀과 금속 결합에서 발생하는 접촉 저항을 줄이기 위한 목적으로, 소자 제작에 사용되는 $SiO_2$ 기판의 표면을 플라즈마를 사용하여 에칭하는 최적의 조건에 대해 연구하였다. 기존에 발표된 연구 결과에 따라 $SF_6$$O_2$를 섞어 플라즈마 처리를 하였고, 플라즈마 방전에 사용 된 두 가스의 혼합 비율을 조절함으로써 소자 제작에 적합한 조건을 찾고자 하였다. 플라즈마 처리 전후의 $SiO_2$ 기판의 표면 측정은 AFM (Atomic Force Microscope)을 사용하였고, 단면은 SEM(Scanning Electron Microscope)을 통해 확인하였다.

  • PDF

Dispersion Property of CNT/CB Composite influenced EEA (EEA에 미치는 CNT/CB Composite 분산 특성)

  • Yang, Hoon;Park, Dae-Hee
    • Proceedings of the KIEE Conference
    • /
    • 2008.05a
    • /
    • pp.185-186
    • /
    • 2008
  • Use of the carbon nanotube is superior to general powder state materials of dispersion property. Because its ratio of diameter and length(aspect ratio) is very large, it has been known as a type of ideal nano-reinforcement composite. It used solution mixing method for specimen fabrication. To research dispersion property, we used FE-SEM(Field Emission Scanning Electron Microscope) and AFM(Atomic Force Microscope). As a result, this tendency confirms new conductivity network in which the carbon nanotube between carbon black constitute molecules shows a bond by similar constructive property.

  • PDF

High resolution patterning of polyfluorene derivative containing photo cross-linkable oxetane units

  • Park, Moo-Jin;Lee, Jeong-Ik;Chu, Hye-Yong;Kim, Seong-Hyun;Zyung, Taeh-Young;Hwang, Do-Hoon
    • 한국정보디스플레이학회:학술대회논문집
    • /
    • 2005.07b
    • /
    • pp.1419-1420
    • /
    • 2005
  • We have synthesized a photo patternable blue lightemitting polyfluorene (PF) derivative containing cross-linkable oxetane units. Poly(9,9-bis-(4-octyloxyphenyl)- fluorene-2,7-diyl-alt-9,9-bis-((3-hexyloxy-3'- ethyl)-oxetane)-fluorene-2,7-diyl) has been synthesized by Suzuki coupling polymerization. The relationship between patterning property and several variables such as the intensity of the exposed UV light, the concentrations of additives, has been studied by using optical microscope UV/visible spectroscopy, photoluminescence and scanning electron microscope (SEM). We obtained fine patterns with 10 mm resolution using the polymer film after exposure and development. This patterning method using conjugated polymers can be applicable to make fine pixels for PLEDs and OFETs.

  • PDF

Electrical and optical characteristics of ITO films with different composition (ITO의 조성에 따른 전기적, 광학적 특성)

  • Lee, Seo-Hee;Jang, Gun-Eik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2010.06a
    • /
    • pp.216-216
    • /
    • 2010
  • ITO는 n- type 반도체 재료로 Sn의 첨가로 인한 매우 낮은 전기저항과 안정성때문에 널리 사용되고 있는 재료이며 비교적 높은 band gap(3.55Ev)를 가짐으로 인하여 가시광선 영역에서 높은 투과도를 가지는 특징이 있다. 단점으로는 박막 제조 시에 증착시간의 증가함에 따라 음이온 충격 및 온도 상공으로 인한 막의 표면손상이 발생하게 되고 이것은 전기저항이 증가하는 요인으로 작용하는 문제점이 있다. 본 연구에서는 3가지 조성의 ITO박막을 스퍼터 장치를 이용하여 증착하고 그에 따른 전기적, 구조적, 광학적 특성을 분석 하였다. 증착된 ITO성막의 표면분석을 위해 AFM (Atomic Force Microscope)으로 표면 거칠기값 분석, XRD (X-ray diffraction)을 이용 결정성장분석, SEM (Scanning Electron Microscope)으로 표면의 미세구조관찰, 4Point pobe로 면 저항분석, spectrophotometer로 박막의 투과율과 흡수율을 분석하였다. 조성변화와 공정변수에 따른 전기적, 구조적, 광학적 특성변화의 원인분석으로 고효율의 ITO 박막성장 가능성을 조사하였다.

  • PDF

A Experimental Study on the Alkali-Silica Reaction of Crushed Stones (Part 1 : The Identification of Reactive Aggregate and the Influence of Aggregate Content to the Alkali-Silica Reaction) (쇄석 골재의 알칼리-실리카 반응에 관한 실험적 연구(제 1보 : 반응성골재의 판정과 골재혼입율이 알칼리-실리카 반응에 미치는 영향))

  • 윤재환;이영수;정재동;노재호;이양수;조일호
    • Proceedings of the Korea Concrete Institute Conference
    • /
    • 1993.10a
    • /
    • pp.103-107
    • /
    • 1993
  • The Alkali Aggregate Reaction(AAR), reported first by T. E. Stanton in 1940, is a reaction between certain siliceous aggregate and hydroxyl ions present in the pore fluid of a concrete. The damage of concrete structures, deteriorated by AAR, have been reported since using the crushed stones caused by the exhaustion of natural aggregates. This study was performed to investigate the AAR of crushed stones using chemical analysis, polarization microscope, XRD, chemical method(KS F 2545, ASTM C 289), mortar bar method(KS F 2546, ASTM C 227) and Scanning Electron Microscope(SEM) and Energy Dispersive X-ray Analysis (EDXA) of reaction products by AAR in mortar bar.

  • PDF

Evaluation of Cavitation Characteristics of 5083-O Al Alloy with Amplitude (5083-O 알루미늄 합금의 진폭에 따른 캐비테이션 침식 특성 평가)

  • Lee, Seung Jun;Kim, Seong Jong
    • Corrosion Science and Technology
    • /
    • v.11 no.5
    • /
    • pp.205-212
    • /
    • 2012
  • With recent advances in engineering and technology, a damage on industrial machineries performing high-speed and high-power requirements has become a problem. There is an increasing possibility of cavitation damage, especially in pumps, propellers and high-speed vessels in a flowing liquid accordingly. There are several factors affecting cavitation damage on materials, including viscosity, pressure, temperature, amplitude applied. In this study, effects of cavity pressure in seawater on the damage for 5083-O aluminium alloy were evaluated by modulating amplitude. Trend of the damage with respect to time and amplitude was analyzed comparatively, and surface degradation of specimens was investigated by using Scanning Electron Microscope(SEM) and 3D microscope. The result reveals that the amount of the damage increased consistently with the increase in time and amplitude while the plastic deformation zone where no appreciable damage occurred was in less than 30 minutes.

Characteristics of AlN thin films for SAW filters based on substrates (기판의 종류에 따른 SAW 필터용 AlN 박막의 특성)

  • Ko, Bong-Chul;Nam, Chang-Woo
    • Journal of Sensor Science and Technology
    • /
    • v.16 no.3
    • /
    • pp.240-245
    • /
    • 2007
  • AlN thin film for SAW filter application was deposited on (100) silicon, sapphire, $Si_{3}N_{4}$/Si, and $Al_{2}O_{3}$/Si substrates by reactive magnetron sputtering method, respectively. The structural characteristics were dependent on the structure of substrates. Scanning Electron Microscope (SEM), X-ray Diffraction (XRD) and Atomic Force Microscope (AFM) have been used to analyze structural properties and preferred orientation of AlN thin films. Preferred orientation and SAW characteristic of AlN were improved by insertion of $Al_{2}O_{3}$ buffer layer. Insertion loss of SAW devices using AlN/Si and AlN/$Al_{2}O_{3}$/Si were about 33.27 dB and 30.20 dB, respectively.