• Title/Summary/Keyword: Roughness factor

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Electrochemical and Mechanical Characteristics of Covalently Cross-Linked SPEEK Polymer Electrolyte Membrane for Water Electrolysis (수전해용 공유가교 SPEEK 고분자 전해질 막의 전기 화학적 및 기계적 특성)

  • Kim, Kyung-Eon;Jang, In-Young;Kweon, Oh-Hwan;Hwang, Yong-Koo;Moon, Sang-Bong;Kang, An-Soo
    • Transactions of the Korean hydrogen and new energy society
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    • v.18 no.4
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    • pp.391-398
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    • 2007
  • The covalently cross-linked sulfonated polyetheretherketone (CL-SPEEK) membrane was prepared by four-step synthesis of sulfonation-sulfochlorination, partial reduction, lithiation, and cross-linking, and its electrochemical and mechanical properties were investigated for water electrolysis application. The prepared ion exchange membranes showed good electrochemical and mechanical properties; proton conductivity of 0.116 S/cm at $80^{\circ}C$, water uptake of 44.6%, ion exchange capacity of 1.75 meq/g-dry-memb., tensile strength of 64.25 MPa and elongation of 61.11%. The membrane electrode assembly (MEA) with homemade membranes were prepared by non-equilibrium impregnation-reduction (I-R) method. Especially, the electrochemical surface area (ESA) and roughness factor of CL-SPEEK electrolyte by cyclic voltammetry method were 23.46 $m^2/g$ and 307.3 $cm^2-Pt/cm^2$, respectively. The prepared MEA was used in the unit cell of water electrolysis and the cell voltage was 1.81 V at 1 A/$cm^2$ and $80^{\circ}C$, with platinum loadings of 1.31 mg/$cm^2$.

Fabrication of Ceramic 3D Integration Technology for Ink-jet Printing (Ink-jet Printing을 이용한 3D-Integration 구현)

  • Hwang, Myung-Sung;Kim, Ji-Hoon;Kim, Hyo-Tae;Yoon, Young-Joon;Kim, Jong-Hee;Moon, Joo-Ho
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.332-332
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    • 2010
  • We have successfully demonstrated the inkjet printing method to create $Al_2O_3$ films withouWe have successfully demonstrated the inkjet printing method to create $Al_2O_3$ films without a high temperature sintering process. In order to remove the coffee ring effect in the ink drop, we have introduced a co-solvent system in order to create Marangoni flow in the ink drop, which leads to the dense packing of ceramic powders on the substrate during inkjet process. The packing density of the Inkjet-printed $Al_2O_3$ films is around 60% (max. 70%) which is very high compared to the value obtained from the same material films by other conventional methods such as film casting, dip coating process, etc. The voids inside the films (which are around 40% of the entire film volume) are filled with the polymer resin (Cyanate ester) by the infiltration process. This resin infiltration is also implemented by the inkjet printing process right after the Ah03 film ink-jetting process. The microstructures of the printed $Al_2O_3$ films are investigated by Scanning Electron Microscope (SEM) to understand the degree of packing density in the printed films. The inkjet-printed $Al_2O_3$ films have been characterized to investigate its thickness and roughness. Quality factor of the printed $Al_2O_3$ film is also measured to be over 300 at 1MHz.

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Estimation of Design Wind Speed for Building Using Spatial Information Analysis (공간정보 분석을 통한 건축물의 설계풍속 산정)

  • Lee, Seong-Yun;Jo, Hyun-Jae;Lee, Hyun-Ki;Choi, Se-Hyu
    • Spatial Information Research
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    • v.23 no.3
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    • pp.79-89
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    • 2015
  • Once the building is higher than certain size, the wind effect plays very important role in structure design. Moreover, this is more important in Korea because dangerous phenomena like typhoons are common. Rational wind resistant design is being magnified considering the global flow and climate changes. This research presented the estimation method of design wind load using spatial information analysis based on 1:5,000 digital map and performed comparative analysis with actual application cases. The wind velocity pressure exposure coefficient and topographic coefficient turned out to be more quantitative and rational when calculated through the proposed method. The time and cost are comparatively low when compared with traditional method which contribute to the economic and rational wind resistant design.

Problems and Solutions for Ultra-compact LED Package Development (극소형 LED 패키지 개발의 문제점과 해결 방안)

  • Lee, Jong Chan
    • Journal of Industrial Convergence
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    • v.17 no.4
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    • pp.9-14
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    • 2019
  • This paper presents several problems that can occur in the development of the ultra-compact LED package of less than 1.0mm and introduces the solution to them. In the existing mold structure, since the upper and lower core parts are integrated, various errors have occurred due to the roughness of EDM in the small model, which is a limiting factor in further reducing the mold size. As a countermeasure, the prefabricated model was presented in an earlier study to overcome the obstacles to the development of a ultra-compact LED package. In this paper, several problems have been found during the fabrication of prototypes as a starting work to produce the results for the presented model. The types are suggested and the solutions are discussed. And by changing the existing 2-row structure to 3-row structure in the same size lead frame, the aspect of efficient production is considered. The experimental procedure verifies the proposed solution and conducts a test to produce a prototype to confirm that a good product can be produced.

Structure and Magnetic Properties of Fe-N Films Deposited by Dc Magnetron Sputtering (DC Magnetron Sputtering 방법으로 증착한 Fe-N 박막의 구조와 자기적 성질)

  • 이종화;이원종
    • Journal of the Korean Magnetics Society
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    • v.3 no.2
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    • pp.87-93
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    • 1993
  • Iron nitride (Fe-N) magnetic thin films were deposited using a DC magnetron sputtering system. Microstructures and magnetic properties were examined as a function of deposition power and nitrogen gas input ratio. The nitrogen content in the film was found to be the major factor determining the microstructure and the magnetic properties. The films deposited at low nitrogen input ratios have an $\alpha$-Fe structure of which the lattice is expanded due to the nitrogen atoms incorporated at the interstitial sites. As the nitrogen content in the film increases, the degree of lat-tice expansion increases and the value of saturation magnetization decreases linearly. The films with a high degree of lattice expansion give very low values of coercivity, which is attributed to the disturbance of colunmar growth and the decrease of surface roughness. Further increase in the nitrogen input ratio causes the phase transfonnation from $\alpha$-Fe to $Fe_{2-3}N$, resulting in the marked reduction in the saturation magnetization. The phase transformation occurs when, regardless of deposition conditions, the nitrogen content reaches at 15 at.% and the lattice is expanded by 5%.

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Psychoacoustical Study for Sound Quality Index of Steady State Noise of Refrigerators (냉장고 정상상태 소음의 음질 인덱스 개발을 위한 심리음향학적 연구)

  • Kong, Kyung-Soo;Jung, Weui-Bong;Kim, Tae-Hoon;Shin, Dae-Sik;Ahn, Se-jin
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.26 no.5
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    • pp.536-545
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    • 2016
  • Household refrigerator radiates noise of which the pattern is dependent on the operating condition of its parts, such as compressor, flow fans, etc. Thus the refrigerator noise has a variety of frequency characteristics. Therefore, it is required to consider the noise characteristics for evaluating the noise quality and eventually developing the sound quality index of the refrigerator noise. In this study, five units of household refrigerator were selected to measure their noises that were used to generate sound sources for jury test of the study. The measured noises of five refrigerators were divided into ten kinds of sound source by considering operating condition and frequency characteristics. Additionally, the ten sources were each edited to have the same SPL of 30 dBA. Totally twenty kinds of sound sources (10-original SPL, 10-edited SPL 30 dBA) were evaluated by twenty-two subjects, and compared with their sound quality metrics. It was found that only the loudness of the metrics was meaningfully correlated with the subjective evaluation. The rests, sharpness, roughness and fluctuation strength, were not related. The conclusion of this study is that a new sophisticated index is necessary to be developed to qualitatively evaluate the household refrigerator noise.

Electron Discharge Machining (EDM) and Hole EDM of Cold Heat-treated Tool Steel Molds (STD11) by using Cu Electrodes (냉간 금형용 공구강의 Cu 전극을 이용한 방전 홀에 관한 연구)

  • Park, In-Soo;Lee, Eun-Ju;Kim, Hwa-Jeong;Wang, Deok-Hyun
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.17 no.4
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    • pp.76-82
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    • 2018
  • 3D formed Electrical Discharge Machining (EDM) and hole EDM were conducted for die and mold manufacturing with electrodes which were made by mechanical machining and wire EDM. It is difficult to machine the hardened material after heat treatment and quenching with traditional machining. The only method of machining hardened material is die-sinking EDM. In this research, hole EDM was conducted for heat-treated cold-worked tool steel (SKD11) for use as a die material. The EDM surfaces were analyzed by pulse-on time and peak current of EDM current, according to the machining conditions of EDM. The EDM surface profiles were affected by the peak current. The contribution of each factor is peak current (91.63%) and pulse-on time (0.93%). The best surface roughness was obtained with a $130{\mu}s$ pulse-on time and a 14.2 A peak current. With uniform EDM processing, the surface deteriorated with increasing pulse-on time and peak current. The thickness of the solidified layer induced by EDM was increased as the peak current, crater shapes, and erupted shapes of EDM surfaces were increased. Therefore, microcracking gaps induced by surface tension were increased.

A STUDY ON THE FRACTURE TOUGHNESS OF DENTAL COMPOSITE RESINS (치과용 복합레진의 파괴인성에 관한 실험적 연구)

  • Park, Jin-Hoon;Min, Byung-Soon;Choi, Ho-Young;Park, Sang-Jin
    • Restorative Dentistry and Endodontics
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    • v.15 no.2
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    • pp.17-33
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    • 1990
  • The purpose of this study was to evaluate the fracture toughness of dental composite resins and to investigate the filler factor affecting the fracture behaviour on which the degree of fracture toughness depends. Six kinds of commercially available composite resin;, including two of each macrofilled, microfilled, and hybrid type were used for this study, The plane strain fracture toughness ($K_{10}$) was determined by three-point bending test using the single edge notch specimen according to the ASTM-E399. The specimens were fabricated with visible light curing or self curing of each composite resin previously inserted into a metal mold, and three-point bending test was conducted with cross-head speed of 0.1mm/min following a day's storage of the specimens in $37^{\circ}C$ distilled water. The filler volume fractions were determined by the standard ashing test according to the ISO-4049. Acoustic Emission(AE), a nondestructive testing method detecting the elastic wave released from the localized sources In material under a certain stress, was detected during three-point bending test and its analyzed data was compared with, canning electron fractographs of each specimen. The results were as follows : 1. The filler content of composite resin material was found to be highest in the hybrid type followed by the macrofilled type, and the microfilled type. 2. It was found that the value of plane strain fracture toughness of composite resin material was in the range from 0.69 MPa$\sqrt{m}$ to 1 46 MPa$\sqrt{m}$ and highest In the macrofilled type followed by the hybrid type, and the microfilled type. 3. The consequence of Acoustic Emission analysis revealed that the plane strain fracture toughness increased according as the count of Acoustic Emission events increased. 4. The higher the plane strain fracture toughness became, the higher degree of surface roughness and irregularity the fractographs demonstrated.

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Three-Dimensional Laboratory Experiments for Tsunami Inundation in a Coastal City (지진해일 범람이 해안도시에 미치는 영향에 대한 3차원 수리모형실험)

  • Kim, Kyuhan;Park, Hyoungsu;Shin, Sungwon;Cox, Daniel T.
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.24 no.6
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    • pp.400-403
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    • 2012
  • Laboratory experiments were conducted for tsunami inundation to an urban area with large building roughness. The waterfront portion of the city of Seaside which is located on the US Pacific Northwest coast, was replicated in 1/50 scale in the wave basin. Tsunami heights and velocities on the inundated land were measured at approximately 31 locations for one incident tsunami heights with an inundation height of approximately 10 m (prototype) near the shoreline. The inundation pattern and speed were more severe and faster in some areas due to the arrangement of the large buildings. Momentum fluxes along the roads were estimated using measure tsunami inundation heights and horizontal fluid velocities. As expected, the maximum momentum flux was near the shoreline and decreased landward. Inundation heights and momentum flux were slowly decreased through the road with buildings on each side. The results from this study showed that the horizontal inundation velocity is an important factor for the external force of coastal structures.

The Development of Automatic Grease Lubricator Driven by Gear Mechanism with Controlled Operating Time (주유시간 조절이 가능한 기어 메커니즘 구동방식의 자동그리스주유기 개발)

  • Wang, Duck-Hyun;Lee, Kyu-Young;Lee, Sang-Hoon
    • Journal of the Korean Society for Precision Engineering
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    • v.23 no.2 s.179
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    • pp.199-206
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    • 2006
  • Automatic grease lubricator is equipment that provides adequate amount of fresh grease constantly to the shaft and the bearings of machines. It minimizes the friction heat and reduces the friction loss of machines to the least. This research is to develop automatic grease lubricator by gear driven mechanism with controlled operation time. The ultimate design of this equipment is to lubricate an adequate amount of grease by a simple switch clicking according to the advanced set cycle. The backlash of the gear was minimized to increase the output power. To increase the power of gear mechanism, the binding frequency and the thickness of the coil were changed. To control the rotating cycles of the main shaft according to its set numbers, different resistance and chips were used to design the circuit to controls electrical signals with pulse. The body of the lubricator was analyzed by stress analysis with different constructed angle. The stress analysis for differing loading pressures applied to the exterior body of grease lubricator due to the setup angle, was found that the maximum stress was distributed over the outlet part where the grease lubricator suddenly narrowed contracts. Digital mock-up was analyzed and the rapid prototyping(RP) trial products were tested with PCB circuit and grease. The evaluation of the outlet capacity for RP trial products was conducted, because the friction caused by the outlet on the wall surface was an important factor in the operation of the equipment. Finally, the finishing process was applied to decrease the roughness of the surface to a comparable level and was able to test the performance examination for the product.