• Korea-Australia Rheology Journal
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• 제14권2호
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• pp.71-76
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• 2002

Metal thin films, which are indispensable constituents of ULSI (Ultra Large Scale Integration) circuits, have been fabricated by physical or chemical methods. However, these methods have a drawback of using expensive high vacuum instruments. In this work, the fabrication of tungsten metal film by spin coating was investigated. First of all, inorganic peroxopolytungstic acid (W-IPA) powder, which is soluble in water, was prepared by dissolving metal tungsten in hydrogen peroxide and by evaporating residual solvent. Then, the solution of W-IPA was mixed with organic solvent, which was spin-coated on wafers. And then, tungsten metal films, were obtained after reduction procedure. By selecting an appropriate organic solvent and irradiating UV, the sheet resistance of the tungsten metal film could be remarkably reduced.

• 한국유변학회:학술대회논문집
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• 한국유변학회 2001년도 Australian-Korean Rheology Conference 2001
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• pp.156.5-156
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• 2001

(No abstract, see full-text)

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2004년도 추계학술대회논문집
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• pp.103-106
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• 2004

The new rheology fabrication process has been developed to rheo die casting and rheo forming process. Thixoforming process has disadvantages in terms of induction reheating process, scrap recycling, loss of raw material and cycle time. Therefore, to reduce the number of process, new rheology fabrication process with specially designed the rotational barrel type equipment has been proposed to apply in various part productions. The barrel type equipment, which could continuously fabricate the rheology materil, was specially designed to have a function to control cooling rate, shear rate and temperature. During the continuous rotation of barrel with a constant temperature, the shear rate is controlled with the rotation speed. The barrel surface has both the induction heating system and the cooling system to control the temperature of molten metal. By using this system, the effect of the rotation speed and the rotation time on the microstructure was widely examined. The possibility for the rheoforming process was investigated with microstructural characteristic.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2007년도 춘계학술대회 논문집
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• pp.131-134
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• 2007

A semi-solid forming technology has a lot of advantages compared to the die casting, squeeze casting and hot/cold forging, so semi-solid forming has been studied actively. Semi-solid forming has two methods. One is thixoforming with reheating of prepared billet, the other is rheoforming with cooled melt until semi-solid state. Thixoforging technology can produce non-dendritic alloys for semi-solid forming complex shaped parts in metal alloys. In this study, the thixoforging was experimented with made rheology materials by the spiral stirrer equipment. Rheology materials for forging were made by A356 casting aluminum alloy and A6061 wrought aluminum alloy. After experiment, forged samples were measured microstructure and were heat treated for high mechanical properties.

• 소성∙가공
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• 제8권2호
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• pp.188-199
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• 1999

Semi-Solid Forming Process(Thixoforming, Rheocasting) is a novel forming process which has some advantages compared with conventional die casting, squeeze casting and hot/cold forging. In this study. Thixoforming process was selected as analysis processing in terms of billet handling and easiness of automation process. The Thixoforming process consists of reheating process of billet, billet handling, filling inot the die cavity and solidification of SSM part. In filling process, two rheology models which were Newtonian and Non-Nettonian model (Ostwald-deWaele)were verified with experimental results. The Ostwald-deWaele model shows the good agreement to the real flow and filling phenomena in die cavity. To give a boost the economical efficiency of Thixoforming process and to ensure the good forming result, reheating device coupled die set was proposed and the initial billet temperature for system that was found from experimental resluts. This study presents an overview of application of numerical analysis for simulation of semi-solid metal forming process to reduce the lead time for development of manufacturing part in industrial field.

• 유변학
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• 제1권1호
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• pp.36-45
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• 1989

아이어닝 공정은 제품의 치수정밀도가 정확하게 조절괴는 정밀 금속 성형공정이다. 아이어닝 공정은 대개 냉간상태에서 행하여지며 그리고 때로는 단공정 대신에 다단식이 적 용된다. 본연구의 목적은 강소성 유한 요소법으로 단공정과 다단식 아이어닝 공정을 해석하 여 아이어닝 공정에 대한 적절한 설계변수와 최적 설계조건을 찾는데 있다. 본 연구에서는 공정설계게 있어서 공정변수를 다이의 원추각과 단의 개수로 주었다. 본 해석에서는 단공정 아이어닝과 다단식 아이어닝 공정의 성형하중, 응력과 변형도 분포 그리고 격자 변형을 계 산하였다 그리고 이 값들에 대한 공정 변수의 영향을 검토한 결과 성형하중과 격자 변형에 있어서 계산 결과와 잘 일치하였다.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2005년도 추계학술대회 논문집
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• pp.358-361
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• 2005

The rotational barrel type equipment has been designed for the new rheology fabrication process. During the continuous rotation of barrel with a constant temperature, the shear rate is controlled with the rotation speed and rotation time of barrel. The barrel surface can be controlled the temperature by the induction heating and cooling system. Many experiments were widely examined by using this system with controlling the rotation speed and the rotation time. The possibility for the rheoforming process was investigated with microstructural characteristics.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2005년도 추계학술대회 논문집
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• pp.645-648
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• 2005

The rotational barrel type equipment has been designed for the new rheology fabrication process. During the continuous rotation of barrel with a constant temperature, the shear rate is controlled with the rotation speed and rotation time of barrel. The barrel surface can be controlled the temperature by the induction heating and cooling system. Many experiments were widely examined by using this system with controlling the rotation speed and the rotation time. The possibility for the rheoforming process was investigated with microstructural characteristics.

• Korean Chemical Engineering Research
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• 제58권2호
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• pp.176-183
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• 2020

이 연구에서는 작은 유기 분자 말단의 하이드록실기와 전이 금속 사이의 배위 결합을 통해 고분자와 유사하게 연결된 복합체를 제작하고, 점착 부여제를 추가하여 해당 물질의 점착제로의 사용 가능성을 확인하였다. 점착제 합성에 사용한 타닌산(tannic acid, TA)은 하이드록실기를 풍부하게 보유하고 있어 전이 금속과는 배위 결합이 가능하고 친수성 고분자와는 수소 결합이 가능하다. 위의 성질을 이용하여 타닌산과 전이 금속, 고분자 세 가지 성분을 한 번에 간단히 섞어 기판에 잘 펴지며 점착 능력을 보유한 특별한 유변 물성을 가지는 물질을 제작하였다. 합성에 사용한 전이 금속의 종류(Fe³⁺, Ti⁴⁺), 고분자의 종류, 처리 조건 등에 따른 유변 물성의 변화를 확인하는 과정을 통해 점착제로 사용하기에 가장 적합한 성분의 조합을 발견하였으며, 인체에 무해하며 높은 응집력과 접착력을 보유한 다목적 점착제로의 사용 가능성을 확인하였다.

• 한국추진공학회지
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• 제15권5호
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• pp.96-106
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• 2011

젤 추진제는 젤 추진 시스템에서 액체 추진 시스템과 같이 제어의 용이성, 저장성, 취급성, 비누설성 등과 같은 장점을 포함한다. 또한, 젤 추진제는 액체 추진제와 비교했을 때 보다 높은 발열량 특성을 나타내며, 금속 입자(알루미늄, 보론)의 첨가로 높은 비추력을 얻을 수 있다. 미립화 특성과 관련하여 젤 추진제는 젤화제의 다양한 점도와 금속 입자의 첨가 정도에 따라 저조한 미립화 특성을 나타낸다. 젤 추진제의 미립화 특성 향상과 연소 효율을 증대 시키기 위해 젤화제의 함유량 변화와 금속 입자의 첨가 정도에 따른 젤 추진제 제조 기술을 바탕으로 동적 분무 특성, 연소 특성 연구를 수행하고 있으며, 이에 대한 연구동향을 소개한다.