• Korea-Australia Rheology Journal
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• v.14 no.2
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• pp.71-76
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• 2002

Metal thin films, which are indispensable constituents of ULSI (Ultra Large Scale Integration) circuits, have been fabricated by physical or chemical methods. However, these methods have a drawback of using expensive high vacuum instruments. In this work, the fabrication of tungsten metal film by spin coating was investigated. First of all, inorganic peroxopolytungstic acid (W-IPA) powder, which is soluble in water, was prepared by dissolving metal tungsten in hydrogen peroxide and by evaporating residual solvent. Then, the solution of W-IPA was mixed with organic solvent, which was spin-coated on wafers. And then, tungsten metal films, were obtained after reduction procedure. By selecting an appropriate organic solvent and irradiating UV, the sheet resistance of the tungsten metal film could be remarkably reduced.

• Proceedings of the Korean Society of Rheology Conference
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• 2001.09a
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• pp.156.5-156
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• 2001

(No abstract, see full-text)

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.10a
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• pp.103-106
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• 2004

The new rheology fabrication process has been developed to rheo die casting and rheo forming process. Thixoforming process has disadvantages in terms of induction reheating process, scrap recycling, loss of raw material and cycle time. Therefore, to reduce the number of process, new rheology fabrication process with specially designed the rotational barrel type equipment has been proposed to apply in various part productions. The barrel type equipment, which could continuously fabricate the rheology materil, was specially designed to have a function to control cooling rate, shear rate and temperature. During the continuous rotation of barrel with a constant temperature, the shear rate is controlled with the rotation speed. The barrel surface has both the induction heating system and the cooling system to control the temperature of molten metal. By using this system, the effect of the rotation speed and the rotation time on the microstructure was widely examined. The possibility for the rheoforming process was investigated with microstructural characteristic.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.05a
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• pp.131-134
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• 2007

A semi-solid forming technology has a lot of advantages compared to the die casting, squeeze casting and hot/cold forging, so semi-solid forming has been studied actively. Semi-solid forming has two methods. One is thixoforming with reheating of prepared billet, the other is rheoforming with cooled melt until semi-solid state. Thixoforging technology can produce non-dendritic alloys for semi-solid forming complex shaped parts in metal alloys. In this study, the thixoforging was experimented with made rheology materials by the spiral stirrer equipment. Rheology materials for forging were made by A356 casting aluminum alloy and A6061 wrought aluminum alloy. After experiment, forged samples were measured microstructure and were heat treated for high mechanical properties.

• Transactions of Materials Processing
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• v.8 no.2
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• pp.188-199
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• 1999

Semi-Solid Forming Process(Thixoforming, Rheocasting) is a novel forming process which has some advantages compared with conventional die casting, squeeze casting and hot/cold forging. In this study. Thixoforming process was selected as analysis processing in terms of billet handling and easiness of automation process. The Thixoforming process consists of reheating process of billet, billet handling, filling inot the die cavity and solidification of SSM part. In filling process, two rheology models which were Newtonian and Non-Nettonian model (Ostwald-deWaele)were verified with experimental results. The Ostwald-deWaele model shows the good agreement to the real flow and filling phenomena in die cavity. To give a boost the economical efficiency of Thixoforming process and to ensure the good forming result, reheating device coupled die set was proposed and the initial billet temperature for system that was found from experimental resluts. This study presents an overview of application of numerical analysis for simulation of semi-solid metal forming process to reduce the lead time for development of manufacturing part in industrial field.

• The Korean Journal of Rheology
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• v.1 no.1
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• pp.36-45
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• 1989

아이어닝 공정은 제품의 치수정밀도가 정확하게 조절괴는 정밀 금속 성형공정이다. 아이어닝 공정은 대개 냉간상태에서 행하여지며 그리고 때로는 단공정 대신에 다단식이 적 용된다. 본연구의 목적은 강소성 유한 요소법으로 단공정과 다단식 아이어닝 공정을 해석하 여 아이어닝 공정에 대한 적절한 설계변수와 최적 설계조건을 찾는데 있다. 본 연구에서는 공정설계게 있어서 공정변수를 다이의 원추각과 단의 개수로 주었다. 본 해석에서는 단공정 아이어닝과 다단식 아이어닝 공정의 성형하중, 응력과 변형도 분포 그리고 격자 변형을 계 산하였다 그리고 이 값들에 대한 공정 변수의 영향을 검토한 결과 성형하중과 격자 변형에 있어서 계산 결과와 잘 일치하였다.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2005.10a
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• pp.358-361
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• 2005

The rotational barrel type equipment has been designed for the new rheology fabrication process. During the continuous rotation of barrel with a constant temperature, the shear rate is controlled with the rotation speed and rotation time of barrel. The barrel surface can be controlled the temperature by the induction heating and cooling system. Many experiments were widely examined by using this system with controlling the rotation speed and the rotation time. The possibility for the rheoforming process was investigated with microstructural characteristics.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.10a
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• pp.645-648
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• 2005

The rotational barrel type equipment has been designed for the new rheology fabrication process. During the continuous rotation of barrel with a constant temperature, the shear rate is controlled with the rotation speed and rotation time of barrel. The barrel surface can be controlled the temperature by the induction heating and cooling system. Many experiments were widely examined by using this system with controlling the rotation speed and the rotation time. The possibility for the rheoforming process was investigated with microstructural characteristics.

• Korean Chemical Engineering Research
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• v.58 no.2
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• pp.176-183
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• 2020

In this study, synthesis of a hydrogel consisted of a coordination bond network between small organic molecules and transition metals had been carried out. By adding a tackifying material to the gel, the potential of the gel to be used as an adhesive material had been also confirmed. Synthesis of the adhesive had been done with simple mixing of 3 components: tannic acid, transition metal, and polymer. The tannic acid molecule possesses multiple hydroxyl groups that can form coordination bonds with the transition metals and hydrogen bonds with the hydrophilic polymers. Due to the morphology of the metal-organic complex and polymer dispersed in water, the fabricated material exhibited high adhesiveness and cohesiveness. Optimizing the rheological property had been conducted for use in adhesive by the synthesis with varying the transition metal (Fe³⁺, Ti⁴⁺), polymer, and treatment conditions. Rheological measurement results demonstrate the promising potential of the material as a bio-compatible and versatile pressure-sensitive adhesive with both high adhesiveness and cohesiveness.

• Journal of the Korean Society of Propulsion Engineers
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• v.15 no.5
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• pp.96-106
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• 2011

There are many advantages in applying gel propellant to a gel propulsion system. These include higher performances, the energy management of liquid propulsion system, reliable storability and low leakage characteristics. Additionally, gel propulsion system are preferable to the high density impulse of propulsion system. Also, when compared to liquid propellants, the gel propellants acquire greater heat energy. Gel propellants achieve a high specific impulse when metal particles with aluminum and boron are added. With respect to atomization, an inactive process occurs due to the variable viscosity of the metal particles and gelling agents. To improve the defect of atomization and combustion characteristics of gel propellant, a variety of issues related to spray and combustion is introduced here.