• Food Quality and Culture
• /
• v.2 no.1
• /
• pp.13-19
• /
• 2008

Recently, though mulberry's superiority as a functional food has been proven, its use as a food material is limited. Therefore, in this study, to develop jelly using mulberry that is compatible with Korean tastes as health functional food by grafting the method to manufacture jelly consumed as a dessert or a snack in the west, according to the central composite design, mulberry jelly was produced by varying the content of citric acid ($X_1$), sucrose ($X_2$), and gelatin ($X_3$) at 5 levels. And by applying the response surface methodology, rheology and sensory preference experiment results were analyzed, the optimization of mulberry jelly manufacturing condition was carried out, and studies on the analysis of composition were performed. As the sensory preference of mulberry jelly, except the flavor, the remaining hardness, elasticity, sweetness, color, and the overall quality were found to be significant. And similarly, it was found to be influenced greatly by gelatin content generally. Based on the overlapped part of categories, in the range of factors that satisfy all the sensory categories, the value located in the middle was calculated, the optimization point was obtained, and it was found to be 6.2 g citric acid, 141.0 g sugar, and 13.5 g gelatin.

• Proceedings of the Korean Institute of Building Construction Conference
• /
• 2005.11a
• /
• pp.57-61
• /
• 2005

Cement paste is originally the basic material and crucial factor consisting concrete. This study investigates the relationship between flow apparatuses, which are ring flow(R-F), flow cone(F-C) and mini slump(M-S), in order to estimate the fluidity of cement Paste. For quantitatively evaluating the measured data this study also investigated the calibration of the rheology consistent, such as yield value and plastic viscosity, of cement paste using viscometer For this purpose the present work discussed the influence of 3 type of ordinary portland cement with different companies, affecting the fluidity of cement paste. and it also demonstrated the influence of the various kinds of mineral admixtures, such as fly ash(FA), blast furnace slag(BS) and silica fume(SF) and that of incorporating ratio. The author concluded that using R-F apparatus is the most effective flow test method of cement paste and it is exactly proportional to other apparatus' rheological properties.

• Proceedings of the Computational Structural Engineering Institute Conference
• /
• 1995.10a
• /
• pp.185-193
• /
• 1995

The softening behaviors of concrete have been the object of numerous experimental and numerical studies, because the load carrying capacity of cracked concrete structure is not zero. Numerical studies are devoted to the investigation of three-dimensional softening behaviors of concrete on the basis of a viscoplastic theory, which may be able to represent the effects of plasticity and also of rheology. In order to properly describe material behaviors corresponding to different stress levels, two surfaces in stress space are adopted; one is a yield surface, and the other is a failure or bounding surface. When a stress path reaches the failure surface, it is considered that the softening behaviors are initiated as micro-cracks coalesce and are simulated by assuming that the actual strain increments in the post-peak region are less than the equivalent viscoplastic strain increment. The experimental studies and the finite element analyses have been carried out under the displacement control. Numerically simulated results indicate that the model is able to predict the essential characteristics of concrete behaviors such as the non-linearity, stiffness degradation, different behaviors in tension and compression, and specially dilatation under uniaxial compression.

• Advances in concrete construction
• /
• v.11 no.2
• /
• pp.141-149
• /
• 2021

This study is a basic research for evaluating the buildability of cementitious materials for three-dimensional (3D) printing. In the cement paste step, the thixotropy behavior according to the resting time, which represents the time interval between each layer, was analyzed. In addition, the relationship between the thixotropy behavior and 3D concrete printing buildability was derived by proposing a measurement method that simulates the 3D concrete printing buildup process. The analysis of the tendency of the thixotropy behavior according to the resting time revealed that the area of the hysteresis loop (AHyst) showed a tendency to increase and then converge as the resting time increased, which means hysteresis loop approach critical resting time for sufficient buildability. In the thixotropy behavior analysis that simulates the 3D concrete printing buildup process, the buildup ratio, which is the recovery rate of the shear stress, showed a tendency to increase and then converge as the resting time increased, which are similar results like hysteresis loop. It was concluded that AHyst and the buildup ratio can be used as parameters for determining the resting time, and they have close relationships with 3D concrete printing buildability.

• Geomechanics and Engineering
• /
• v.12 no.5
• /
• pp.849-862
• /
• 2017

With growing interests in using bacterial biopolymers in geotechnical practices, identifying mechanical properties of soft gel-like biopolymers is important in predicting their efficacy in soil modification and treatment. As one of the promising candidates, dextran was found to be produced by Leuconostoc mesenteroides. The model bacteria utilize sucrose as working material and synthesize both soluble and insoluble dextran which forms a complex and inhomogeneous polymer network. However, the traditional rheometer has a limitation to capture in situ properties of inherently porous and inhomogeneous biopolymers. Therefore, we used the particle tracking microrheology to characterize the material properties of the dextran polymer. TEM images revealed a range of pore size mostly less than $20{\mu}m$, showing large pores > $2{\mu}m$ and small pores within the solid matrix whose sizes are less than $1{\mu}m$. Microrheology data showed two distinct regimes in the bacterial dextran, purely viscous pore region of soluble dextran and viscoelastic region of the solid part of insoluble dextran matrix. Diffusive beads represented the soluble dextran dissolved in an aqueous phase, of which viscosity was three times higher than the growth medium viscosity. The local properties of the insoluble dextran were extracted from the results of the minimally moving beads embedded in the dextran matrix or trapped in small pores. At high frequency (${\omega}>0.2Hz$), the insoluble dextran showed the elastic behavior with the storage modulus of ~0.1 Pa. As frequency decreased, the insoluble dextran matrix exhibited the viscoelastic behavior with the decreasing storage modulus in the range of ${\sim}0.1-10^{-3}Pa$ and the increasing loss modulus in the range of ${\sim}10^{-4}-1\;Pa$. The obtained results provide a compilation of frequency-dependent rheological or viscoelastic properties of soft gel-like porous biopolymers at the particular conditions where soil bacteria produce bacterial biopolymers in subsurface.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.27 no.2
• /
• pp.85-90
• /
• 2014

Ag paste has been used in the front electrode of the Si-solar cell. It is composed by Ag powder, glass frit, binder, solvent and dispersant. The role of the binder and the solvent is to make a flow and a printing property. However, it was not enough to report the printing properties with the variation of binder in the controled viscosity. In this study, we selected 3 kinds of typical binder which were used as binder for the paste in the industry, such as Ethyl cellulose, Hydroxypropyl cellulose and Acrylic. Ag pastes using these were prepared, controled viscosity and printed on the SiNx coated Si wafer. In the 'A paste' used Acrylic binder, printed hight was highest and 'H paste' used Hydroxypropyl cellulose binder was lowest. Because 'H paste' was high viscosity due to the molecular weight, the solvent was added in the paste to control the viscosity. Therefore, the content of solid was lower in 'H paste'. The relative pattern width which is related to the spreading of paste was the best in the case of 'H paste' and 'EH paste' at $30^{\circ}C$. It is thought that the optimization of the relative pattern width is possible for a paste by the controling shear thinning phenomenon. In the case of 'A paste', though printing hight was best, the pattern width was dependant on the temperature.

• Journal of Korean Tunnelling and Underground Space Association
• /
• v.20 no.6
• /
• pp.989-1002
• /
• 2018

Grouting for the rock joint is to strengthen the rock strata by infiltrating cement grout materials into the rock joints. Grouting is one of a field of study which is difficult to develop deterministic and quantitative design approach because of multiphase behaviors of grout materials and 3 dimensional features of rock joints. Therefore, GIN (Grouting Intensity Number) can be a good index with appropriate monitoring of pressure and volume of grout. In this paper, we investigate the effects of joint roughness (JRC) and rheology of cement material during the infiltration of cement grout material into rock joint through CFD (computational fluid dynamics) analyses. With rough joint surface and increase of WC ratio, the frictional resistance during the grouting increases. The results have been summarized with polynomial correlations.

• Advances in concrete construction
• /
• v.8 no.2
• /
• pp.155-163
• /
• 2019

The objective of this study was to derive a cementitious material for three-dimensional (3D) concrete printing that fulfills key performance functions, extrudability, buildability and bondability for 3D concrete printing. For this purpose, the rheological properties shown by different compositions of cement paste, the most fundamental component of concrete, were assessed, and the correlation between the rheological properties and key performance functions was analyzed. The results of the experiments indicated that the overall properties of a binder have a greater influence on the yield stress than the plastic viscosity. When the performance of a cementitious material for 3D printing was considered in relation with the properties of a binder, a mixture with FA or SF was thought to be more appropriate; however, a mixture containing GGBS was found to be inappropriate as it failed to meet the required function especially, buildability and extrudability. For a simple quantitative evaluation, the correlation between the rheological parameters of cementitious materials and simplified flow performance test results-time taken to reach T-150 and the number of hits required to reach T-150-in consideration of the flow of cementitious materials was compared. The result of the analysis showed a high reliability for the correlation between the rheological parameters and the time taken to reach T-150, but a low reliability for the number of hits needed for the fluid to reach T-150. In conclusion, among several performance functions, extrudability and buildability were mainly assessed based on the results obtained from various formulations from a rheological perspective, and the suitable formulations of composite materials for 3D printing was derived.

• The Korean Journal of Rheology
• /
• v.11 no.2
• /
• pp.82-90
• /
• 1999

Electrorheological(ER) fluid is a material that shows the dramatic change of rheological properties under an electric field and responds reversibly in a few milliseconds. ER fluid's response to an electric field along with its fast switching capability allows ER devices to be precisely controlled. The real application with ER fluid, however, has many limitations to be overcome; temperature fluctuation, moisture, dust, aggregation, precipitation, and low yield stress, for example. The magnitude and the characteristics of yield stress of ER fluid plays an important role in practical applications. In this research, a dynamic simulation on the squeezing flow of the ER fluid was carried out. Numerical simulation on isolated chains was performed to find out the effect of hydrodynamic and electrostatic force depending on the chain location, the squeezing rate, and the chain structure. Suspension model that is composed of a large number of particles was also investigated. The increase of normal stresses as well as the existence of a yield stress at an earlier stage could be observed, and the effective control of the normal stresses could be achieved at an optimal condition of the hydrodynamic force and the electrostatic force.

• Journal of the Korea institute for structural maintenance and inspection
• /
• v.25 no.6
• /
• pp.193-198
• /
• 2021

In this study, the rheological characteristics and of 3D printing composite materials and the compressive strength characteristics according to the lamination patterns were evaluated. As a result of rheology test, rapid material change was observed after 60 minutes of extrusion, yielding stress 1.4 times higher than immediately after mixing, and plastic viscosity was 14.94-25.62% lower. The compressive strength of the specimens manufactured in the mold and the laminated specimens were compared, and the lamination pattern of the laminated specimens were 0°, 45°, and 90° as variables. The compressive strength of the mold casting specimen and the laminated specimen from 1 to 28 days of age showed similar performance regardless of the lamination pattern. In particular, at the age of 28 days, the modulus of elasticity, maximum compressive strength, and strain at maximum stress of all specimens were almost the same. In order to analyze the interface of the laminated specimens, X-ray CT analysis of the specimen whose compressive strength were measured was performed. Through CT analysis, it was confirmed that cracks did not occur at the lamination interface, which can be judged that the interface in the laminated specimen behaved in an integrated manner.