• Journal of the Korean Ceramic Society
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• v.48 no.5
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• pp.458-462
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• 2011

The strength of ceramic was improved by lamination by suppressing the propagation of cracks with compressive residual stress in the face layer of the laminate. Hot pressed SiAlON+SiC/SiC/SiAlON+SiC laminate discs were fabricated for tailored residual stress. The residual stress in this laminate was studied by X-ray diffraction (XRD). There was considerable compressive residual stress in the face layer. A Finite Element Analysis (FEA) was performed to support the measured XRD results and to determine the stress field in the laminate. The residual stress measured by XRD had satisfactory agreement with the analytically calculated and FEA values. The measured value by XRD was -385 ${\pm}$ 20 MPa over most of the face layer. The calculated and FEA values were -386 MPa and -371MPa, respectively. FEA also showed significantly modified stresses and the maximum tensile stress near the edge region which are possible crack generators in the presence of flaws or contact damage.

• Korean Journal of Materials Research
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• v.22 no.2
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• pp.82-85
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• 2012

The effect of the alloy systems Al-Mg alloy and Al-Si alloy in this study on the characteristics of die-casting were investigated using solidification simulation software (MAGMAsoft). Generally, it is well known that the casting characteristics of Al-Mg based alloys, such as the fluidity, feedability and die soldering behaviors, are inferior to those of Al-Si based alloys. However, the simulation results of this study showed that the filling pattern behaviors of both the Al-Mg and Al-Si alloys were found to be very similar, whereas the Al-Mg alloy had higher residual stress and greater distortion as generated due to solidification with a larger amount of volumetric shrinkage compared to the Al-Si alloy. The Al-Mg alloy exhibited very high relative numbers of stress-concentrated regions, especially near the rib areas. Owing to the residual stress and distortion, defects were evident in the Al-Mg alloy in the areas predicted by the simulation. However, there were no visible defects observed in the Al-Si alloy. This suggests that an adequate die temperature and casting process optimization are necessary to control and minimize defects when die casting the Al-Mg alloy. A Tatur test was conducted to observe the shrinkage characteristics of the aluminum alloys. The result showed that hot tearing or hot cracking occurred during the solidification of the Al-Mg alloy due to the large amount of shrinkage.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.21 no.3
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• pp.405-413
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• 1997

In the present paper, it is attempted to reconfirm the "Intelligent" material properties using both the sintered TiNi/Al(1100) matrix composite made by powder metallurgy method and the squeeze-casted TiNi/Al6061 specimens. A metal matrix composite is, its fault has been considered to deteriorate a strength of composite by heating residual stress of the matrix. Therefore, it is necessary to remove a tensile residual stress, to produce the strength of a composite better. On the contrary, if compressive residual stress happens in matrix of composite in place of tensile residual stress, it will make the strength of composite better. So that, this paper introduce the development of a high strength of composite, by using compressive residual stress well, on the study. By using these specimens, shape memory strengthening effects in tensile strength and fatigue crack propagation above inverse transformation temperature of TiNi fiber were investigated. We occurs the prestrain and volume fraction for to discuss the effects of a composite strength. Moreover, by SEM observation, the effect of the residual stress at the interface between Al matrix and TiNi fiber and some brittle precipitation layers such as inter metallic compounds on fracture mechanisms was discussed metallurgically.urgically.

• Journal of Welding and Joining
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• v.6 no.4
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• pp.54-62
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• 1988

Major problems in welding Al-7020 include shrinkage, rpopositgy in welds and loss of strength in the heat affected zone. Thus it is important to examine the mechanical properties and reliability of welds. In this study, a series of experiments was carried out to determine the mechanical properties such as micro-hardness distribution, tensile strength, porosity and residual stress distribution of the Al-7020 weldment made by pulse-GMA welding. The resuts of the experiemnts are as folows. 1) The micro-hardness of weld metal and heat affected zone was lower than that of the base metal. 2) The tensile strength of the deposited metal was much lower than that of the base metal. 3) The porrosity in weld metal zone was negligible under the adopted conditsion of experiemnts. 4) The residual stress in the weld metal was lower than that of the heat affected zone, because the weld metal was softened. And the mciro-hardness distribution, the tensile strength and the residual stess distribution of the weldment in the as-welded condition were compared with those of the weldment after heat treatment.

• Journal of Environmental Science International
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• v.32 no.5
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• pp.385-394
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• 2023

There is a need for a method that can effectively remove wastewater containing small-sized particles such as TiO₂. In this study, we attempted to remove TiO₂ wastewater using electrocoagulation-electroflotation two-step separation. The TiO₂ wastewater was effectively removed via batch electrocoagulation-electroflotation separation. However, in the batch process, the simultaneous operation of electrocoagulation and electoflotation was challenging due to the high residual turbidity. In the continuous operation, electrocoagulation and electoflotation reactors were kept separate. The turbidity removal in continuous operation was similar to that in the batch process, nevertheless, the residual Al concentration was high, leading to the conclusion that counterterm ensures against residual Al were necessary.

• Journal of the Korean Society of Clothing and Textiles
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• v.21 no.5
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• pp.922-932
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• 1997

Blue jeans are finished with stonewashing process to give it optimal softness and color contrast of blue and white. So, Yellowing may well be generated during storage or use and thereby, their appearance may be damaged much. So, this study was aimed at finding the solutions to reduce the yellowing problem caused by residual metals after stonewshing. To this end, sample blue jeans were made to be finished with various methods of wet-treatment and then, be subject to daylight to check their photoyellowing. The results of this test can be summarized as follows; Since the stonewashing process was found to affect the yellowing, the residual metals of stone- washed blue jeans was analyzed. And it was found that it contained such residual metal as Al, Ca, Cu, Ti, Si, K and Zn. In particular, it was conceived that Al was a prime cause affecting the yellowing. Meanwhile, when the blue jeans were treated by the metal ionchelating agent of EDTA-2Na, the residual levels of Al and Ti were reduced by about 50%, while the photoyellolving was lowered by 75%, which is suggesed that EDTA is very effective in preventing the yellowing. On the other hand, when the blue jeans were bleached by the hypochlorite, chlorine remained in blue jean accelerated the yellowing. However, when this blue jean was treated again by the sodium thiosulfate for its dechloridization, the residual of chlorine was reduced, and the yellowing was lowered by about 43%.

• Journal of the Korean Society for Heat Treatment
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• v.36 no.2
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• pp.61-68
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• 2023

Ti and Ti alloys are used in the automobile and aerospace industries due to their high specific strength and excellent corrosion resistance. However their application is limited due to poor formability at room temperature and high unit cost. In order to overcome these issues, dissimilarly jointed materials, such as cladding materials, are widely investigated to utilize them in each industrial field because of an enhanced plasticity and relatively low cost. Among various dissimilar bonding processes, the rolled cladding process is widely used in Ti alloys, but has a disadvantage of low bonding strength. Although this problem can be solved through post-heat treatment, the mechanical properties at the bonded interface are deteriorated due to residual stress generated during post-heat treatment. Therefore, in this study, the microstructure change and residual stress trends at the interfaces of Ti/Al cladding materials were studied with increasing post-heat treatment temperature. As a result, compared to the as-rolled specimens, no difference in microstructure was observed in the specimens after postheat treatment at 300, 400, and 500℃. However, a new intermetallic compound layer was formed between Ti and Al when post-heat treatment was performed at a temperature of 600℃ or higher. Then, it was also confirmed that compressive residual stress with a large deviation was formed in Ti due to the difference in thermal expansion coefficient and modulus of elasticity between Ti Grade II and Al 1050.

• Journal of the Korean Ceramic Society
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• v.49 no.4
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• pp.301-307
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• 2012

SiAlON glasses are silicates or alumino-silicates, containing Mg, Ca, Y or rare earth (RE) ions as modifiers, in which nitrogen atoms substitute for oxygen atoms in the glass network. These glasses are found as intergranular films and at triple point junctions in silicon nitride ceramics and these grain boundary phases affect their fracture behaviour. This paper provides an overview of the preparation of M-SiAlON glasses and outlines the effects of composition on properties. As nitrogen substitutes for oxygen in SiAlON glasses, increases are observed in glass transition temperatures, viscosities, elastic moduli and microhardness. These property changes are compared with known effects of grain boundary glass chemistry in silicon nitride ceramics. Oxide sintering additives provide conditions for liquid phase sintering, reacting with surface silica on the $Si_3N_4$ particles and some of the nitride to form SiAlON liquid phases which on cooling remain as intergranular glasses. Thermal expansion mismatch between the grain boundary glass and the silicon nitride causes residual stresses in the material which can be determined from bulk SiAlON glass properties. The tensile residual stresses in the glass phase increase with increasing Y:Al ratio and this correlates with increasing fracture toughness as a result of easier debonding at the glass/${\beta}-Si_3N_4$ interface.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.21 no.5
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• pp.463-467
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• 2008

Aluminum nitride (AlN) thin films have been deposited on Au electrodes by using reactive RF magnetron sputtering method in a gas mixture of Ar and $N_2$ at different substrate temperature. It was found that substrate temperature was varied in the range up to $400^{\circ}C$, highly c-axis oriented film can be obtained at $300^{\circ}C$ with full width at half maximum (FWHM) $3.1^{\circ}$. Increase in surface roughness from 3.8 nm to 5.9 nm found to be associated with increase in grain size, with substrate temperature; however, the AlN film fabricated at $400^{\circ}C$ exhibited a granular type of structure with non-uniform grains. The Al 2p and N 1s peak in the X-ray photoelectron spectroscopy (XPS) spectrum confirmed the formation of Al-N bonds. The XPS spectrum also indicated the presence of oxynitrides and oxides, resulting from the presence of residual oxygen in the vacuum chamber. It is concluded that the AlN film deposited at substrate temperature of $300^{\circ}C$ exhibited the most desirable properties for the application of high-frequency surface acoustic devices.

• Journal of the Korean Society for Nondestructive Testing
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• v.26 no.5
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• pp.291-296
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• 2006

The residual stress in shot-peened Al 7075 alloy was evaluated using surface acoustic wave (SAW). Shot peening was conducted to produce a variation in the residual stress with the depth below the surface under a shot velocity of 30 m/s. The SAW velocity was measured from the V(z) curve using a scanning acoustic microscopy (SAM). The Vickers hardness profile from the surface showed a significant work hardening near the surface layer with a thickness of about 0.25 mm. As the residual stress became more compressive, the SAW velocity increased, whereas as the residual stress became more tensile, the SAW velocity decreased. The variation in the SAW velocity through the shot peened surface layer was in good agreement with the distribution of the residual stress measured by X-ray diffraction technique.