• Title/Summary/Keyword: Residual Al

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ENHANCED REMOVAL OF RESIDUAL ALUMINUM AND TURBIDITY IN TREATED WATER USING POLYMERS

  • Kim, Seung-Hyun
    • Environmental Engineering Research
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    • v.10 no.4
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    • pp.155-164
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    • 2005
  • This study investigated the possibility of reducing the residual aluminum (Al) in the treated water using polymers. Two raw waters (lake and river water) and three kinds of polymers (coagulant, flocculant, and filtration aids) were used for this purpose. This study found that coagulation at the high dose did not necessarily lead to the high concentration of the residual Al in the treated water. The coagulation efficacy was found more important in determining the residual Al than the coagulant dose. The use of a polymer enhanced the removal of turbidity as well as the residual Al. The coagulant aid removed the dissolved Al as well as the particulate Al by helping the coagulation and the solid-liquid separation. The flocculant aid and the filtration aid preferentially removed the particulate Al while helping the solid-liquid separation. The filtration aid reduced the residual Al substantially more effectively than the flocculant aid. The polyamine-based coagulant aid (FL) showed the better performance in reducing the residual Al and turbidity than DADMAC (WT). The cationic flocculant aid with weak charge density and the medium molecular weight (SC-020) showed the best performance in reducing the residual Al.

Measurement of Residual Stress of AlN Thin Films Deposited by Two-Facing-Targets (TFT) Sputtering System (Two-Facing-Targets (TFT) 스퍼터링장치를 이용하여 증착한 AlN박막의 잔류응력 측정)

  • Han, Chang-Suk;Kwon, Yong-Jun
    • Korean Journal of Materials Research
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    • v.31 no.12
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    • pp.697-703
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    • 2021
  • Aluminum nitride having a dense hexagonal structure is used as a high-temperature material because of its excellent heat resistance and high mechanical strength; its excellent piezoelectric properties are also attracting attention. The structure and residual stress of AlN thin films formed on glass substrate using TFT sputtering system are examined by XRD. The deposition conditions are nitrogen gas pressures of 1 × 10-2, 6 × 10-3, and 3 × 10-3, substrate temperature of 523 K, and sputtering time of 120 min. The structure of the AlN thin film is columnar, having a c-axis, i.e., a <00·1> orientation, which is the normal direction of the glass substrate. An X-ray stress measurement method for crystalline thin films with orientation properties such as columnar structure is proposed and applied to the residual stress measurement of AlN thin films with orientation <00·1>. Strength of diffraction lines other than 00·2 diffraction is very weak. As a result of stress measurement using AlN powder sample as a comparative standard sample, tensile residual stress is obtained when the nitrogen gas pressure is low, but the gas pressure increases as the residual stress is shifts toward compression. At low gas pressure, the unit cell expands due to the incorporation of excess nitrogen atoms.

A Study on the Relationship between Residual Stress and Wear Peroperty in Hypereutectic Al-Si Alloys (과공정 Al-Si 합금의 마모 특성에 미치는 잔류응력의 영향에 관한 연구)

  • Kim, Heon-Joo;Kim, Chang-Gyu
    • Journal of Korea Foundry Society
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    • v.20 no.2
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    • pp.89-96
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    • 2000
  • The effects of modification processing on the refinement of primary Si and the wear behavior of hyper-eutectic Al-Si alloys have been mainly investigated. Refining effects of primary Si in Al-17%Si alloy was more efficient than that of B.390 alloy. Optimum condition of getting the finest primary Si microstructure was when AlCuP modifier is added into the melt at $750^{\circ}C$ and held it at $700^{\circ}C$ for 30 minutes. Wear loss in the specimens of as-cast condition decreases as the size of primary Si decreases, in the order of B.390 alloy, B.390 alloy with AlCuP addition, Al-17%Si alloy and Al-17%Si alloy with AlCuP addition. Wear loss in the aged condition of Al-17%Si alloy, B.390 alloy and B.390 alloy with AlCuP addition decreased due to the increase of compressive residual stress in the matrix by the aging treatment. While, wear loss increased in the aged specimens of Al-17%Si alloy with AlCuP addition and Hepworth addition in which compressive residual stress decreases by the aging treatment. Therefore, it is assumed that higher compressive residual stress in the matrix can reduce the wear loss in composite materials such as hyper-eutectic Al-Si alloys.

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Study on a Residual Stress Reduce in Laser Welding Process using Ti6Al4V (티타늄 합금의 레이저 용접 공정 시 잔류 응력 저감 방안에 대한 연구)

  • Lee, Wooram;Park, Taesung;Park, Ikkeun
    • Journal of Welding and Joining
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    • v.34 no.6
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    • pp.35-41
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    • 2016
  • The experimental study has been performed through residual stress using the Ti6Al4V, investigate the effect of laser shock peening on laser welding process residual stress of Ti6Al4V welds in a reduce safety weld zone. This research evaluated the effects of shock waves from laser shock peening with a pulsed Nd:YAG laser on Ti6Al4V welding specimens, through the analysis of the residual stress of the specimens. The residual stress could be formed by the depth of 1 mm if the proposed method of reducing the residual stress is performed in the optimal condition. The welded structures and products during the production process increase the mechanical property of repeated stress, which could be expected to extend the fatigue life of the structure.

Effect of Residual Stress in Al5083 TIG Weld Region on Fatigue Crack Propagation Behavior (Al5083재 TIG용접부의 잔류응력이 피로균열전파거동에 미치는 효과)

  • Lee, Ouk-Sub;Park, Chan-Young
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.23 no.6 s.165
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    • pp.943-951
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    • 1999
  • The welded structure unnecessarily remains residual stress due to the very high heating of local region and lastly cooling. The residual stress sometimes causes fracture initiation of welded structures. In this paper, distribution and magnitude of tensile and compressive residual stresses in the TIG(Tungsten Inert Gas) welded aluminum alloy such as Al5083-H112 are measured by using the hole-drilling method. Furthermore, the effects of residual stresses in the TIG welded aluminum CCT(Center Crack Tension) and SEN(Single Edge Notched) Specimens on the fatigue crack propagation behavior are analyzed. The fatigue cracks initiated at residual stresses region are influnced by tensile and compressive residual stresses. However, the effects are found to be released fast for both cases according to the cyclic loads and extension of crack length.

Effects of Sand Blasting on TiAlN Coating on WC Hard Metal Alloy Tip (WC위 TiAlN 코팅층에 미치는 Sand Blasting 처리의 영향)

  • Lee, Han-Young
    • Tribology and Lubricants
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    • v.37 no.2
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    • pp.54-61
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    • 2021
  • The effect of the sand blasting before TiAlN coating in the manufacture of WC hard metal alloy tips have been studied. For four different tips, according to the status of processing of the sand blasting and the coating, residual stress measurement by X-ray diffraction and several tests for mechanical properties have been conducted. The results suggest that there was no difference in static mechanical properties, such as hardness, surface roughness and elastic modulus, between two coatings. Furthermore, compressive residual stress was generated equally on their surfaces. Additionally, the compressive residual stress in substrate WC was found to increase greatly when subjected to sand blasting treatment. However, the compressive residual stress decrease after coating regardless of sand blasting treatment. Nevertheless, it is confirmed that the compressive residual stress generated in the coating after sand blasting is less than that in the non-sandblasting coating. This was attributed to the plastic deformation occurring in the WC substrate during coating after sand blasting. In contrast to the scratch test results, sand blasting was assumed to have a negative effect on the adhesion between the coating and substrate. This is because there is a high possibility of microcracks due to plastic deformation in the WC substrate under the coating after sand blasting.

Evolution of grains to relieve additional compressive stress developed in Al-Mg alloy films during thermal annealing (Al-Mg 합금 박막의 압축응력 완화를 위한 어닐링 공정상의 입자 발달)

  • Lee, Jun-Seong;Yang, Ji-Hun;Jeong, Jae-In;Jeong, Yong-Hwa;Gwak, Yeong-Jin;Kim, Sang-Seop
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2014.11a
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    • pp.47-51
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    • 2014
  • In this work, a possible mechanism for grain evolution in Al-Mg alloy films during thermal annealing is suggested on the basis of the phase transition and the related residual stress. Al-Mg alloy films with compositions of 14.0 and 18.0 wt% Mg content were deposited on cold-rolled steel substrates by the direct current co-sputtering method using Al and Mg targets. After the deposition, the samples were thermally annealed at $400^{\circ}C$ for 10 min. The featureless, dense cross-sectional microstructure of the as-deposited films turned into a grainy microstructure after the thermal annealing. According to the residual stress evaluated by using the $XRD-sin2{\psi}$ technique and the phase analysis by XRD, it is likely that grains were created in order to relieve the additional accumulation of residual stress originating from the phase transition from face-centered cubic Al (${\alpha}$) to Al3Mg2 (${\beta}$) and Mg (${\delta}$) phases, suggesting interplay between the microstructure and residual stress.

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Mechanical Properties and Microstructure of AlN/W Composites (AlN/W계 복합재료의 기계적 특성과 미세구조)

  • 윤영훈;최성철;박철원
    • Journal of the Korean Ceramic Society
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    • v.33 no.1
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    • pp.83-91
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    • 1996
  • Monolithic AlN and AlN-W composites were fabricated by pressure-less sintering at 190$0^{\circ}C$ under nitrogen atmosphere and the influences of tungsten phase on the microstructure and mechanical properties were investi-gated. In the fabrication of sintered specimen no additive was used. And monolithic AlN showed substantial grain growth and low relative density. AlN-W composites were fully densified and grain growths of matrix were inhibited. The densification behavior of composites were inferred to be achieved through the liquid phase sintering process such as particle-rearrangement and solutino-reprecipitation. Also the oxid phases which is expected to form liquid phases duringsintering process were detected by XRD analysis. As the tungsten volume content increases fracture strength was decreased and fracture toughness was increased. It was suppo-sed that the strength decrease of composites with tungsten content was due to existence of interface phases. The subcritical crack growth behavior was observed from the stress-strain curve of composites. The effect of the secondary phase and interface phases on toughness in crease were studied through observation of crack propagation path and the influence of residual stress on crack propagation was investigated by X-ray residual stress measurement. In the result of residual stress measurement the compressive stress of matrix in composi-test was increased with tungsten volume content and the compressive stress distribution of matrix must have contributed to the inhibition of crack propagation.

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Effects of Re-Peening on the Compressive Residual Stress and Fatigue Life of Al7075-T6 (Al7075-T6의 압축잔류응력 및 피로 수명에 미치는 재피닝의 효과)

  • Oh, Sung-Hun;Lee, Yong-Sung;Cheong, Seong-Kyun
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.25 no.4
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    • pp.253-257
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    • 2016
  • The effects of re-peening on the compressive residual stress and fatigue life of Al7075-T6 were investigated. The compressive residual stress induced on the surface of components by shot peening is known to increase the fatigue life. However, the fatigue load relaxes the compressive residual stress of components. Re-peening is a technique to again induce the relaxed compressive residual stress and increase the total fatigue life of components. In this study, the re-peening process was applied to fatigue-loaded specimens. The compressive residual stress and fatigue life were examined for re-peened specimens with fatigue ratios of 30%, 50%, and 70%. The results showed that the compressive residual stress of the specimens was relaxed under the fatigue load. The re-peening process significantly increases the compressive residual stress and total fatigue life.

Evaluation of Coagulation-UF Process Considering Residual Aluminuim Concentration as Seawater Desalination Pretreatment (해수담수화 전처리 공정으로써 잔류 알루미늄 농도를 고려한 응집-UF 공정 연구)

  • Son, Dong-Min;Kang, Lim-Seok
    • Journal of Korean Society of Environmental Engineers
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    • v.35 no.7
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    • pp.495-502
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    • 2013
  • This work was performed to investigate proper condition of coagulation treatment as UF process pretreatment that consider UF permeate flux and residual Al concentration. The coagulant used an alum as $Al_2(SO_4)_3{\cdot}16H_2O$ and PACl (r = 1.5) made this study. The experiment was tested in adjusting conditions such as alum dose, flocculation time and coagulation pH of seawater. Consequently, higher coagulant dose lead to elevation of UF permeate flux while residual aluminium also increased in condition of pH 8.0. The most suitable condition which has a good permeate flux and low residual aluminium, in this works, was coagulant dose of 0.7 mg/L (as Al, alum) and 1.2 mg/L (as Al, PACl) and coagulation pH 6.5. In addition, applying the flocculation time with 1.2 mg/L of PACI reduced. The flocculation time reduced UF permeate flux in using alum.