• Title/Summary/Keyword: Reference standards

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A Study on the Evaluation of Uncertainty of Rockwell Hardness C Scale According to the Korean Industrial Standards(KS) (한국산업표준(KS)에 따른 로크웰 경도 시험기의 불확도 산정에 관한 연구)

  • Bahng, G.W.;Tak, Nae-Hyung
    • Journal of the Korean Society for Heat Treatment
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    • v.13 no.3
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    • pp.163-169
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    • 2000
  • Recently, uncertainty of hardeness became a major concem for the people working on the laboratory evaluation and accreditation. It is required to indicate uncertainty of hardness tester on the report after calibration. In addition to this, uncertainty of certified hardness reference block is also required to indicate on the certification sheet. Method on the evaluation of uncertainty in hardness measurement is agreed only recently for Rockwell hardness C scale. In this paper, a preliminary calculation of uncertainty based on type B evaluation has been made for hardness testers which satisfies the requirements of Korean Standards. It was found that the tolerance limit of mean value specified in KS should be increased to be compatible with the calculated uncertainty.

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Development of an Apparatus for In-situ Vacuum Gauge Calibration (In-situ 진공게이지 교정장치 개발)

  • Hong, S.S.;Lim, I.T.;Jho, M.J.;Chung, W.H.
    • Journal of the Korean Vacuum Society
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    • v.15 no.6
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    • pp.605-611
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    • 2006
  • We have developed in-situ vacuum gauge calibration system in the range 1 Pa to 100 kPa by using constant volume method. The system is capable of gauge calibration by comparison method without demount the reference gauges. The system will be useful for dissemination of national vacuum standards to foreign developing countries and domestic industries.

A Study on the Development of the Defense Standardization System (군수분야 표준화업무 발전방안)

  • Jeong, Ji-Sun;Kwon, Taek-Man;Hwang, Woo-Yull
    • Journal of Korean Society for Quality Management
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    • v.40 no.3
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    • pp.295-305
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    • 2012
  • Purpose: This study identified the standardization activities from the early stage of acquisition to disposal during the materiel life cycle and proposed the improvement of standardization process. Methods: Through improvement of duplicated deliberation for the revision of military specification, unification of technical change proposal reception organization, and resolution between the conflicting parts of laws and regulations, simplifying the standardization procedure and strengthening linkages between the civilian standards were gained. Results: We have redefined the concept of the standards and standardization in the field of defense and proposed the standards-driven documentary standards as a measurement standards and reference standards to expand the activities. Conclusion: Through a standardization survey, we came to conclusion that we need to change the concept of standardization in the field of national defense from making the specification to using the means of efficient management of military resources.

Optimization of Enzyme Digestion Conditions for Quantification of Glycated Hemoglobin Using Isotope Dilution Liquid Chromatography-Tandem Mass Spectrometry

  • Jeong, Ji-Seon
    • Mass Spectrometry Letters
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    • v.5 no.2
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    • pp.52-56
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    • 2014
  • Glycated hemoglobin (HbA1c) is used as an index of mean glycemia over prolonged periods. This study describes an optimization of enzyme digestion conditions for quantification of non-glycated hemoglobin (HbA0) and HbA1c as diagnostic markers of diabetes mellitus. Both HbA0 and HbA1c were quantitatively determined followed by enzyme digestion using isotope dilution liquid chromatography-tandem mass spectrometry (ID-LC-MS/MS) with synthesized N-terminal hexapeptides as standards and synthesized isotope labeled hexapeptides as internal standards. Prior to quantification, each peptide was additionally quantified by amino acid composition analysis using ID-LC-MS/MS via acid hydrolysis. Each parameter was considered strictly as a means to improve digestion efficiency and repeatability. Digestion of hemoglobin was optimized when using 100 mM ammonium acetate (pH 4.2) and a Glu-C-to-HbA1c ratio of 1:50 at $37^{\circ}C$ for 20 h. Quantification was satisfactorily reproducible with a 2.6% relative standard deviation. These conditions were recommended for a primary reference method of HbA1c quantification and for the certification of HbA1c reference material.

Quantification of $Cu(In_xGa_{1-x})Se_2$ Solar Cell by SIMS

  • Jang, Jong-Shik;Hwang, Hye-Hyen;Kang, Hee-Jae;Min, Hyung-Sik;Han, Myung-Sub;Suh, Jung-Ki;Cho, Kyung-Haeng;Chung, Yong-Duck;Kim, Je-Ha;Kim, Kyung-Joong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.275-275
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    • 2012
  • The relative composition of $Cu(InGa)Se_2$ solar cells is one of the most important measurement issues. However, quantitative analysis of multi-component alloy films is difficult by surface analysis methods due to severe matrix effect. In this study, quantitative depth profiling analysis of CIGS films was investigated by secondary ion mass spectrometry (SIMS). The compositions were measured by SIMS using the alloy reference relative sensitivity factors derived from the certified compositions and the total counting numbers of each element. The compositions measured by SIMS were linearly proportional to those by inductively coupled plasma-mass spectrometry (ICP-MS) using isotope dilution method. In this study, the quantification measured by ICP-MS method is compared with the composition calculated by SIMS depth profiles with AR-RSFs obtained from the reference. The SIMS depth profile of CIGS thin films according to the manufacturing condition was converted into compositional depth profile.

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Accurate Determination of Malachite Green and Leucomalachite Green in Fish using Isotope Dilution Liquid Chromatography/Mass Spectrometry (ID-LC/MS)

  • Ahn, Seong-Hee;Kim, Byung-Joo;Lee, Yun-Jung;Kim, Jeong-Kwon
    • Bulletin of the Korean Chemical Society
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    • v.31 no.11
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    • pp.3228-3232
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    • 2010
  • Malachite green (MG) has been used world-widely in aquaculture as a parasiticide or fungicide. Although MG performed successfully, it has not been permitted for use in aquaculture from European Union, USA, and Canada because of its carcinogenicity and mutagenicity. We developed a sensitive and specific method to determine MG and its principal metabolite, leucomalachite green (LMG), respectively by isotope dilution liquid chromatography mass spectrometry (ID-LC/MS). To enhance the extraction recovery of MG and LMG from fish tissue, an additional step, saponification, was introduced in sample preparation process to remove fat in sample extract, which hampered the performance of SPE columns. The residue of MG and LMG in fish was analyzed using liquid chromatography mass spectrometry in the selected ion monitoring (SIM) mode by monitoring at m/z 329 and 334 for MG and $d_5$-MG and at m/z 331 and 337 for LMG and $^{13}C_6$-LMG, respectively. This method was validated by comparing with the value of the reference material provided by Laboratory Government Chemistry (LGC). The results agreed within the measurement uncertainty and the accuracy was much improved than the provided reference value by LGC.

The Communication Protocol Model for Semiconductor Equipment with Internet of Things (사물인터넷을 이용한 반도체 장비 통신 프로토콜 모델)

  • Kim, Doo Yong;Kim, Kiwan
    • Journal of the Semiconductor & Display Technology
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    • v.18 no.4
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    • pp.40-45
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    • 2019
  • The smart factory has developed with the help of several technologies such as automation, artificial intelligence, big data, smart sensors and communication protocols. The Internet of things(IOT) among communication protocols has become the key factor for the seamless integration of various manufacturing equipment. Therefore, it is important that the IOT cooperate with the standards of communication protocols proposed by the SEMI in the semiconductor industry. In this paper, we suggest a novel reference model of the communication protocols for semiconductor equipment by introducing an IOT service layer. With the IOT service layer, we can use the functions and the additional services provided by the IOT standards that give the inter-operability between factory machines and host computers. We implement the standard of the communication protocols for semiconductor equipment with the IOT service layer by using ns3 simulator. It concludes that it is necessary to provide the platform for the IOT service layer to deploy efficiently the proposed reference model of the communication protocols.

Relative Humidity Transducer Proficiency Test for KOLAS Humidity Calibration Laboratories (KOLAS 교정기관 간 측정 동등성 확립을 위한 상대습도 변환기 숙련도 시험)

  • Sang-Wook Lee;Young-Suk Lee;Byung-Il Choi
    • Journal of Sensor Science and Technology
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    • v.32 no.6
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    • pp.447-454
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    • 2023
  • The Korea Laboratory Accreditation Scheme (KOLAS) operates accreditation programs for ensuring measurement traceability with the International System (SI) of Units - the highest calibration standard that measurements can be tested against. As of September 2023, there are 70 KOLAS-accredited laboratories in the Republic of Korea that specialize in humidity calibration. Among them, 32 KOLAS laboratories, along with one laboratory not affiliated with KOLAS, participated in the proficiency test (PM 2023-11) for relative humidity transducers in 2023. This proficiency test was conducted within a relative humidity range of 20-90% at a temperature of approximately 20 ℃, taking into consideration the calibration and measurement capability (CMC) of the participating laboratories. The primary objective of the proficiency test was to establish the measurement equivalence between each participating laboratory and the reference laboratory, by calculating the number of equivalence (En). When |En| was less than 1, the measurements from the participating and reference laboratory were equivalent. Out of the 33 participating laboratories, 32 successfully met this criterion and passed the proficiency test.

Development of the Logistics Process Reference Model for the Domestic Application of RosettaNet Standard (로제타넷 표준의 국내 적용을 위한 물류 프로세스 참조 모델 개발)

  • Kim, Sun-Ho;Choi, Hyuk-Seung
    • IE interfaces
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    • v.17 no.2
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    • pp.180-189
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    • 2004
  • In this paper, we propose a reference model for logistics processes to improve the effect of RosettaNet standards application to domestic industry. First of all, implementation cases applied to logistics processes in the world are investigated. Second, logistics processes of domestic manufacturers are analyzed for the application of RosettaNet standards, and the processes are compared with PIP. Finally, a new logistics processes model and corresponding PIP documents which reflect domestic situations are proposed.

Technology and Standardization in Telematics: Telematics Reference Model

  • Kim K. H.;Jang J. A.;Han E. Y.
    • Proceedings of the KSRS Conference
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    • 2004.10a
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    • pp.87-90
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    • 2004
  • Telematics is an emerging industrial field made up of the convergence of technologies. The key technologies for Telematics are server-side technology, terminal-side technology, communication-related technology, and positioning technology. Standardization in Telematics is now getting more notice these days. Domestic situation is explained for several related facilities such as ETRI, TTA, and Telematics Standardization Forum. In this paper, we will focus especially on the standard reference model that is the most fundamental framework of Telematics technology standardization. In the reference model, the Telematics system is composed of Telematics client part, communication part, and Telematics server part. The Telematics client part consists of terminal, positioning device, and car electronic devices. Communication part can be composed of various telecommunication channels such as CDMA, WLAN, DMB, WiBro, etc. which can guarantee the seamless two-way communication. Telematics server part is composed of TSP(Telematics Service Provider) server and CP(Contents Provider) servers gathering and managing the various Telematics services. This Telematics reference model is expected to be utilized as the base architecture in developing the technology and standards from now on.

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