• Korean Journal of Metals and Materials
• /
• v.48 no.1
• /
• pp.77-84
• /
• 2010

Annealing characteristics of an oxygen free copper (OFC) processed by differential speed rolling (DSR) were investigated in detail. An OFC sample with a thickness of hum was rolled to 35% reduction at ambient temperature without lubrication, varying the differential speed ratio from 1.0:1 to 2.2:1, and then annealed for 0.5h at various temperatures from 100 to $400^{\circ}C$. Different recrystallization behavior was observed depending on the differential speed ratio, especially in the case of annealing at $200^{\circ}C$ Complete recrystallization occurred in the specimens annealed at temperatures above $250^{\circ}C$ regardless of the differential ratios. The hardness distribution in the thickness direction of the rolled OFC sheets varied depending on the differential speed ratios. These annealing characteristics were explained by the magnitude of shear strain introduced during rolling.

• Korean Journal of Metals and Materials
• /
• v.56 no.12
• /
• pp.861-869
• /
• 2018

To determine the origin of the inhomogeneous microstructure and texture observed in drawn and annealed high purity copper wires, two kinds of drawing process conditions and their influence was investigated. The regular condition, based on a symmetric die, and a condition designed intentionally to produce an inhomogeneous shear deformation using an asymmetric die were employed. The difference in intensity of <111>-<100> distributed texture between the two wires confirmed that the wire drawn under the asymmetric die condition experienced a higher amount of shear deformation. The extensive shear strain in the wire drawn under the asymmetric die condition gave rise to inhomogeneous primary and secondary recrystallization behavior. After annealing at $200^{\circ}C$, grains with <100> texture, which were larger than the surrounding recrystallized grains, were extensively present on one half circle of the wire drawn under the asymmetric die condition, while larger grains with <100> were sparsely observed around the middle region of the wire drawn under the regular condition. Interestingly, the area where the larger grains with <100> texture existed was identical to the area where the high shear strain occurred during drawing in both wires. During annealing at $400^{\circ}C$, grains with <112> texture started to grow abnormally at the center of both wires as a result of secondary recrystallization. After annealing at $900^{\circ}C$ grains with <112> due to secondary recrystallization occupied the entire region of the wire drawn under the regular condition. On the other hand, in the wire drawn under the asymmetric die condition and then annealed at $900^{\circ}C$, the <100> oriented grains as a result of the normal grain growth of the larger <100> grains which were observed after annealing at $200^{\circ}C$, coexisted with the abnormally grown <112> grains. These results indicate that dynamic recrystallization induced by the shear strain during drawing plays an important role in the inhomogeneity of the microstructure and texture of wires after annealing.

• Journal of the Korean Vacuum Society
• /
• v.2 no.4
• /
• pp.468-473
• /
• 1993

Damages on Si substrate induced by Ar ion implantation and it annealing behavior during rapid thermal annealing were investigated by the cross-sectional TEM (transmissin electron microscopy), RB(Rutherfordbackscattering) spectra an dthermal wave (TW) modulation reflectance methods. Continuous amorphous layer extending to the surface were generated by Ar ion implantation for higher doses than 1 $\times$1015cm-2. The recrystallization of the amorphous layer prodeeded as the annealing temperature increased . However the amorphous /crystal interfacial undulations caused the micro twins and damage clusters. Damage clusters generated by lower doses than 1 $\times$1015 cm-2 disappeared slowly as the annealing temperature increased, but even at 110$0^{\circ}C$ a few damage clusters still remained.

• Journal of Korea Foundry Society
• /
• v.22 no.1
• /
• pp.11-16
• /
• 2002

Hot deformation behavior of GCD-50 cast iron has been investigated by employing the compressive test. Phenomenological deformation behaviors, which were modeled based on the dynamic materials model and the kinetic model, have been correlated with the microstructural change taken place during compression. Microstructural investigation revealed that the adiabatic shear band caused by the locallized deformation was taken place in low temperature and high strain rate. On the other hand, the wavy and curved grain boundaries, which repersent the occurrence of dynamic microstructure change such as dynamic recovery and dynamic recrystallization, were observed in high temperature and low strain rate. Deformation model based on hyperbolic sine law has also been suggested.

• Proceedings of the Korean Powder Metallurgy Institute Conference
• /
• 2006.09b
• /
• pp.855-856
• /
• 2006

In the present work, hot workability of particulate-reinforced Al6061-20%SiC composite produced by direct hot extrusion technique was studied. Uniaxial hot compression test at various temperatures and strain rates was used and the workability behavior was evaluated from the flow curves and the attendant microstructures. It was shown that the presence of SiC particles in the soft Al6061 matrix deteriorates the hot workability. Bulging of the specimens and flow lines were observed, which indicate the plastic instability during hot working. Microstructure of the composites after hot deformation was found to be heterogeneous, i.e. the reinforcement clusters were observed at the flow lines. The mechanism of deformation was found to be controlled primarily by dynamic recrystallization.

• Metals and materials international
• /
• v.24 no.6
• /
• pp.1249-1255
• /
• 2018

High temperature compression tests for newly developed Al-Zn-Mg alloy were carried out to investigate its hot deformation behavior and obtain deformation processing maps. In the compression tests, cylindrical specimens were deformed at high temperatures ($300-500^{\circ}C$) and strain rates of 0.001-1/s. Using the true stress-true strain curves obtained from the compression tests, processing maps were constructed by evaluating the power dissipation efficiency map and flow instability map. The processing map can be divided into three areas according to the microstructures of the deformed specimens: instability area with flow localization, instability area with mixed grains, and stable area with homogeneous grains resulting from continuous dynamic recrystallization (CDRX). The results suggest that the optimal processing conditions for the Al-Zn-Mg alloy are $450^{\circ}C$ and a strain rate of 0.001/s, having a stable area with homogeneous grains resulting from CDRX.

• Journal of the Korean Society for Heat Treatment
• /
• v.31 no.4
• /
• pp.180-186
• /
• 2018

High temperature flow behaviors of Fe-Cr-Mo-V-W-C tool steel were investigated using isothermal compression tests on a Gleeble simulator. The compressive test temperature was varied from 850 to $1,150^{\circ}C$ with the strain rate ranges of 0.05 and $10s^{-1}$. The maximum height reduction was 45%. The dynamic softening related to the dynamic recrystallization was observed during hot deformation. The constitutive model based on Arrhenius-typed equation with the Zener-Hollomon parameter was proposed to simulate the hot deformation behavior of Fe-Cr-Mo-V-W-C steel. An artificial neural network (ANN) model was also developed to compare with the constitutive model. It was concluded that the ANN model showed more accurate prediction compared with the constitutive model for describing the hot compressive behavior of Fe-Cr-Mo-V-W-C steel.

• Journal of the Korean Society for Heat Treatment
• /
• v.30 no.5
• /
• pp.187-196
• /
• 2017

High temperature flow behaviors of AISI 4340 steel were investigated using isothermal compression tests under the temperature range from 850 to $1100^{\circ}C$ and a strain rate from 0.01 to $10s^{-1}$. The flow stress decreased with increasing compression temperature and decreasing strain rate. The dynamic softening related to the dynamic recrystallization was observed during hot deformation. The constitutive model based on Arrheniustyped equation with the Zener-Hollomon parameter was used to simulate the hot deformation behavior of AISI 4340 steel. The modification of the Zener-Hollomon parameter and lnA parameter resulted in the improvement of the calculation accuracy of the proposed constitutive model compared with the experimental flow curves. In addition, the process map of AISI 4340 steel was proposed. The instable process condition for hot deformation was predicted and its reliability was verified with the experimental observation.

• Polymer(Korea)
• /
• v.31 no.5
• /
• pp.385-392
• /
• 2007

Poly (N-vinylpyrrolidone) (PVP) groups were grafted onto a poly(3-hydroxybutyrate-co-3-hydroryvalerate) (PHBV) backbone in order to modify its properties and synthesize a novel biocompatible copolymer. The crystallization behavior of PHBV and grafted PHBV was investigated by differential scanning calorimetry (DSC) and polarized optical microscopy (POM). During the cooling-induced crystallization process, the crystallization temperature and the crystallization rate of the grafted PHBV decreased with increasing PVP weight fraction. On the heating scans of all grafted PHBV samples, a new crystallization exothermic peak appeared at almost the same temperature, suggesting the operation of a recrystallization process, while the melting temperature ($T_m$) and the apparent enthalpy of fusion (${\Delta}H_f$) were not affected by graft modification. During the isothermal crystallization process at the same temperature, the presence of side PVP groups decreased the spherulitic growth rate and the spherulitic band spacing with increasing PVP weight fraction in samples.

• Korean Journal of Metals and Materials
• /
• v.49 no.7
• /
• pp.541-548
• /
• 2011

Thermomechanical fatigue (TMF) behavior of heat resistant austenitic stainless steel was evaluated in the temperature range from 100$^{\circ}C$ to peak temperatures of 600 to 800$^{\circ}C$; The fatigue lives under TMF conditions were plotted against the plastic strain range and the dissipated energy per cycle. In the expression of the inelastic strain range versus fatigue life, the TMF data obtained at different temperature ranges were located close to a single line with a small deviation; however, when the dissipated energy per cycle, calculated from the area of the stress-strain hysteresis loops at the half of the fatigue life, was plotted against the fatigue life, the data showed greater scattering than the TMF life against the inelastic strain range. A noticeable stress relaxation in the stress-strain hysteresis curve took place at the peak temperatures higher than 700$^{\circ}C$, but all specimens in this study exhibited cyclic hardening behavior with TMF cycles. Recrystallization occurred during the TMF cycle concurrent with the formation of fine subgrains in the recrystallized region, which is considered to cause the cyclic hardening of the steel.