• Title/Summary/Keyword: Quantitative and Objective

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Validation of the Analytical Procedure for Quantitative Determination of Four Trace Metals (As, Cd, Pb, and Hg) in Fish Lipids Using Inductively Coupled Plasma-Mass Spectrometry (ICP-MS)

  • Kasun S. Jayakody;Ranjith K. B. Edirisinghe;Suchithra A. Senevirathne;Lalith Senarathna
    • Mass Spectrometry Letters
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    • v.15 no.3
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    • pp.149-157
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    • 2024
  • The objective of the present study was to validate the analytical procedure for the quantitative determination of four trace metals (As, Cd, Pb, and Hg) in extracted fish lipids using Inductively Coupled Plasma-Mass Spectrometry, ICP-MS. The extracted lipids using Bligh and Dyer method were digested by means of microwave-assisted acid digestion and introduced into an optimized ICP-MS instrument. The validation of the analytical method was carried out in accordance with the international standards and guidelines outlined in the European Pharmacopeia (2022), which included specificity, selectivity, linearity, limit of detection, limit of quantification, precision, and accuracy. The linearity ranges of the calibration curves were R2 > 0.999, while the relative standard deviation (%RSD) for precision was within 5%. All targeted trace metals have shown mean recoveries between 88.0%-114.9%. The obtained LOD and LOQ values for this analytical protocol indicated the ability to detect and quantify of As, Cd, Pb, and Hg at trace levels. The overall validation confirms the described analytical method was appropriate for routine analyses of As, Cd, Pb, and Hg in fish lipids.

Research Trends in Inclusive Child-care for Young Children with Disabilities (어린이집 장애영유아 통합보육에 관한 연구 동향)

  • Cho, Kwi Hee;Mun, Ye Eun;Lee, Joo-Yeon
    • Korean Journal of Childcare and Education
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    • v.16 no.1
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    • pp.21-49
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    • 2020
  • Objective: The purpose of this study was to understand the research trends of inclusive child-care for young children with disabilities and suggest some implications for future research on inclusive child-care. Methods: There were a total 330 previous research papers about child-care inclusion, which means the practice of educating and caring for children aged 0 to 5 years old with disabilities alongside their typically developing peers at child-care centers. The studies were analyzed in terms of main research topic, subject, and research methods. Results: The major results of this study were as follow. First, a quantitative increase of the research since 2003 and a sharp increase of total research in this area since 2006 were found. Second, as a result of the main topic analysis, recognition and attitude research was the most frequently conducted, followed by the research about child-care programs, teacher and family support, and the effect of inclusive child-care. Third, more than half of the researches were done by teachers. Lastly, quantitative research methods were mainly used. Conclusion/Implications: Based on these findings, this study suggested to extend the research on inclusive child-care effect, intervention programs, non-disabled children, infants, and qualitative research.

Characteristics and Assessment of Printer Toner Adhesion (프린터 토너의 점착력 특성 및 평가 기법)

  • Lee, Jung-Eun;Kim, Kwang-Il;Kim, Hyun-Joon;Kim, Dae-Eun
    • Transactions of the Society of Information Storage Systems
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    • v.5 no.2
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    • pp.82-88
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    • 2009
  • Understanding the adhesion behavior and characteristics of toner film is required to achieve image and text printing with high quality resolution. Toner can be considered as a thin film coating on a media such as paper or polymer film. Quantitative measurement of adhesion characteristics of the thin film is important to assess the reliability of the system. In this work the main objective was to investigate the adhesion characteristic between the toner and the media by ramp loading scratch test method. The scratch test may be used to obtain quantitative information about the adhesion of the film to the substrate. In the scratch test a diamond tip was used to scratch the surface of the toner film under an increasing normal load until the toner detached or fractured. The critical load (LC) was obtained from the experimental results. Also, the relationship between the critical load and the adhesive strength of the interface between the substrate and the toner was obtained by measuring the normal and tangential forces during the scratch test. Finally, theoretical analysis of the toner scratch characteristics was performed based on Benjamin and Weaver theory, Plowing model, and Laugier model.

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The Antecedents of Relationship Marketing and Customer Loyalty: A Case of the Designed Fashion Product

  • KHOA, Bui Thanh
    • The Journal of Asian Finance, Economics and Business
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    • v.7 no.2
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    • pp.195-204
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    • 2020
  • Customer loyalty is a desired and essential result for companies in a business environment with a lot of competition, of which the fashion industry is no exception. For the fashion industry, the competition between businesses is increasingly fierce with the appearance of tailored fashion brands for each customer, also known as a designed fashion brand. The objective of this study is to examine the relationship between the antecedents of the relationship (reputation of designer, social media marketing) and customer relationship (trust and intimacy), and loyalty of customer for a designed fashion brand. The mixed research method is used to achieve research objectives with qualitative and quantitative research method. Qualitative data was collected through in-depth interview with 12 participants in Ho Chi Minh City, while quantitative data was collected by a survey of 799 respondents in Ho Chi Minh City and Hanoi City. The results show that the antecedents of relationship marketing positively affect on customer relationship and customer loyalty. Moreover, customer relationship has a positive impact on the customer loyalty when shopping for fashion products. From the research results, some managerial implications are also proposed for the designed fashion brands to improve the relationship marketing performance.

A Quantitative Analysis of Fatal Accidents Related to Cranes Using the FMEA Method (FMEA 기법을 활용한 크레인 관련 중대 재해의 정량적 분석에 관한 연구)

  • Kim, Hong-Hyun;Lee, Ghang
    • Journal of the Korea Institute of Building Construction
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    • v.7 no.3
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    • pp.115-122
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    • 2007
  • As buildings become higher, larger, and more complex, safety issues for construction workers working at such environments become more important. We analyzed 83 critical accident cases reported to the KOSHA(Korea Occupational Safety & Health Agency) for construction cranes by types of cranes and by patterns of accidents and causes. There are more number of accidents related to mobile cranes than that related to tower cranes, but the numbers of dead were similar in both cases. The most dominant cause of crane accidents was "fall of materials". We also analyzed the cases of crane accidents using the FMEA(Failure Mode and Effect Analysis) in order to set up a priority for safety management and also to prioritize research and development items relating tower cranes. In the process, we tried to eliminate subjective indexes such as an expert group survey and use objective and quantitative indexes. As a result, it was found that critical crane accidents occurs most during the "lifting and translating" activity.

Perceived Dark Rim Artifact in First-Pass Myocardial Perfusion Magnetic Resonance Imaging Due to Visual Illusion

  • Taehoon Shin;Krishna S. Nayak
    • Korean Journal of Radiology
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    • v.21 no.4
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    • pp.462-470
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    • 2020
  • Objective: To demonstrate that human visual illusion can contribute to sub-endocardial dark rim artifact in contrast-enhanced myocardial perfusion magnetic resonance images. Materials and Methods: Numerical phantoms were generated to simulate the first-passage of contrast agent in the heart, and rendered in conventional gray scale as well as in color scale with reduced luminance variation. Cardiac perfusion images were acquired from two healthy volunteers, and were displayed by the same gray and color scales used in the numerical study. Before and after k-space windowing, the left ventricle (LV)-myocardium boarders were analyzed visually and quantitatively through intensity profiles perpendicular the boarders. Results: k-space windowing yielded monotonically decreasing signal intensity near the LV-myocardium boarder in the phantom images, as confirmed by negative finite difference values near the board ranging -1.07 to -0.14. However, the dark band still appears, which is perceived by visual illusion. Dark rim is perceived in the in-vivo images after k-space windowing that removed the quantitative signal dip, suggesting that the perceived dark rim is a visual illusion. The perceived dark rim is stronger at peak LV enhancement than the peak myocardial enhancement, due to the larger intensity difference between LV and myocardium. In both numerical phantom and in-vivo images, the illusory dark band is not visible in the color map due to reduced luminance variation. Conclusion: Visual illusion is another potential cause of dark rim artifact in contrast-enhanced myocardial perfusion MRI as demonstrated by illusory rim perceived in the absence of quantitative intensity undershoot.

A Study on the Quantitative Analysis of Scientific Communication (학술 커뮤니케이션의 수량학적 분석에 관한 연구)

  • Kim Hyun-hee
    • Journal of the Korean Society for Library and Information Science
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    • v.14
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    • pp.93-130
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    • 1987
  • Scientific communication is an information exchange activity between scientists. Scientific communication is carried out in a variety of informal and formal ways. Basically, informal communication takes place by word of mouth, whereas formal communication occurs via the written word. Science is a highly interdependent activity in which each scientist builds upon the work of colleagues past and present. Consequently, science depends heavily on scientific communication. In this study, three mathematical models, namly Brillouin measure, logistic equation, and Markov chain are examined. These models provide one with a means of describing and predicting the behavior of scientific communication process. These mathematical models can be applied to construct quality filtering algorithms for subject literature which identify synthesized elements (authors, papers, and journals). Each suggests a different type of application. Quality filtering for authors can be useful to funding agencies in terms of identifying individuals doing the best work in a given area or subarea. Quality filtering with respect to papers can be useful in constructing information retrieval and dissemination systems for the community of scientists interested m the field. The quality filtering of journals can be a basis for the establishment of small quality libraries based on local interests in a variety of situations, ranging from the collection of an individual scientist or physician to research centers to developing countries. The objective of this study is to establish the theoretical framework for informetrics which is defined as the quantitative analysis of scientific communication, by investigating mathematical models of scientific communication.

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Volatile Aroma Compounds of Several Domestic Thymus quinquecostatus by Thermal Desorption Gas Chromatograph Mass Spectrometer (열탁착식 가스크로마토질량분석기에 의한 국내 산지별 백리향의 휘발성향기성분)

  • Chiang, Mae-Hee;Lee, Kwang-Woo;Baik, Jung-Ae
    • Journal of Bio-Environment Control
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    • v.20 no.1
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    • pp.14-20
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    • 2011
  • Objective of this research was to investigate the volatile aroma compounds and phenol contents for preservative effects. Aerial part of 5 Korean natured species of thyme located in Jeju alpine, jeju middle mountain, Kyeonggido, Ulleung island, and Gangwondo was analyzed by thermal desorption gas chromatograph mass spectrometer (TD-GC-MSD) method. Jeju middle mountain thyme was relatively high 62 species and has been investigated a high concentration of $7365.22{\mu}g/m^3$ contents according to the quantitative analysis. Total phenol contents containing thymol and carvacrol of Jeju middle mountain thyme were relatively high and showed 35.92%.

Development of Diagnosis of Trouble Model for Effective Operation of Air-compressor (효율적인 공기압축기 운영을 위한 이상진단모델 연구)

  • Im, Sang Don;Jung, Young Deuk;Kim, Jong Rae
    • Journal of the Korea Safety Management & Science
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    • v.16 no.3
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    • pp.239-248
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    • 2014
  • Most systems used in industrial sites, actually have non-linearity and uncertainty. Therefore there are a lot of difficulties in evaluating conditions of these systems. Generally, the quantitative analysis and expression are found hard because the general public cannot easily make an accurate interpretation on the systems. Thus development of a system that utilizes an expertise from skilled analysts is required. In this research, a real-time sensor signal conditioning system and Fuzzy-expert system have been separately set up into an inference algorithm. So that it ensures a fast, accurate, objective and quantitative operational condition value provided to the manager. Therefore, FE_AFCDM is suggested in this literature, as an effective system for diagnosing the problems related to the air compressor. It can quantify the uncertain and absurd condition to operate the air compressor facilities safely and financially.

Estimating the fisheries losses due to Chinese's illegal fishing in the Korean EEZ (중국어선 불법어업에 따른 수산부문 손실 추정)

  • Lee, Kwang-Nam;Jung, Jin-Ho
    • The Journal of Fisheries Business Administration
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    • v.45 no.2
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    • pp.73-83
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    • 2014
  • This study estimated quantitatively the loss of the fisheries due to China's illegal fishing that prevailed in the EEZ of the country in recent and has been an object to present a basic data in the implementation of government policy as to strengthen the enforcement capacity, setting up the direction of the crackdown of Chinese through to figure out an objective loss according to that. The analyzed result of this study setting a reasonable scenario, fisheries resources reduction is estimated about 67.5 million ton and the estimated amount of the loss is about 1.3 trillion won. This is 21.2% of about 318.3 ten thousand tons of the total fishery production of the country and accounts for 61.9% compared to coastal and offshore fisheries production. Therefore it is a very serious problem due to China's illegal fishing in Korea fisheries sector. It is significant to the point that estimating the qualitative and quantitative losses that can achieve a realistic and effective policy.