• 제목/요약/키워드: Quantitative Analysis

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실리콘에 도핑된 붕소의 정량분석에 대한 공동분석연구 (RRT Study for the Quantitative Analysis of Boron in Silicon)

  • 김경중;김현경;문대원;홍태은;정칠성;김이경;김재남;임철호;김정호
    • 한국진공학회지
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    • 제11권4호
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    • pp.218-224
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    • 2002
  • 반도체 박막의 분석에서 중요한 분석 대상의 하나인 미량 불순물의 정량분석을 위한 표준절차를 확립하고 그에 필요한 인증표준물질의 개발하였으며 이를 이용하여 국내공동분석을 실시하였다. 공동분석에 사용된 붕소가 균질하게 도핑된 박막 인증표준물질과 분석시편은 이온빔 스퍼터증착법에 의해 제작하였으며, 가장 정량적이고 감도가 높은 ICP-MS를 이용한 동위원소희석법으로 인증하였다. 이러한 인증표준물질과 SIMS에 의한 실리콘 내 의 붕소의 정량분석에 대해 이미 확립되어 있는 국제표준절차인 ISO/DIS-14237에 의거하여 국내 공동 분석을 시행하였는데, 이번의 공동분석에서 얻어진 붕소농도의 전체 평균값이 ICP-MS에 의한 인증치에 약 2% 정도의 오차를 보여주고 있어 분석의 정확성이 확인되었다.

영국과 한국의 건강도시 사업 평가방법 비교 연구: 리버풀과 원주시를 중심으로 (A Comparative Study of Healthy City Project Evaluation in U.K. and Korea: Focusing on Liverpool City and Wonju City)

  • 강신희;남은우;문지영
    • 보건교육건강증진학회지
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    • 제30권2호
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    • pp.93-103
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    • 2013
  • Objectives: This study was to compare two healthy cities, Liverpool in England and Wonju in Korea, which evaluated healthy city projects and to reorient evaluation strategy which fits into Korean Healthy cities. Methods: Comparatives analysis was used by reviewing documents, healthy city plan and evaluation report, of two cities. Results: Healthy city projects in two cities, fifteen programs were identical items among twenty-seven but there were differences in seven items for Liverpool and five items for Wonju. In Liverpool evaluation was done by a stakeholder group called Liverpool Local Involvement Network(LINK), while in Wonju by Yonsei Healthy City Research Center. The evaluation tool was two types; quantitative and qualitative analysis. Liverpool mostly used qualitative and added quantitative, vice versa in Wonju. Conclusions: Evaluation plan for Healthy city projects need to be made in the first phase of the projects, instead of in the end. Moreover, it is important to include stakeholder in conducting qualitative analysis for unquantifiable evidence of effectiveness, as well as quantitative analysis.

Quantitative Analysis of Bioactive Marker Compounds from Cinnamomi Ramulus and Cinnamomi Cortex by HPLC-UV

  • Jeong, Su Yang;Zhao, Bing Tian;Moon, Dong Cheul;Kang, Jong Seong;Lee, Je Hyun;Min, Byung Sun;Son, Jong Keun;Woo, Mi Hee
    • Natural Product Sciences
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    • 제19권1호
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    • pp.28-35
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    • 2013
  • In this study, quantitative and pattern recognition analysis for the quality evaluation of Cinnamomi Ramulus and Cinnamomi Cortex using HPLC/UV was developed. For quantitative analysis, three major bioactive compounds were determined. The separation conditions employed for HPLC/UV were optimized using an ODS $C_{18}$ column ($250{\times}4.6$ mm, 5 ${\mu}m$) with gradient conditions of acetonitrile and water as the mobile phase, at a flow rate of 1.0 mL/min and a detection wavelength of 265 nm. This method was fully validated with respect to linearity, accuracy, precision, recovery, and robustness. The HPLC/UV method was applied successfully to the quantification of three major compounds in the extract of Cinnamomi Ramulus and Cinnamomi Cortex. The HPLC analytical method for pattern recognition analysis was validated by repeated analysis of thirty eight Cinnamomi Ramulus and thirty five Cinnamomi Cortex samples. The results indicate that the established HPLC/UV method is suitable for quantitative analysis.

점토질 암석의 광물정량 분석법 연구 (A Study of Mineral Quantification on Clay-Rich Rocks)

  • 손병국;안기오
    • 광물과 암석
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    • 제35권4호
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    • pp.431-445
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    • 2022
  • 점토질 암석의 광물함량을 효과적이고 실용적으로 분석하는 방법을 X-선 분말회절분석 실험을 통하여 연구하였다. 점토질 암석의 X-선 분말회절 정량분석을 위해서는 측면마운팅(side mounting) 방법에 의한 무작위 배향(random orientation)의 전암(whole-rock) 분말시료의 준비가 필요하다. 또한, 암석을 구성하고 있는 점토광물의 감정을 위하여 2 ㎛ 이하 점토입도의 배향성 마운트(oriented mount)시편의 준비와 에틸렌글리콜 처리, 열처리 등의 실험과정이 요구된다. 정량분석을 위하여 RIR(reference intensity ratio)방법과 리트벨트(Rietveld) 회절도 계산 방법을 사용하였다. RIR값을 사용하여 전암 X-선 회절도로부터 총 점토 함량과 비점토광물(non-clay minerals)들의 함량을 얻을 수가 있었다. 또한, 점토입도의 배향성 X-선 회절도로부터는 각각 점토광물의 상대함량을 계산하여 이를 총 점토광물에 할당할 수가 있었다. 전암 X-선 회절의 리트벨트 방법에서는 10°(2θ) 미만의 X-선 회절 영역은 제외한 후에 리트벨트 회절도를 계산하였을 때 효과적인 정량분석 값을 얻을 수 있었다. 분석결과는 RIR방법과 리트벨트 방법이 서로 근사한 정량분석 값을 보여주었다. 따라서, 연구결과는 실험실에서의 일상적인 점토질암의 광물정량분석을 성공적으로 수행하는 것이 가능함을 지시한다. 그러나, 점토광물은 화학적 및 구조적 특정이 다른 수많은 변종이 존재하기 때문에 점토질암의 정량분석은 아직도 도전해야 하는 과제이다.

Studies on Determination of Aliphatic Carbamates -Quantitative Analysis of Carisoprodol-

  • Kim, Jeoung-Sook;Kim, Bak-Kwang
    • Journal of Pharmaceutical Investigation
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    • 제15권3호
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    • pp.151-159
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    • 1985
  • For the determination of aliphatic carbamates, the quantitative analysis of carisoprodol was investigated by gab chromatography (GC) and spectrophotometry. All the methods studied were found to be very quantitative. The minimum experimental amounts of GC method, spectrophotometric method I and II were approximately $10^{-9},\;10^{-5}$ and $10^{-8}$ mole, respectively. The obtained results showed that GC method I was much more sensitive and rapid than spectrophotometric method II.

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Quantitative Application of TM Data in Shallow Geological Structure Reconstruction

  • Yang, Liu;Liqun, Zou;Mingxin, Liu
    • 대한원격탐사학회:학술대회논문집
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    • 대한원격탐사학회 2003년도 Proceedings of ACRS 2003 ISRS
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    • pp.1313-1315
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    • 2003
  • This paper is dedicated to studying the quantitative analysis method with remote-sensing data in shallow geological structure reconstruction by the example of TM data in western China. A new method of computing attitude of geological contacts from remote-sensing data is developed and assessed. We generate several geological profiles with remotely derived measurements to constrain the shallow geological structure reconstruction in three dimensions.

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주거용 건물에서의 투영법에 의한 조망의 정량적 분석에 관한 연구 (A Study on the Quantitative Analysis of View by the Projection Method in the Residential Buildings)

  • 김용이;김광우
    • 한국주거학회논문집
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    • 제14권5호
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    • pp.37-46
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    • 2003
  • The quantitative analysis of view tells how surroundings and sky are showed, and requires understanding of visual perception and three dimensional information of buildings. The visual perception and the existing projection methods for view analysis are examined. The results of this study are as follows: The visual perception on the size is determined by the visual angle, which can be described as a solid angle. The analysis of view by planar projection can be narrow-sighted according to the size of the window and the location of the viewpoint, which will cause the obstacles in the normal direction of the window interfere the view. For the analysis of view by fisheye projection, the area around the focus point is calculated wider than other areas, and so the view ratio depends on the position of the focus point. When analyzing sky view by dividing the sky vault into the differential area, the distortion by projection can be minimized.

자율주행을 위한 레이더 기반 인지 알고리즘의 정량적 분석 (Quantitative Analysis of Automotive Radar-based Perception Algorithm for Autonomous Driving)

  • 이호준;채흥석;서호태;이경수
    • 자동차안전학회지
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    • 제10권2호
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    • pp.29-35
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    • 2018
  • This paper presents a quantitative evaluation method and result of moving vehicle perception using automotive radar. It is also important to analyze the accuracy of the perception algorithm quantitatively as well as to accurately percept nearby moving vehicles for safe and efficient autonomous driving. In this study, accuracy of the automotive radar-based perception algorithm which is developed based on interacting multiple model (IMM) has been verified via vehicle tests on real roads. In order to obtain experimental data for quantitative evaluation, Long Range Radar (LRR) has been mounted on the front of the ego vehicle and Short Range Radar (SRR) has been mounted on the rear side of both sides. RT-range has been installed on the ego vehicle and the target vehicle to simultaneously collect reference data on the states of the two vehicles. The experimental data is acquired in various relative positions and velocity, and the accuracy of the algorithm has been analyzed according to relative position and velocity. Quantitative analysis is conducted on relative position, relative heading angle, absolute velocity, and yaw rate of each vehicle.

만성 조현병 환자의 시계 그리기 검사 수행과 신경심리 기능 간의 관련성 (Relationship between Clock-Drawing Performance and Neuropsychological Functions in Patients with Chronic Schizophrenia)

  • 권미연;박민석;김명선
    • 대한조현병학회지
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    • 제23권1호
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    • pp.15-28
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    • 2020
  • Objectives: This study investigated the relationship between clock-drawing test (CDT) performance and neuropsychological functions in patients with chronic schizophrenia. Methods: Thirty-one patients with schizophrenia and 30 healthy controls participated in this study. The CDT was administered in three conditions and analyzed using both quantitative and qualitative scoring systems. Comprehensive neuropsychological tests were administered. Results: The results of the quantitative analysis showed that the schizophrenia group performed significantly worse in all three conditions of the CDT compared with the control group. However, no significant differences were observed between the two groups, when the IQ and educational level were controlled. The qualitative analysis showed that the schizophrenia group exhibited significantly more errors in "graphic difficulty" compared with the control group. In addition, CDT quantitative scores were significantly correlated with visuospatial function, memory, attention and executive functions in patients with schizophrenia. Conversely, each qualitative error type was correlated with specific cognitive domains. Furthermore, "graphic difficulty" and "spatial/planning deficit" were identified as predictors of depression symptoms in patients with schizophrenia. Conclusion: The present study demonstrated that the CDT is useful for assessing cognitive dysfunctions in patients with schizophrenia, while qualitative analyses provide more specific information about cognitive deficits compared with quantitative analyses.

Quantitative and Pattern Recognition Analyses for the Quality Evaluation of Magnoliae Flos by HPLC

  • Fang, Zhe;Shen, Chang Min;Moon, Dong-Cheul;Son, Kun-Ho;Son, Jong-Keun;Woo, Mi-Hee
    • Bulletin of the Korean Chemical Society
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    • 제31권11호
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    • pp.3371-3381
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    • 2010
  • In this study, quantitative and pattern recognition analysis for the quality evaluation of Magnoliae Flos using HPLC/UV was developed. For quantitative analysis, eleven major bioactive lignan compounds were determined. The separation conditions employed for HPLC/UV were optimized using ODS $C_{18}$ column ($250{\times}4.6\;mm$, $5\;{\mu}m$) with isocratic elution of acetonitrile and water with 1% acetic acid as the mobile phase at a flow rate of 1.0 mL/min and a detection wavelength of 278 nm. These methods were fully validated with respect to the linearity, accuracy, precision, recovery, and robustness. The HPLC/UV method was applied successfully to the quantification of eleven major compounds in the extract of Magnoliae Flos. The HPLC analytical method for pattern recognition analysis was validated by repeated analysis of twenty one reference samples corresponding to seven different species of Magnoliae Flos and nine samples purchased from market. The results indicate that the established HPLC/UV method is suitable for the quantitative analysis and quality control of multi-components in Magnoliae Flos.