• Transactions of the Korean Society of Mechanical Engineers A
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• v.21 no.2
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• pp.288-296
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• 1997

Curved beam elements with two nodes based on shallow beam geometry and strain interpolations are employed in eigenvalue analysis. In these elements, the displacement interpolation functions and mass matrices are consistent with strain fields. To assess the quality of the element mass matrix in free vibration problems, several numerical experiments are performed. In these analysis, both the inconsistent mass matrices using linear displacement interpolation function and the consistent mass matrices are used to show the difference. The numerical results demonstrate that the accuracy is closely related to the property of the mass matrix as well as that of the stiffness matrix and that the mass matrix consistent with strain fields is very beneficial to eigenvalue analysis. Also, it is proved that the strain based elements are very efficient in a wide range of element aspect ratios and curvature properties.

• Mass Spectrometry Letters
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• v.6 no.1
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• pp.21-25
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• 2015

In this paper, I describe the importance of matrix spraying conditions in imaging mass spectrometry (IMS) to obtain successful imaging results. My developed matrix application methodology, which is a "two-step matrix application" sequentially combined with matrix sublimation and spraying matrix solution can provide high reproducibility and high ion yield compared with a conventional direct spraying method. However, insufficient IMS results were obtained occasionally despite the two-step method. Therefore, I wanted to characterize the methodology to continuously provide high quality data. According to my results, the sublimation time was not a strict parameter, and the most important step was the first spraying condition. This means that the extraction conditions from the tissue section and co-crystallization of the matrix were the most important factors.

• Proceedings of the SCSK Conference
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• 2003.09b
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• pp.480-507
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• 2003

A rapid and efficient method for analyzing the nonionic surfactants and silicone polymers, which control the shape and characteristics of cosmetic products and give influence on product quality, has been developed using Matrix-Assisted Laser Desorption Ionization Time of Flight Mass Spectrometry (MALDI- TOF IMS). The MALDI-TOF/MS could easily and effectively determine the molecular weight distribution and monomer units of nonionic surfactants. As a result, creating a library of mass spectrum data of surfactants used in cosmetic products using MALDI-TOF/MS and analyzing surfactants extracted from the products may become a useful method for detailed structural characterization of the surfactants. Furthermore, the MALDI-TOF/MS analysis was effective in obtaining the spectrum of silicone polymers from which the molecular weight distribution could be determined. The repetition units and structural data could also be obtained through molecular mass peaks. Additionally, the monomer ratio and terminal groups as properties of silicone copolymers could be determined

• Geomechanics and Engineering
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• v.21 no.1
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• pp.11-21
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• 2020

The traditional formulations for estimation of bearing capacity in rock mechanics assume a homogeneous and isotropic rock mass. However, it is common that the rock mass consists of different layers of different rock properties or of the same rock matrix with distinct geotechnical quality levels. The bearing capacity of a heterogeneous rock is estimated traditionally through the weighted average. In this paper, the solution of the weighted average is compared to the finite difference method applied to a bilayer rock mass. The influence of different parameters such as the thickness of the layers, the rock type, the uniaxial compressive strength and the overall geotechnical quality of the rock mass on the bearing capacity of a bilayer rock mass is analyzed. A parametric study by finite difference method is carried out to develop a bearing capacity factor in function of the layer thickness and the rock mass quality expressed in terms of the geological strength index, which is presented in a form of a chart. Therefore, this correlation factor allows estimating the bearing capacity of a rock mass that is formed by two layers with distinct GSI, depending on the bearing capacity of the rock mass formed only by the upper layer and considered by that way as homogenous and isotropic rock mass.

• Mass Spectrometry Letters
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• v.11 no.4
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• pp.77-81
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• 2020

Characterization of the various chemical aspects of composite polymers is important for quality control of manufactured polymers. In this study, we compared three suitable matrices (α cyano-4-hydroxycinnamic acid [CHCA], 2,5 dihydroxy benzoic acid [2,5-DHB], and dithranol), to characterize various synthetic polymers by matrix-assisted laser desorption/ionization time-of-flight mass spectrometry. Although the spectra obtained with the CHCA and 2,5-DHB matrices were generally good, in certain samples ghost peaks disappeared only when dithranol was used as the matrix. Furthermore, we examined the use of sodium trifluoroacetate (NaTFA) as an additive to reduce interference by metals and copolymers in the spectra. In conclusion, appropriate selection of a matrix, according to the characteristics of the polymer, and the use of additives to improve sensitivity are important considerations for polymer analysis and development.

• Journal of Korean Society for Quality Management
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• v.46 no.3
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• pp.441-452
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• 2018

Purpose: The purpose of this paper is to study quantitative risk grade assessment for objective government quality assurance activities based on risk management in initial mass production for weapon systems. Methods: The Defense quality management regulations and foreign risk assessment documents are referred to analyze problems performing quality assurance actives. The failure rate data, maintainability and cost of products have been studied to quantify the risk Likelihood and impact. The analyzed data were classified as risk grade assessment through K-means Cluster Analysis method. Results: Results show that a proposed method can objectively evaluate risk grade. The analyzed results are clustered into three levels such as high, middle and low. Two products are allocated high, eleven low and seven middle. Conclusion: In this paper, quantitative risk grade assessment methods were presented by analyzing risk ratings based on objective data. The findings showed that the methods would be effective for initial mass production for weapon systems.

• Journal of the Korea Safety Management & Science
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• v.8 no.6
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• pp.55-78
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• 2006

In spite of the development of the service industry, research on measuring customers' service satisfaction is far insufficient. Therefore, ways to measure the service quality accurately need to be established due to the ambiguous types of service business. This research classifies the types of service business into service factory, service shop, mass service, professional service by using Schmenner's Service Process Matrix and conducts research on domestic literature that measured service satisfaction with Servqual and ServPerf. This study intends to suggest guidelines to measure customer satisfaction according to types of service business by researching ways to measure service satisfaction according to the types of service business and analysing the actual application methods based on a table that summarizes previous research on Servqual and Servperf.

• Journal of Korean Society of Environmental Engineers
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• v.36 no.6
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• pp.387-395
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• 2014

A highly sensitive analytical method based on stir bar sorptive extraction (SBSE) technique and gas chromatography/tandem mass spectrometry (GC-MS/MS) has been developed, allowing the simultaneous multi-analyte determination of 11 synthetic fragrances (SFs) in water samples. The stir bar coated with polydimethylsiloxane (PDMS) was added to 40 mL of water sample at pH 3 and stirred at 1,100 rpm for 120 min. Other SBSE parameters (salt effect and presence of organic solvent) were optimised. The method shows good linearity (coefficients > 0.990) and reproducibility (RSD < 10.9%). The extraction efficiencies were above 83% for all the compounds. The limits of detections (LOD) and limits of quantification (LOQ) were 2.1~4.1 ng/L and 6.6~12.9 ng/L, respectively. The developed method offers the ability to detect 11 SFs at ultra-low concentration levels with only 40 mL of sample volume. Matrix effects in tap water, river water, wastewater treatment plant (WWTP) final effluent water and seawater were investigated and it was shown that the method is suitable for the analysis of trace level of 11 SFs. The method developed in the present study has the advantage of being rapid, simple, high-sensitive and both user and environmentally friendly.

• Journal of Korean Society for Atmospheric Environment
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• v.22 no.1
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• pp.85-97
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• 2006

The PAMS data collected at four sites in Seoul metropolitan area in 2004 were analyzed using the positive matrix factorization (PMF) technique, in order to identify the possible sources and estimate their contributions to ambient VOCs. Ten sources were then resolved at Jeongdong, Bulgwang, Yangpyeong, and Seokmo, including vehicle exhaust, LPG vehicle, petroleum evaporation, coating, solvent, asphalt, LNG, Industry & heating, open burning, and biogenic source. The PMF analysis results showed that vehicle exhaust commonly contributed the largest portion of the predicted total VOCs mass concentration, more than $30\%$ at four sites. The contribution of other resolved sources were significantly different according to the characteristics of site location. In the case of Jeongdong and bulgwang located in urban area, various anthropogenic sources such as coating, solvent, asphalt, residual LPG, and petroleum evaporation contributed about $40\%$ of total VOCs mass. On the other hand, at yangpyeong and Seokmo located in rural and remote area, the portion of these anthropogenic sources was reduced to less than $30\%$ and the contribution of natural sources including open burning and biogenic source clearly observed. These results were considerably corresponding to the emission inventory investigated in this region.

• Mass Spectrometry Letters
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• v.14 no.4
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• pp.166-172
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• 2023

The utilization of methyl 2-aminobenzoate as a biocide and pesticide has raised concerns regarding its potential toxicity. To assess its safety, it is crucial to determine its quantity and related toxicity using reference materials (RMs) or certified reference materials (CRMs). As an RM and CRM containing methyl 2-aminobenzoate within a biocidal product matrix is currently unavailable, this study aimed to produce a high-quality RM containing methyl 2-aminobenzoate, ensuring its homogeneity and stability, following the ISO Guide 35 and ISO 17034. The study determined that the produced RM exhibited homogeneity, as indicated by a calculated F-value (1.91) smaller than the critical F-value (3.02). In the assessment of isochronous short-term stability, the slope of the linear regression for the RM showed no statistically significant difference from zero when stored at temperatures of 4, 18, and 60 ℃ for 4 weeks. Regarding classical long-term stability, the RM demonstrated sustained stability over the course of one year when stored at 4 ℃. This study has successfully developed an RM for monitoring methyl 2-aminobenzoate in biocides and pesticides. Its quality underwent rigorous evaluation, confirming both homogeneity and stability.