• Title/Summary/Keyword: Pure lead

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Piezoelectric and Dielectric Properties of (Na,K,Li)(Nb,Sb,Ta)O3 Ceramics as a Function of Fe2O3 Addition (Fe2O3첨가에 따른 (Na,K,Li)(Nb,Sb,Ta)O3계 세라믹스의 압전 및 유전 특성)

  • Lee, Gwang-Min;Shin, Sang-Hoon;Yoo, Ju-Hyun
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.27 no.9
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    • pp.555-560
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    • 2014
  • In this paper, in order to develop outstanding Pb-free composition ceramics, the $Fe_2O_3$-doped ($Na_{0.525}K_{0.443}Li_{0.037}$)($Nb_{0.883}Sb_{0.08}Ta_{0.037}$)$O_3$ + 0.3 wt% $Bi_2O_3$ + x wt% $Fe_2O_3$ (x= 0~1.0 wt%)(abbreviated as NKL-NST) lead-free piezoelectric ceramics have been synthesized using the ordinary solid state reaction method. The effect of $Fe_2O_3$-doping on their microstructure and electrical properties were investigated. XRD diffraction pattern studies confirm that $Fe_2O_3$ completely diffused into the NKL-NST lattice to form a new stable soild solution with $Fe^{3+}$ entering the $Nb^{5+}$, $Sb^{5+}$ and $Ta^{5+}$ of B-site. And, phase structure of all the ceramics exhibited pure perovskite phase and no secondary phase was found in the ceramics. The ceramics doped with 0.6 wt% $Fe_2O_3$ have the optimum values of piezoelectric constant($d_{33}$), planar piezoelectric coupling coefficient($k_p$) and mechanical quality factor($Q_m$) : $d_{33}$ = 233 [pC/N], $k_p$= 0.44, $Q_m$= 95. These results indicate that the ($Na_{0.525}K_{0.443}Li_{0.037}$)($Nb_{0.883}Sb_{0.08}Ta_{0.037}$)$O_3$ +0.3 wt% $Bi_2O_3$ + 0.6 wt% $Fe_2O_3$ ceramic is a promising candidate for lead-free piezoelectric ceramics.

Radiation parameterizations and optical characterizations for glass shielding composed of SLS waste glass and lead-free materials

  • Thair Hussein Khazaalah;Iskandar Shahrim Mustafa ;M.I. Sayyed
    • Nuclear Engineering and Technology
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    • v.54 no.12
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    • pp.4708-4714
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    • 2022
  • The novelty in the present search, the Soda-Lime-Silica (SLS) glass waste to prepare free lead glass shielding was used in order to limit the accumulation of glass waste, which requires extensive time to decompose. This also saves on the consumption of pure SiO2, which is a finite resource. Furthermore, the combining of BaO with Bi2O3 into a glass network leads to increased optical properties and improved attenuation. The UV-Visible Spectrophotometer was used to investigate the optical properties and the radiation shielding properties were reported for current glass samples utilizing the PhysX/PDS online software. The optical property results indicate that when BaO content increases in glass structure, the Urbach energy ΔE, and refractive index n increases while the energy optical band gap Eopt decreases. The result of the metallisation criteria (M) revealed that the present glass samples are nonmetallic (insulators). Furthermore, the radiation shielding parameter findings suggest that when BaO was increased in the glass structure, the linear attenuation coefficient and effective atomic number (Zeff) rose. But the half-value layer HVL declined as the BaO concentration grew. According to the research, the glass samples are non-toxic, transparent to visible light, and efficient radiation shielding materials. The Ba5 sample is considered the best among all the samples due to its higher attenuation value and lower HVL and MFP values, which make it a suitable candidate as transparent glass shield shielding.

A scientific analytical study on the sarira reliquary recovered from the octagonal ninestoried pagoda of Woljeongsa Temple (월정사 팔각구층석탑내 발견 유물의 자연과학적 분석 연구)

  • Hong, Jong-Ouk;Han, Min-Su;Lee, Oh-Hee
    • 보존과학연구
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    • s.25
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    • pp.5-29
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    • 2004
  • This research carried out ancient technique and composition of the relics recovered from the octagonal nine-storied pagoda of Woljeongsa temple using the scientific methods and obtained the following results. Firstly, The silver sarira inner case is consists of Ag, its materials comes out near 98wt%and comparing with the relics of Hwangnamdaechong, the contents of Ag and Ni are almost same with it. Secondly, The bronze sarira outer case, its contents of Cu is almost same with pure copper of which average is 99.7wt%. So, it should be named the copper sarira outer caserather than the bronze sarira outer case that has been called. Thirdly, The bronze mirror, though the contents of tin and lead are less than other contents which have been studied, they tend to have white color so they need to be made a close study. Especially, Because cultural property of nondestructive surface analytic method is not analyzed by the analysis of cross section and the moisten analysis, it may be occurred analytical errors by other factors.

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Reader Collision Avoidance Scheme for Mobile RFID-Sensor Integrated Networks

  • Ko, Doo-Hyun;Kim, Song-Min;Lee, Sang-Bin;An, Sun-Shin
    • Journal of IKEEE
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    • v.13 no.2
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    • pp.108-117
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    • 2009
  • In recent years, one of alternatives for constructing RFID networks that provide mobile services is using wireless sensor networks (WSN) to enhance network capacity, utility and scalability. Due to absence of compatible reader anti-collision control and channel capture phenomenon, the medium access control protocols as used in the RFID networks lead to reader collision and starvation problem. In this paper, we develop a MAC protocol which is called Enhanced Collision Avoidance MAC (ECO) to avoid reader to reader collisions in an integrated RFID network. ECO is a CSMA-based MAC protocol, and operates on integrated nodes which consist of a RFID reader and a mote. Performance evaluation shows superior results to pure-CSMA protocols under dense deployment environments, both in number of failures and in throughput.

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High-temperature Semiconductor Bonding using Backside Metallization with Ag/Sn/Ag Sandwich Structure (Ag/Sn/Ag 샌드위치 구조를 갖는 Backside Metallization을 이용한 고온 반도체 접합 기술)

  • Choi, Jinseok;An, Sung Jin
    • Journal of the Microelectronics and Packaging Society
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    • v.27 no.1
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    • pp.1-7
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    • 2020
  • The backside metallization process is typically used to attach a chip to a lead frame for semiconductor packaging because it has excellent bond-line and good electrical and thermal conduction. In particular, the backside metal with the Ag/Sn/Ag sandwich structure has a low-temperature bonding process and high remelting temperature because the interfacial structure composed of intermetallic compounds with higher melting temperatures than pure metal layers after die attach process. Here, we introduce a die attach process with the Ag/Sn/Ag sandwich structure to apply commercial semiconductor packages. After the die attachment, we investigated the evolution of the interfacial structures and evaluated the shear strength of the Ag/Sn/Ag sandwich structure and compared to those of a commercial backside metal (Au-12Ge).

An Analysis on the Performance of a Twin Stator Single-Phase Induction Manchine (단상 Twin sSator유도기의 특성해석에 관한 연구)

  • Young Moon Hwang
    • 전기의세계
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    • v.21 no.3
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    • pp.7-18
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    • 1972
  • An analysis is made for the performance of twin stator single-phase induction machine having any movable asymmetrical angle of stator windings, with any symmetrical or asymmetrical magnetizing reactance and winding turn-ratio between two stators, provided that asymmetrical common squirrel cage rotor is utilized. This mechanism is a new type, which has the advantage of mading only not the performance prediction in applications as a single-phase electromagnetic driving mechanism but also the analysis prediction of single-phase induction motor with not in quadrature axis. The basis of the analyses are lead by Kron's primitive machine matrix and Morrill's double-revolving field concept. All the performances can be calculated from the test values and design details of the asymmetrical magnetizing reactance twin stator single-phase induction machine and verified by test. And its validity is still demonstrated to the pure twin stator single-phase induction machine.

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Finite element analysis of axisymmetric extrusion with strain rate sensitive materials (속도의존성 재료에 대한 축대칭 전방압출의 유한요소 해석)

  • 최재찬;김병민;이종수;조남춘
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.15 no.2
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    • pp.537-543
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    • 1991
  • In this study, the strain rate effects are considered in the formulation by introducing the constitutive equation of the strain rate sensitive materials and rigid-viscoplastic finite element program is developed for axisymmtric extrusion. The effect of strain rate sensitivity on the flow characteristics and forming pressure are investigated and the experiments are carried out for extrusion with pure lead specimens. The theoretically predicted forming pressure showed reasonably good agreement with the experimental values.

Expression of Antibacterial Cationic Peptides from Methylotrophic Yeast, Pichia pastoris

  • Lee, Gang-U;Choe, Yun-Jae
    • 한국생물공학회:학술대회논문집
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    • 2000.11a
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    • pp.669-671
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    • 2000
  • Antimicrobial cationic peptides have attracted increasing research and clinical interest as a natural antibiotics due to their broad spectrum of antimicrobial activites and the rapid development of multidrug-resistant pathogenic microorganisms. In this study, first, we synthesized artificial fusion partner and cationic peptide genes (lactoferricin, magainin, protegrin-1, and indolicidin). Second, we constructed recombinant expression vectors and then transformed Pichia pastoris. Finally, expressed cationic peptides were purified and tested for their antimicrobial activites. Antimicrobial activity has been tested upon the appearance of clearing zone on the plate with the lawn of gram negative E.coli XL- I blue and garm positive Staphylococcus aureus. Protegrin-1 and Indolicidin have apparant activity of cationic peotides. This fusion technique may lead to a general and suitable tool for production of pure antimicrobial cationic peptides in Pichia pastoris.

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Fabrication of Undoped PbTiO3 Ceramics via Sol-Gel Processing (Sol-Gel Processing에 의한 순수 $PbTiO_3$ Ceramics 제조)

  • 김선욱;윤만순;임종인;김성숭;김남흥
    • Journal of the Korean Ceramic Society
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    • v.29 no.3
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    • pp.211-215
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    • 1992
  • Crack free PbTiO3 ceramics were produced by sol-gel processing using alkoxide, which has not been reported to be successful. The PbTiO3 gels were prepared from Ti alkoxide and lead acetate without any dopants. They were calcined at $600^{\circ}C$ and miled to produce fine PbTiO3 powder. It was pressed into discs and they were sintered at 110$0^{\circ}C$ for a few hours. The sintered ceramics were relativley hard and dense as having about 96% of theoretical density of PbTiO3. Fabrication of pure PbTiO3 ceramics by sol-gel processing is possibly due to their small grain size and uniform distribution of residual stress created during cubic-tetragonal transition over large number of small grains in fine grain PbTiO3 ceramics.

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An Elastohydrodynamic Lubrication of Elliptical Contacts : Part II - The Effect of Spin Motion (타원접촉의 탄성유체윤활 : 제2보 - 스핀운동의 영향)

  • Park, Tae-Jo
    • Tribology and Lubricants
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    • v.23 no.2
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    • pp.49-55
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    • 2007
  • A numerical analysis of elastohydrodynamic lubrication of elliptical contacts with both rolling and spinning has been carried out. A finite difference method with non-uniform grid systems and the Newton-Raphson method are applied to solve the problems. The velocity vectors resulting from combined spinning and rolling/sliding motion lead to asymmetric pressure distributions and film shapes. Pressure distributions, film contours and variations of the minimum and central film thicknesses are compared with various spin-roll ratios. Reduction of the minimum film thickness under spinning is remarkable whereas the central film thickness is relatively less. The spin motion have large effect on variations of the minimum film thickness with load parameter which are small in pure rolling/sliding cases. Therefore present numerical scheme can be used in the analysis of general elliptical contact EHL problems and further studies are required.