• Title/Summary/Keyword: Pulsed DC

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Surface hardening and enhancement of Corrosion Resistance of AISI 310S Austenitic Stainless Steel by Low Temperature Plasma Nitrocarburizing treatment.

  • Lee, Insup
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2012.11a
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    • pp.175-177
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    • 2012
  • A corrosion resistance and hard nitrocarburized layer was distinctly formed on 310 austenitic stainless steel substrate by DC plasma nitrocarburizing. Basically, 310L austenitic stainless steel has high chromium and nickel content which is applicable for high temperature applications. In this experiment, plasma nitrocarburizing was performed in a D.C. pulsed plasma ion nitriding system at different temperatures in $H_2-N_2-CH_4$ gas mixtures. After the experiment structural phases, micro-hardness and corrosion resistance were investigated by the optical microscopy, X-ray diffraction, scanning electron microscopy, micro-hardness testing and Potentiodynamic polarization tests. The hardness of the samples was measured by using a Vickers micro hardness tester with the load of 100 g. XRD indicated a single expanded austenite phase was formed at all treatment temperatures. Such a nitrogen and carbon supersaturated layer is precipitation free and possesses a high hardness and good corrosion resistance.

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Current-voltage Characteristics of Ceramics with Positive Temperature Coefficient of Resistance

  • Li, Yong-Gen;Cho, Sung-Gurl
    • Journal of the Korean Ceramic Society
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    • v.40 no.10
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    • pp.921-924
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    • 2003
  • A current-voltage relation for Positive Temperature Coefficient of Resistance (PTCR) ceramic was derived and compared with the experimental data. The new current-voltage relation was developed based on Heywangs double Schottky barrier model and a bias distribution across the grain boundary. The voltage limitation V < 4${\Phi}$$\sub$b/ suggested by Heywang is no longer necessary in the new expression for the voltage dependence of the resistance. The pulsed voltages were applied to the PTCR ceramic specimen in order to avoid possible temperature variation during the measurement.

Effect of Magnetic Field on NOx Removal for Wire-Plate Plasma Reactor (선대 평판형 플라즈마 반응기에서 NOx 제거에 미치는 자계의 영향)

  • Park, J.Y.;Son, S.D.;Han, S.B.;Lee, D.H.;Kim, J.D.;Mun, Y.H.
    • Proceedings of the KIEE Conference
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    • 1999.07e
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    • pp.2251-2252
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    • 1999
  • In this paper, the effect of magnetic field was measured on NOx removal characteristics for wire-plate plasma reactor with magnetic field applied to electric field vertically. NOx from simulated diesel engine flue gas are decomposed by the corona discharge of DC, AC and Pulsed voltages in wire-plate reactor. Consumption power increased with increasing discharge voltage. When magnetic field was applied to electric field vertically, consumption power decreased. NOx removal rate and arc transition voltage of plasma reactor with magnetic field were higher than those of plasma reactor without magnetic field.

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Directonal Square Pulse Generator construct for Blumlein lain (Blumlein 회로로 구성한 단방향 구형파 펄스 발생기)

  • Kim, Jung-Dal;Chang, Gi-Hyuk;Joo, Sung-Chul;Jung, Jang-Gun;Lee, Duck-Jin;Lee, Yong-Gill
    • Proceedings of the KIEE Conference
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    • 1998.07e
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    • pp.1779-1781
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    • 1998
  • We are going to design the Square Pulse Generator use of PCPS (Photo-Conductive Power Switch) for Blumlein lain. The circeuit is made of LC device and it is simulated by Schematics Evaluation Version 8.0 of MicroSim. After charged by DC voltage 15[kV]. When the switch is ON, Square pulse is generated after pause time 1.7857[${\mu}s$]. The square pulse is maximum peak voltage 13.987[kV], pulsed width 3.4017[${\mu}s$], rising time 0.7474[${\mu}s$], falling time 1.1718[${\mu}s$].

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Characteristics of Laser-Guided DC Discharge for Modes by Infrared Laser (모드 변화에 따른 적외선 레이저에 의한 방전 유도 특성)

  • Lee, D.H.;Nahm, G.H.;Kim, H.J.;Cho, J.S.
    • Proceedings of the KIEE Conference
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    • 1997.07e
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    • pp.1905-1907
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    • 1997
  • The experiments of laser-guided de discharge were carried out by using pulsed Nd:YAG laser radiation at low air pressure ranging from 0.3 to 20 torr. The minimum laser-guided de discharge voltages($V_{MD}$) at given pressure and distances between anode and cathode electrode were obtained. In order to generate TEM(transverse electromagnetic waves) modes, a pinhole was installed between a rod and a half mirror, and its diameter was adjusted from 6mm to 1.7mm. And then, we investigated the characteristics of laser-guided de discharge corresponding to different TEM modes. As a result, it was found that $V_{MD}$ at $TEM_{00}$ mode was lower than $V_{MD}$ at multimodes.

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Investigation of Charge distribution in an Electric double layer capacitor (전기이중층 캐패시터 내의 전하분포 고찰)

  • Endrowednes, Kuantama;Jessi, Darma;Sung, Youl-Moon;Kim, Kwang-Tae
    • Proceedings of the Korean Institute of IIIuminating and Electrical Installation Engineers Conference
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    • 2008.10a
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    • pp.201-204
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    • 2008
  • The use of the pulsed electro acoustic (PEA) method allowed us to perform the direct observations of spatio-temporal charge distributions in Electric double layer capacitors (EDLCs) based on polarizable nanoporous carbonaceous electrode. The negative charge density became the maximum, about 205 C/$m^3$ at the region where was near to collector layer in EDLCs for case $V_{DC}$ = 2.5 V, while the positively charged density became the maximum, about 61.1 C/$m^3$ at the region where it was located around the cathode layer. The PEA measurement used here is a very useful method to quantitively investigates the spatio-temporal charge distribution in EDLCs.

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Bipolar Pulse Bias Effects on the Properties of MgO Reactively Deposited by Inductively Coupled Plasma-Assisted Magnetron Sputtering

  • Joo, Junghoon
    • Applied Science and Convergence Technology
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    • v.23 no.3
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    • pp.145-150
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    • 2014
  • MgO thin films were deposited by internal ICP-assisted reactive-magnetron sputtering with bipolar pulse bias on a substrate to suppress random arcs. Mg is reactively sputtered by a bipolar pulsed DC power of 100 kHz into ICP generated by a dielectrically shielded internal antenna. At a mass flow ratio of $Ar/O_2$ = 10 : 2 and an ICP/sputter power ratio of 1 : 1, optimal film properties were obtained (a powder-like crystal orientation distribution and a RMS surface roughness of approximately 0.42 nm). A bipolar pulse substrate bias at a proper frequency (~a few kHz) prevented random arc events. The crystalline preferred orientations varied between the (111), (200) and (220) orientations. By optimizing the plasma conditions, films having similar bulk crystallinity characteristics (JCPDS data) were successfully obtained.

Corrosion Characteristics of Cast Stainless Steel under Plasma Ion Nitriding Process Temperature in Marine Environment (주조 스테인리스강의 해양환경 하에서 플라즈마 이온질화 공정온도에 따른 부식특성 연구)

  • Chong, Sang-Ok;Kim, Seong-Jong
    • Journal of the Korean institute of surface engineering
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    • v.50 no.6
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    • pp.504-509
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    • 2017
  • In order to improve corrosion resistance for cast stainless steel in seawater, the characteristics of corrosion resistance after plasma ion nitriding was investigated. Plasma ion nitriding process was conducted in a mixture of nitrogen of 25% and hydrogen of 75% at substrate temperature ranging from 350 to $500^{\circ}C$ for 10 hours using pulsed-DC glow discharge plasma with working pressure of 250 Pa in vacuum condition. Corrosion tests were carried out for as-received and plasma ion nitrided specimens. The corrosion characteristics were investigated by measurement of weight loss and observation of surface morphology. In anodic polarization experiment, relatively less damage depth and weight loss were presented at a nitrided temperature of $400^{\circ}C$, attributing to the formation of S-phase.

Development of $Al_2O_3-Ni$ FGMs Produced by Spark Plasma Sintering

  • Casari, Francesco;Zadra, Mario;Girardini, Luca;Molinari, Alberto
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.87-88
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    • 2006
  • Ceramic-Metal Functionally Graded Materials (FGM) are of great interest for application as Thermal Barrier Coating (TBC) or Wear Resistant Coating (WRC). Spark Plasma Sintering (SPS) is a promising techniques for time-saving consolidation of laminated/graduated powder systems: SPS is a pressure-assisted electrical sintering method which directly applies a pulsed DC current as heat source. In the present work, production of $Al_2O_3-Ni$ FGMs by means of Spark Plasma Sintering is considered; effect of sintering condition on density, hardness and fracture toughness is studied. Problems correlated to this new processing technology are discussed.

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The non-uniformity study of AZO thin films by pulse magnetron sputtering for large area (대면적 펄스 마그네트론 스퍼터링에 의한 AZO 박막의 균일도 문제)

  • Yang, Won-Gyun;Ju, Jeong-Hun
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2008.11a
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    • pp.23-24
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    • 2008
  • Bipolar pulsed dc magnetron sputtering을 이용하여 태양전지의 투명 전도막용으로 유리기판 위에 Al doped ZnO (AZO) 박막을 증착하였다. $400{\times}400\;mm$의 대면적 기판에 증착하기 위해서 $5{\times}25$ inch 대형 사각 AZO target (Al 2 wt%)을 사용했고, $50{\sim}250\;kHz$의 bipolar pulse를 인가하였다. 실제로는 $400{\times}400\;mm$ 면적의 기판에 slide glass 16개를 사용했으며, 약 700 nm 두께에서 두께와 투과도, 비저항의 균일도를 평가하였다. Bipolar pulse의 주파수 150 kHz일 때, 가장 우수한 특성을 갖는 AZO가 증착되었으며, $2.13{\times}10^{-3}{\Omega}{\cdot}cm$의 비저항에 가시광선 영역에서 82%의 투과율을 보였다. 또한, $400{\times}400\;mm$ 대면적 기판에서의 두께와 투과도, 비저항의 불균일도는 각각 5%, 1%, 9% 였다.

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