• 제목/요약/키워드: Pressure sintering process

검색결과 160건 처리시간 0.025초

Ceramic Diesel Particulate Filter Structure with Inclined Gas Paths

  • Hwang, Yeon;Kang, Dae-Sik;Choi, Hyoung-Gwon;Lee, Choong-Hoon
    • 한국세라믹학회지
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    • 제49권3호
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    • pp.226-230
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    • 2012
  • This paper presents a novel structure for a diesel particulate filter (DPF) with inclined gas paths, which was designed so that the gas paths offered a fluent flow of exhaust gases, and particulate matter (PM) was collected at pores formed in the body. The alumina porous filter was prepared by a conventional sintering process at $1200^{\circ}C$ for 2 h. Straight gas paths with $30^{\circ}$ of inclination from the gas flow direction were formed in the filter body. It is shown that this filter structure worked as a PM filter, in which 90.2% of soot filtration efficiency and 59.6 mbar of pressure drop were achieved.

가열이력 제어에 의한 $Si_3N_4$ 미분말 시편의 급속가열 (Rapid Heating of Ultrafine $Si_3N_4$ Powder Compacts under the Controlled Thermograms)

  • 이형직
    • 한국세라믹학회지
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    • 제30권3호
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    • pp.181-188
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    • 1993
  • The sintering and renitridation behaviors of ultrafine Si3N4 powder compacts, which were heavily oxidized and/or free-Si rich, were investigated with particular attentiion to microstructures. The specimens were heated without restoring to additives and pressure by controlling heating process attained a Xe image apparatus. The effect of particle size, free-Si contents, decomposition and renitridation, were investigated. When fired to 1$650^{\circ}C$ within 15 sec and then immediately held at 135$0^{\circ}C$ for 10min N2 atmosphere, significant densification took place in the limited region, in addition to decreasing oxygen contents to less than 0.3wt%. On the other hand, specimens decomposed due to overheating at the initial stage were rapidly renitridated at the relatively lower temperature of the holding stage. And, then, the activation energy for the renitridation was calculated to be 49kcal/mole.

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구역용융법으로 제작된 NdBaCuO 초전도체의 산소흡착 특성 (Oxygenation of Zone-melting NbBaCuO superconductor)

  • Soh, Dea-Wha;Fan, Zhanguo;Kim, Hee-Nam;Li, Xinyu;Gao, Weiying;Kim, Tae-Wan
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 추계학술대회 논문집 Vol.14 No.1
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    • pp.292-295
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    • 2001
  • The NdBaCuO superconducting samples were prepared by the Zone melting under low oxygen partial pressure. After the zone-melting the oxygenation process of the NdBaCuO samples in a oxygen flow furnace was studied. In order to compare the oxygenation condition the sintering NdBaCuO samples were studied also. In the study it is found that the optimum temperature for the oxygenation is $350^{\circ}C$, and the oxygen flow speed, the sample volume and the surface area of the sample would influence the oxygenation and the oxygen content.

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청동소재의 경도 및 마멸특성에 관한 실험적 연구 (Experimental Study on the Hardness and Wear Characteristics of Bronze Metals)

  • 김청균;김경섭
    • Tribology and Lubricants
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    • 제25권3호
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    • pp.192-196
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    • 2009
  • This paper presents the hardness and wear characteristic of bronze metals, which are manufactured by a sintering process with a high pressuring technology. A bronze metal with a high hardness and anti-wear properties is usually used for a high pressure cylinder and a pin-bush bearing. The new bronze metal in which is manufactured for this experimental study shows very high hardness of 192${\sim}$220 Hv compared with that of a conventional bronze metal of 120${\sim}$140 Hv. The high hardness of new bronze metals is strongly related to the radical reduction of wear volumes and an improved surface roughness of operated worn surfaces. As explained by previous many research works, the improved hardness of nonferrous metals may increase a load-carrying capacity and anti-wear properties of tribological components.

분무 열분해에 의한 미세 BSCCO 전구체 분말의 합성 (Synethisis of fine BSCCO precursor powder by spray pyrolysis)

  • 김성환;유재무;고재웅;김영국;박성창
    • 한국초전도저온공학회:학술대회논문집
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    • 한국초전도저온공학회 2003년도 추계학술대회 논문집
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    • pp.99-102
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    • 2003
  • Many researches on synthesis process for BSCCO precursor powders have been developed for high J$_{c}$ BSCCO-2223/Ag tape. Spray pyrolysis method for fabrication of precursor powder has many advantages, such as high purity, fine particle size of BSCCO precursor powder. Fine, spherical powders were prepared by ultrasonic spray pyrolysis from the aqueous solution of metal nitrates. BSCCO precursor powders were synthesized with 0.1 M concentration and heat treatment conditions. Average particle size for spray pyrolysis powders was 1.5 ~ 3 ${\mu}{\textrm}{m}$. BSCCO -2223/Ag tape was prepared by PIT method and followed by various sintering conditions. The critical current density of BSCCO-2223/Ag tape sintered in low oxygen partial pressure was ~ 23 kAcm$^{-2}$.

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구역용융법으로 제작된 NdBaCuG 초전도체의 산소흡착 특성 (Oxygenation of Zone-melting NdBaCuG Superconductor)

  • Soh, Dea-Wha;Fan, Zhanguo;Kim, Hee-Nam;Li, Xinyu;Gao, Weiying;Kim, Tae-Wan
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 추계학술대회 논문집
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    • pp.292-295
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    • 2001
  • The NdBaCuO superconducting samples were prepared by the Zone melting under low oxygen partial pressure. After the zone-melting the oxygenation process of the NdBaCuO samples in a oxygen flow furnace was studied. In order to compare the oxygenation condition the sintering NdBaCuO samples were studied also. In the study it is found that the optimum temperature for the oxygenation is $350{\circ}C$, and the oxygen flow speed, the sample volume and the surface area of the sample would if1uence the oxygenation and the oxygen content.

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Iron Aluminide-$SiC_p$ 혼합 예비성형체를 사용한 Al합금기 복합재료의 내마모 특성 (Wear Resistance of Al Alloy Matrix Composites Using Porous Iron Aluminide-$SiC_p$ Preforms)

  • 차재상;오선훈;최답천
    • 한국주조공학회지
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    • 제23권1호
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    • pp.30-39
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    • 2003
  • Porous hybrid preforms were fabricated by reactive sintering using the compacts consisting of SiC particles, Fe and Al powders. Squeeze casting processing was employed to produce the composite in which the matrix phase is Al-Si7Mg. The microstructural change and wear resistance of the composites were investigated in terms of an amount of SiC particles. The wear loss was increased with increasing the contact pressure in the alloy containing SiC particles coated with Cu. The most drastic change was found to the specimen tested at 2.5 MPa of contact pressure. Concerning the alloys containing SiC particles coated with Ni-P, a drastic increase in the wear loss exhibited at 2 MPa of contact pressure in those alloys containing 4 and 8 wt. % of SiC particles coated with Ni-P. In the alloy containing 16 wt. % a proportional increase in wear loss was observed to the change of contact pressure. With respecting to the sliding velocity, the wear loss of the alloy containing SiC particles coated with Cu increased at the initial stage of wear process and then decreased. Similar result was found in the alloys containing SiC particles coated with Ni-P. On the basis of the present results obtained, it was found that wear resistance of the alloys tested was improved to show in the order of the alloy reinforced by coated SiC particles > by uncoated SiC particles > by intermetallic compound without SiC particles.

자기펄스 압축성형법에 의한 다이아몬드 공구용 세그먼트 분말 성형 (Consolidation of Segment Powder for Diamond Tool by Magnetic Pulsed Compaction)

  • 윤종수;이정구;이민구;이창규;박문석;홍순직
    • 한국분말재료학회지
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    • 제15권5호
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    • pp.378-385
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    • 2008
  • This article presents the successful consolidation of the mixed Co and Diamond powders for a drilling segment by the combined application of magnetic pulsed compaction (MPC) and subsequent sintering, and their properties were analyzed. Homogeneous hardness (Hv 220) and density (97%) of sintered bulks fabricated by MPC were obtained by the new technique, where higher pressure has been employed for short period of time than that of general process. A fine microstructure and homogeneous hardness in the consolidated bulk were observed without cracks. Relatively higher drilling speed of 9.61 cm/min and life time of 6.55 m were found to the MPCed specimens, whereas the value of the specimens fabricated by general process was 11.71 cm/min and 7.96 m, respectively. A substantial improvement of mechanical properties of segment was achieved through this study.

$SrCO_3$$TiO_2$를 사용한 $SrTiO_3$의 합성반응에 관한 연구 (Synthesis of $SrTiO_3$ from the Mixtures of $SrCO_3$ and $TiO_2$)

  • 이종권;이병하
    • 한국세라믹학회지
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    • 제20권1호
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    • pp.43-48
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    • 1983
  • The formation of strontium titanate from several molar $SrCO_3$ and $TiO_2$ mixtures was studied in air and $CO_2$ gas Mixtures of $SrCO_3$ and $TiO_2$ were heated in air at 400-$600^{\circ}C$ DTA-TG was used to obtain thermal histories of simples heated in air and $CO_2$ gas. X-ray diffraction analysis was used to determine both the phase composition and the amounts of each phase present. The phase relationship of various compounds $SrTiO_3$, $Sr_2TiO_4$, $Sr_2Ti_3O_7$ and $Sr_4Ti_3O_{10}$ formed by the sintering in each composition was shown by the calibration curves. High temperature X-ray analysis was used to determine both the formation process and deformation process of each products. Small amount of SrTiO3 is formed first at the surface af contact SrTiO3 reacts with $SrCO_3$ to form Sr2TiO4 this is affected on the $CO_2$ pressure.

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온간 정수압 공정 조건에 따른 LTCC sheet의 수축률 (Influence of WIP conditions on dimensional change of LTCC sheet)

  • 정명식;윤여환;임성한;윤성만;오수익
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2008년도 춘계학술대회 논문집
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    • pp.507-511
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    • 2008
  • LTCC (Low Temperature Co-fired Ceramic) has been successfully applied to ceramic substrates for circuits and micro-fluidic systems and has proven its superior performance in a variety of applications. The prediction of shrinkage in LTCC process is an important for dimensional control of micro LTCC products which has influences on electronic characteristics. For avoiding the unpredictable shrinkage of LTCC during the sintering which makes accurate placement of the circuit devices difficult, pre-processes such as WIP (Warm Isostatic Pressing) and lamination must be modified. The objective of the present investigation is to establish a proper WIP conditions for near net shape fabrication of LTCC products. This paper discusses the influence of WIP conditions on the dimensional change of LTCC sheet. In the investigation, it is shown that the shrinkage values of sheets depend on WIP conditions and sheet directions. This work is a quantitative evaluation of the effect of WIP pressure on shrinkage of LTCC sheet. Additionally, the results show anisotropic shrinkage behaviour of sheet during LTCC process.

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