• 제목/요약/키워드: Precusor

검색결과 63건 처리시간 0.027초

Synthesis of Some new 2-Azolyl-and Azinylthiopyrimidines

  • Sherif, Laila-Abrahim;Sherif, Sherif-M.;Rasha-A.M. Faty;Fattah, Abdel-Samei-M. Abdel
    • Archives of Pharmacal Research
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    • 제18권1호
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    • pp.51-55
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    • 1995
  • A facile convenient syntheses of the titled compounds, via reacting the precusor 2-amino-2-(pentane-2, 4-dion-3-yithio)-6-phenylpyrimidine-5-carbonitrile (1) with nitrogen nucleophiles and with the carbanions of some active methylene compounds, is reported. Chemical and spectroscopic evidence of the newly syntheised compounds are described.

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비대칭 필터 구조를 이용한 적응형 선형 채널 등화기 (An Adaptive Linear Channel Equalizer Using Asymmetric Transversal Filter)

  • 한종영;임동국;김재명
    • 한국통신학회논문지
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    • 제30권9A호
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    • pp.830-837
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    • 2005
  • 다중경로 무선 채널 환경에서 지연확산에 따른 ISI를 제거하기 위한 등화기는 그 구조에 따라 선형과 비선형 구조로 구분할 수 있다. 본 논문은 ISI제거 성능이 개선된 적응형 선형 등화기를 제안한다. 제안된 등화기는 준 최적의 수신기인 MMSE 기반의 적응 등화기로써, 비대칭적인 구조의 등화 필터로 구성된다. 등화 필터의 비대칭적인 구조는 기준 탭을 필터 중앙으로부터 측면으로 이동시켜 구현하며, 이러한 구조는 precusor ISI와 postcusor ISI의 분리 제거를 가능하게 하여 기존의 선형 적응 등화기에 비해 향상된 ISI 제거 범위를 갖게 된다. UWB 시스템의 채널 모델인 S-V 채널에서 컴퓨터 모의실험을 통해 기존의 선형 적응 등화기와 제안된 등화기의 비튜오류율 성능을 비교한다.

자생식물 미치광이풀의 모상근배양에 의한 Tropane alkaloids 생산

  • 정희영;강민정;강영민;강승미;박우진;윤대진;박정동;최명석
    • 한국생물공학회:학술대회논문집
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    • 한국생물공학회 2001년도 추계학술발표대회
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    • pp.483-486
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    • 2001
  • Growth and tropane alkaloids(hyoscyamine and scopolamine) contents were studied in root cultures from Scopolia paruiflora. All excised roots grew well, even without an addition of a growth regulators. Scopolia roots could be divided scopolamine-rich species. Among the culture media, SH medium was the best for tropane alkaloids production from the hairy roots, whereas the growth increased in SH medium. In precusor experiments, feeding of hyoscyamine was promotive for scopolamine formation. Abiotic elicitors made a slightly production promotion effect.

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$TiCl_3$를 이용해서 합성된 $TiO_2$ 박막의 특성 (Characterisation of $TiO_2$ film synthesized using titaniumtetrachlo precusor)

  • 김강혁;이창근;이규환;김인수
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2003년도 추계학술발표강연 및 논문개요집
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    • pp.111-111
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    • 2003
  • The peroxo titanic acid solution was successfully prepared using titanium trichloride as a precursor. The basic properties of the TiO2 film prepared by the solution were investigated in view of phase change, bandgap energy, crystalline size etc. The film displayed amorphous TiO$_2$ at room temperature, anatase above 281$^{\circ}C$ and a mixture of anatase and rutile at 99$0^{\circ}C$, The crystalline size increases with annealing temperatures, while the bandgap energies decrease due to the quantum size effect and the formation of rutile phase which has low bandgap energy. As a result of TG-DTA, it was found that annealing treatment at 99$0^{\circ}C$ for 2h formed a mixtures of anatase and rutile through three steps: (1) the removal of physically adsorbed water (2) the decomposition of peroxo group (3) amorphous-anatase or anatase-rutile phase transformation.

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양측 신장비대로 진단된 급성림프구성 백혈병 1례 (Bilateral Nephromegaly as a Presenting Symptom of Acute Lymphoblastic Leukemia)

  • 김종호;박지민;정현주;박준은;배기수
    • Childhood Kidney Diseases
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    • 제13권2호
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    • pp.278-281
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    • 2009
  • 소아에서 혈액암의 경우 간비종대 없이 신장 비대만을 보이는 경우는 매우 드물다. 저자들은 한 달간 급속히 진행하는 복부 팽만을 주소로 병원에 온 9개월 된 남아에서, 간비종대가 없이 양측 거대신 소견만을 보이는 급성 림프구성 백혈병을 경험하였기에 그 임상상을 보고하는 바이다.

텅스텐 에톡사이드의 기상 반응을 이용한 초미립 WC 분말의 합성 (Synthesis of Nano-sized Tungsten Carbide Powders by Vapor Phase Reaction of Tungsten Ethoxide)

  • 가미다;하국현;김병기
    • 한국분말재료학회지
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    • 제10권1호
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    • pp.1-5
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    • 2003
  • Nano-sized WC powders were synthesized by vapor phase reaction using the precusor of tungsten ethoxide under helium and hydrogen atmosphere. The phases of the powder were varied with reaction Bone and gas flow rate. The powder size was about 30nm in diameter, and the tungsten carbide powder was coated by carbon layer. The synthesis of nano-sized WC powders was promoted as the hydrogen gas flow rate became higher. Inversely, tungsten oxide was formed by increasing the flow rate of helium gas. The synthesized powders were analyzed by XRD, FE-SEM, carbon analyzer etc.

PZT 후막의 치밀성 향상에 따른 PZT 다층 후막의 구조적 특성 (Structural properties of PZT multilayer thick films of improved densification)

  • 윤상은;이성갑;박상만;이영희
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2006년도 제37회 하계학술대회 논문집 D
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    • pp.2211-2212
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    • 2006
  • Ferroelectric PZT (70/30) thick films were fabricated by the screen printing method. And the PZT (30/70) precusor solution were infiltrated by the spin-coating method on the PZT thick films to obtain a densification. All PZT thick films were sintered at $1050^{\circ}C$ for 10 min. Structural properties, such as crystalline structure, microstructures and compositional ratio, of PZT thick films were investigated with the variation of the number of sol coatings using XRD, SEM and EDS, respectively. All PZT thick films exhibited a perovskite polycrystalline structure without a pyrochloer phase. The thickness of PZT thick films, 4-times screen-printed, was approximately $60{\mu}m$. And the densification of the PZT thick films increased with increasing the number of sol coatings.

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PZT 후막의 치밀성 향상에 따른 PZT 다층 후막의 구조적 특성 (Structural properties of PZT multilayer thick films of improved densification)

  • 윤상은;이성갑;박상만;이영희
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2006년도 제37회 하계학술대회 논문집 A
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    • pp.579-580
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    • 2006
  • Ferroelectric PZT (70/30) thick films were fabricated by the screen printing method. And the PZT (30/70) Precusor solution were infiltrated by the spin-coating method on the PZT thick films to obtain a densification. All PZT thick films were sintered at $1050^{\circ}C$ for 10min. Structural properties, such as crystalline structure, microstructures and compositional ratio, of PZT thick films were investigated with the variation of the number of sol coatings using XRD, SEM and EDS, respectively. All PZT thick films exhibited a perovskite polycrystalline structure without a pyrochloer phase. The thickness of PZT thick films, 4-times screen-printed, was approximately 60fm. And the densification of the PZT thick films increased with increasing the number of sol coatings.

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구형 가돌리늄화합물 입자 제조 (Preparation of Spherical Gadolinium Compound Particles)

  • 김응호;최청송;정경채;박진호;장인순
    • 한국세라믹학회지
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    • 제30권7호
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    • pp.563-570
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    • 1993
  • Spherical, monosized gadolinium compound was prepared by the reaction of Gd(NO3)3 solution with decomposition products of urea in the solution at evaluated temperature. Chemical composition and calcination characteristics of spherical gadolinium compound prepared were investigated by X-ray IR and TG-DTA. The approximate chemical composition of the spherical particle precipitated was Gd(OH)CO3.1.5H2O. Gd(OH)CO3.1.5H2O was calcined to monoclinic type Gd2O3 at 115$0^{\circ}C$ via cubic type Gd2O3 near $600^{\circ}C$. The effects of various parameters such as pH, temperature, concentration ratio of urea to gadolinium precusor, ageing time, and others material (CCl3COOH and HOCNH2) in stead of urea as precipitating agent on the properties of the resulting precipitates were studied systematically.

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솔나방(Dendrolimus spectabilis) 난소의 미세구조 II. 난황막 및 난각형성과정 (Ultrastructural Studies on the Oogenesis of the Pine moth, Dendrolimus spectabilis (Lasiocampidae) II. Vitelline Membrane and Chorion Formation)

  • 김지현;김정상;김우갑
    • Applied Microscopy
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    • 제24권4호
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    • pp.52-60
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    • 1994
  • The developing ovarian oocyte of Dendrolimus spectabilis has been studied by using electron microscopical techniques. After yolk formation the vitelline membrane was laid down in the intercellular space between the follicle cell and the oocyte. But before the vitelline membrane formation the granules with high electron density that the vitelline membrane precusor are observed in the follicle cell. At the late vitellogenesis stage these granules were transported into the intercellular space between the follicle cells and the oocyte. These granules fuse to each other and larger bodies which eventually produce the vitelline membrane. The vitelline membrane was distinguished into the light inner and dark outer membrane. Next the chorion was laid down. It was apparent that the chorion was laid down in the intercellular space immediately adjacent to the vitelline membrane, and that it was formed by the follicle cells only.

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