• Title/Summary/Keyword: Pre-Coating

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A Study on the Preparation of Ternary Transition Metal Coated-Dimensionally Stable Anode for Electrochemical Oxidation (전기화학적 산화를 위한 삼원 전이 금속 코팅 불용성 산화 전극 제조에 관한 연구)

  • Park, Jong-Hyeok;Choi, Jang-Uk;Park, Jin-Soo
    • Applied Chemistry for Engineering
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    • v.32 no.4
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    • pp.409-416
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    • 2021
  • Dimensionally stable electrodes are one of the important components in electrochemical water treatment processes. In the manufacturing of the dimensionally stable electrodes, the type of metal catalyst coated on the surface of the metal substrate, the coating and sintering methods substantially influence their performance and durability. In this study, using Ir-Ru-Ta ternary metal coating, various electrodes were prepared depending on the coating method under the same pre-treatment and sintering conditions, and its performance and durability were studied. As a coating method, brush and spray coating were used. As a result, the reduction in the amount of catalyst ink was achieved because more amount of metal could be coated for the electrode using spraying with the same amount of catalyst ink. In addition, the spray_2.0_3.0 electrode prepared by a specific spray coating method shows the phenomenon of cracking and the uniform coating of the ternary metal on the surface of the coating layer, and results in a high electrochemically active specific surface area, and the decomposition performance of 4-chlorophenol was superior to the other electrodes. However, it was found that there was no significant difference in durability depending on the coating method.

Rutherford Backscattering of Black Chrome Solar Selective Coatings (흑색크롬 태양광 선택흡수막의 Rutherford산란)

  • Lee, Kil-Dong;Chea, Young-Hi;Auh, Paul-Chung-Moo
    • Solar Energy
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    • v.10 no.1
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    • pp.57-62
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    • 1990
  • The influence of substrate materials on the thermal stability of black chrome coating was investigated by Rutherford backscattering spectrometry(RBS). In order to study thermal degradation the sample were annealed in air for 24 hour at temperature of 450. Cu, Ni, and S.S(Stainless steel 304) were used as substrate for selective coating. The experimental results of substrate diffusion was discussed. It was found that little diffusion of substrate material occurred for the sample pre. pared on stainless steel.

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The Characteristic of breakdown Particle Contaminated Model GIS with Epoxy Coated Electrodes (모의 GIS 내부에 파티클 유입시 코팅전극의 절연파괴 특성)

  • Koo, K.S.;Lee, D.Z.;Kwak, H.R.;Kim, Y.C.;Park, J.S.;Park, H.Y.
    • Proceedings of the KIEE Conference
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    • 2002.07c
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    • pp.1887-1889
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    • 2002
  • One of the most frequent sources of the accident is metal contaminant in GIS. This paper deals with the characteristics of breakdown voltage of metallic particles using electrodes of various epoxy coating thickness. As experimental results, breakdown voltage of the thickly coated electrode is higher than that of thinly coated electrode. It is considered that resistance of the epoxy coating impedes the development of pre-discharges in the gas.

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FT-IR Study of Dopant-wool Interactions During PPy Deposition

  • Varesano Alessio;Aluigi Annalisa;Tonin Claudio;Ferrero Franco
    • Fibers and Polymers
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    • v.7 no.2
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    • pp.105-111
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    • 2006
  • Coating the fibre surface by in situ oxidative chemical polymerisation of polypyrrole (using $FeCl_3$ as oxidant) is a readily industrial applicable way to give electrical properties to wool with good ageing stability [1], although pre-treatments are required to avoid damage of the cuticle surface due to the acidic condition of the process. FT-IR and EDX analysis reveal that organic sulphonates and sulphates, used as dopants, are absorbed by wool, while chlorine ions are preferably embedded on the polypyrrole layer. The resulting electrical conductivity seems mainly due to the presence of chlorine as counter-ion of polypyrrole; nevertheless, the presence of arylsulphonate in the polymerisation bath increases the electrical conductivity of the coating layer.

A Case Study on the Assessment of Damaged Cause for the Damaged Reinforced Concrete Pier

  • Chai, Won-Kyu;Kim, Kwang-Il;Son, Young-Hyun
    • International Journal of Safety
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    • v.10 no.1
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    • pp.16-21
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    • 2011
  • In this thesis, appearance inspection, compressive strength of concrete test, arrangement of bar inspection, survey, and bearing stress analysis were performed on a damaged coping of reinforced concrete pier to investigate the damage cause. According to the performed a series of inspections, it was found that the coping of pier was damaged during PSC (Pre-stressed Concrete) beam construction. In this thesis, the repair method for damaged pier was studied. The repair procedure used in this thesis was follows : chipping for damaged part, clean by high-pressure, installation of wire mesh, coating of surface hardening, construction of section restoration material, copula grinding, and prevent coating for far-infrared radiation.

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Influence of processing parameters for adhesion strength of TiN films prepared by AIP technique

  • Fang, W.;Ju, Yun-Gon;Jo, Dong-Yul;Yun, Jae-Hong;Song, Gi-O;Zhang, S.H.
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2007.11a
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    • pp.140-141
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    • 2007
  • The arc ion plating (AIP) technique has been used widely for thin coating in the area of surface engineering. The TiN coating is important in the field of dies, cutting tools and other mechanical parts. When forming the TiN films by AIP technique, the processing parameters such as arc power, bias voltage, working pressure, temperature of substrate and pre-treatment affected the adhesion respectively. The results of scratch test revealed that the adhesion strength was influenced by arc power most strongly. And a sequence of the importance of each parameters has been obtained. The crystal structure and cross-section of TiN films are also be investigated.

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Integration and Control Technology of GaAs Bonding System using DeviceNet (DeviceNet 을 채용한 GaAs 본딩 시스템의 통합 제어기술)

  • 송준엽;이승우;임선종;김원경;배영걸
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.10a
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    • pp.1376-1379
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    • 2004
  • This study is designed integration and control system of GaAs bonding system consisted of multi-processing using DeviceNet and GEM-Protocol. Developing bonding system is composed of resin coating, pre-baking pre-aligner, bonding, material handler(flip robot), and wafer cassette, etc. This system has process-fluent of each a process and share information using GEM-protocol. This study devised virtual bonding simulator to control and to monitor bonding system efficiently. Also we can verify optimizing of system previously through a virtual bonding simulator.

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Mechanical and electro-mechanical analysis in differently stabilized GdBCO coated conductor tapes with stainless steel substrate

  • Nisay, Arman R.;Shin, Hyung-Seop
    • Progress in Superconductivity and Cryogenics
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    • v.15 no.2
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    • pp.29-33
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    • 2013
  • The understanding of the strain dependence of critical current, $I_c$, in the reversible region is important for the evaluation of the performance of coated conductor (CC) tapes in practical applications. In this study, the stress/strain tolerance of $I_c$ in GdBCO CC tapes with stainless steel substrate stabilized by additional Cu and brass laminate was analyzed quantitatively through $I_c$-strain measurement at 77 K under self-field. The variation in irreversible strain limits of CC tapes by the addition of stabilizing layers was analyzed through the consideration of the pre-strain induced on the GdBCO coating film. The results were then compared with the ones previously reported for GdBCO CC tapes with Hastelloy substrate. As a result, GdBCO CC tapes with stainless steel substrate showed much higher strain tolerance of $I_c$ as compared with those adopting Hastelloy substrate.

A Study on Low Temperature Phosphating for Cold Forming (냉간 가공용 인산염 피막처리의 저온화에 관한 연구)

  • 이만식;정충택;이광호;김준호;이근대;홍성수
    • Journal of the Korean institute of surface engineering
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    • v.35 no.5
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    • pp.279-288
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    • 2002
  • Zinc phosphating for cold forming of steel was studied with emphasis on decreasing phosphating temperature. To lower phosphating temperature, some techniques, such as adding Cu ion into bath, using activator in the form of pre-dip, and aeration in bath, instead of using conventional accelerator, namely oxidizing agent, have been tried. It was revealed that phosphating, leading to coatings of Improved uniformity and fine crystal size, can be carried out using above techniques at lower temperature ($55^{\circ}C$) compared to conventional phosphating temperature ($80 ~ 90^{\circ}C$ ). Under present condition, it was seen that optimum concentrations of Cu ion in phosphating bath and activator in pre-dip are 0.015% (w/w) and 2.0 g/1, respectively. The coating weight was within the range of 15 ~ 20 g/$\m^2$. When lubricant was applied into phosphating coatings, the amount of lubricating component (total soap) was found to be 6 ~ 10 g/$\m^2$ and the lubricated panel revealed excellent lubricating properties.

A Study on Low Temperature Phosphating for Cold Forming (냉간 가공용 인산염 피막처리의 저온화에 관한 연구)

  • 이만식;정충택;이광호;김준호;이근대;홍성수
    • Journal of the Korean institute of surface engineering
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    • v.36 no.1
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    • pp.59-68
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    • 2003
  • Zinc phosphating for cold forming of steel was studied with emphasis on decreasing phosphating temperature. To lower phosphating temperature, some techniques, such as adding Cu ion into bath, using activator in the form of pre-dip, and aeration in bath, instead of using conventional accelerator, namely oxidizing agent, have been tried. It was revealed that phosphating, leading to coatings of improved uniformity and fine crystal size, can be carried out using above techniques at lower temperature (55$^{\circ}C$) compared to conventional phosphating temperature ($80∼90^{\circ}C$). Under present condition, it was seen that optimum concentrations of Cu ion in phosphating bath and activator in pre-dip are 0.015 % (w/w) and 2.0 g/1, respectively. The coating weight was within the range of $\15∼20 g/m^2$. When lubricant was applied into phosphating coatings, the amount of lubricating component (total soap) was found to be$ 6∼10 g/\m^2$ and the lubricated panel revealed excellent lubricating properties.